3,5-Dimethyl-2,6-dibromopyridine
- CAS No.
- 117846-58-9
- Chemical Name:
- 3,5-Dimethyl-2,6-dibromopyridine
- Synonyms
- 3,5-Dimethyl-2,6-dibromopyridine;Pyridine, 2,6-dibromo-3,5-dimethyl-;3,5-Dimethyl-2,6-dibromopyridine ISO 9001：2015 REACH
- CBNumber:
- CB62509974
- Molecular Formula:
- C7H7Br2N
- Molecular Weight:
- 264.95
- MDL Number:
- MFCD00234283
- MOL File:
- 117846-58-9.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Product description | Number | Pack Size | Price |
| 2,6-Dibromo-3,5-dimethylpyridine | B426288 | 100mg | $60 |
| 2,6-Dibromo-3,5-dimethylpyridine | X9223 | 250mg | $89 |
| 2,6-Dibromo-3,5-dimethylpyridine | OR315120 | 1g | $99 |
| 2,6-Dibromo-3,5-dimethylpyridine 97% | 3H32-9-8M | 1g | $117 |
| 2,6-Dibromo-3,5-dimethylpyridine | X9223 | 1g | $130 |
| More product size | |||
3,5-Dimethyl-2,6-dibromopyridine price More Price(18)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | B426288 | 2,6-Dibromo-3,5-dimethylpyridine | 117846-58-9 | 100mg | $60 | 2021-12-16 | Buy |
| AK Scientific | X9223 | 2,6-Dibromo-3,5-dimethylpyridine | 117846-58-9 | 250mg | $89 | 2021-12-16 | Buy |
| Apolloscientific | OR315120 | 2,6-Dibromo-3,5-dimethylpyridine | 117846-58-9 | 1g | $99 | 2021-12-16 | Buy |
| SynQuest Laboratories | 3H32-9-8M | 2,6-Dibromo-3,5-dimethylpyridine 97% | 117846-58-9 | 1g | $117 | 2021-12-16 | Buy |
| AK Scientific | X9223 | 2,6-Dibromo-3,5-dimethylpyridine | 117846-58-9 | 1g | $130 | 2021-12-16 | Buy |
3,5-Dimethyl-2,6-dibromopyridine Chemical Properties,Uses,Production
Uses
3,5-Dimethyl-2,6-dibromopyridine is an important intermediate in organic synthesis, mainly used in pharmaceutical intermediates, organic synthesis, and organic solvents. It can also be used in dye production, pesticide production, and fragrance production.
Synthesis
591-22-0
117846-58-9
The general procedure for the synthesis of 3,5-dimethyl-2,6-dibromopyridine from 3,5-dimethylpyridine was as follows: bromine (Br2, 5.64 mL, 110 mmol) was added dropwise to a fuming sulfuric acid solution (40 mL) of 3,5-dimethylpyridine (5.35 g, 50 mmol) under stirring at 177 K. The reaction was carried out in the following manner. The temperature was maintained and stirring of the reaction mixture was continued for 30 minutes. Subsequently, the reaction system was slowly warmed to 353 K and refluxed at this temperature for 36 hours. Upon completion of the reaction, the solution was cooled to room temperature and slowly poured into water. The reaction mixture was neutralized with aqueous sodium hydroxide (NaOH). The crude product was isolated by filtration. The crude product was purified by column chromatography (eluent: dichloromethane) to yield 3,5-dimethyl-2,6-dibromopyridine (10.71 g, 80% yield) as a white solid with a melting point of 102-103 °C. The product was purified by column chromatography. The structure of the product was confirmed by the following characterization data: 1H NMR (400 MHz, CDCl3): δ 7.35 (s, 1H, pyridinium-H), 2.30 (s, 6H, -CH3); 13C NMR (100 MHz, CDCl3): δ 141.11, 139.51, 134.21, 20.96; IR (KBr, ν, cm- 1): 3132, 1585, 1535, 1386, 1082, 974, 705.
References
[1] Tetrahedron Letters, 2013, vol. 54, # 43, p. 5791 - 5794
[2] Tetrahedron Letters, 2013, vol. 54, # 51, p. 7024 - 7028
[3] Journal of the Brazilian Chemical Society, 2016, vol. 27, # 11, p. 1989 - 1997
[4] Acta Crystallographica Section C: Crystal Structure Communications, 2006, vol. 62, # 10, p. o590-o592
3,5-Dimethyl-2,6-dibromopyridine Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49977 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29794 | 58 |
| ANHUI WITOP BIOTECH CO., LTD | +8615255079626 | eric@witopchemical.com | China | 23541 | 58 |
| Dideu Industries Group Limited | +86-29-89586680 +86-15129568250 | 1026@dideu.com | China | 18895 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52705 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25356 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 | market18@leapchem.com | China | 24597 | 58 |
| PT CHEM GROUP LIMITED | +86-85511178; | peter68@ptchemgroup.com | China | 35425 | 58 |
| GIHI CHEMICALS CO.,LIMITED | +86-571-86217390; +8618058761490 | info@gihichemicals.com | China | 49968 | 58 |
View Lastest Price from 3,5-Dimethyl-2,6-dibromopyridine manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
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2025-11-18 | 3,5-Dimethyl-2,6-dibromopyridine
117846-58-9
|
US $1.10 / g | 1g | 99.00% | 100 Tons min | Dideu Industries Group Limited | |
 |
2020-05-13 | 3,5-Dimethyl-2,6-dibromopyridine
117846-58-9
|
US $0.00-0.00 / Kg | 1KG | 99.0% | 500 MT | Shaanxi Dideu Medichem Co. Ltd | |
 |
2019-12-23 | 3,5-Dimethyl-2,6-dibromopyridine
117846-58-9
|
US $1.00 / KG | 1KG | 97%-99.9% | 100kg | Career Henan Chemical Co |
-
- 3,5-Dimethyl-2,6-dibromopyridine
117846-58-9
- US $1.10 / g
- 99.00%
- Dideu Industries Group Limited
-
- 3,5-Dimethyl-2,6-dibromopyridine
117846-58-9
- US $0.00-0.00 / Kg
- 99.0%
- Shaanxi Dideu Medichem Co. Ltd
-
- 3,5-Dimethyl-2,6-dibromopyridine
117846-58-9
- US $1.00 / KG
- 97%-99.9%
- Career Henan Chemical Co
