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3-bromo-5-methylaniline

3-bromo-5-methylaniline Structure
3-bromo-5-methylaniline structure
CAS No.
74586-53-1
Chemical Name:
3-bromo-5-methylaniline
Synonyms
3-AMino-5-broMotoluene;3-bromo-5-methylaniline;3-Bromo-5-methylbenzenamine;3-Bromo-5-methylaniline,98%;BenzenaMine,3-broMo-5-Methyl-;3-Amino-5-bromotoluene, 5-Bromo-m-toluidine
CBNumber:
CB6908751
Molecular Formula:
C7H8BrN
Molecular Weight:
186.05
MDL Number:
MFCD11845553
MOL File:
74586-53-1.mol
MSDS File:
SDS
Last updated:2026-05-28 03:45:31
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3-bromo-5-methylaniline Properties

Melting point 37 °C
Boiling point 150-151 °C(Press: 15 Torr)
Density 1.498±0.06 g/cm3(Predicted)
storage temp. Keep in dark place,Inert atmosphere,Room temperature
form Powder
pka 3.65±0.10(Predicted)
color Brown
Water Solubility Slightly soluble in water.

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H302-H312-H315-H319-H332-H335
Precautionary statements  P261-P280-P304+P340-P305+P351+P338-P405-P501a
HazardClass  6.1
HS Code  2921430090
NFPA 704
0
2 0

3-bromo-5-methylaniline price More Price(52)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical B6015 3-Bromo-5-methylaniline 74586-53-1 5G $173 2026-04-30 Buy
TCI Chemical B6015 3-Bromo-5-methylaniline 74586-53-1 25G $691 2026-04-30 Buy
Apolloscientific OR42210 3-Bromo-5-methylaniline >97% 74586-53-1 5g $21 2026-06-04 Buy
Apolloscientific OR42210 3-Bromo-5-methylaniline >97% 74586-53-1 25g $37 2026-06-04 Buy
Apolloscientific OR42210 3-Bromo-5-methylaniline >97% 74586-53-1 100g $111 2026-06-04 Buy
Product number Packaging Price Buy
B6015 5G $173 Buy
B6015 25G $691 Buy
OR42210 5g $21 Buy
OR42210 25g $37 Buy
OR42210 100g $111 Buy

3-bromo-5-methylaniline Chemical Properties, Uses, Production

Uses

3-Bromo-5-methylaniline is used as pharmaceutical intermediates and chemical intermediate.

Synthesis

3-BROMO-5-NITROTOLUENE

52488-28-5

3-bromo-5-methylaniline

74586-53-1

General procedure for the synthesis of 3-bromo-5-methylaniline from 3-bromo-5-nitrotoluene: 1-bromo-3-methyl-5-nitrobenzene (5 g, 23.1 mmol) was dissolved in a mixed solvent of dioxane/water (3:1, 40 mL), and zinc powder (15 g, 231 mmol) and ammonium chloride (12.3 g, 231 mmol) were added sequentially. The reaction mixture was stirred at room temperature for 4 hours. After completion of the reaction, the reaction mixture was diluted with water and extracted with ethyl acetate. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 3-bromo-5-methylaniline (4.0 g, 93% yield) as a brown solid. Mass spectrometry analysis showed m/z (M+H) of 186.2.

References

[1] Patent: WO2014/149164, 2014, A1. Location in patent: Paragraph 001105
[2] Chemische Berichte, 1880, vol. 13, p. 963
[3] Chemische Berichte, 1881, vol. 14, p. 417
[4] Justus Liebigs Annalen der Chemie, 1878, vol. 192, p. 203
[5] Journal of the Chemical Society, 1929, p. 1255

3-bromo-5-methylaniline Preparation Products And Raw materials

Raw materials

3-Bromo-5-nitrotoluene Ammonium chloride Water ZINC 1,4-Dioxane

Preparation Products

1-Bromo-3-fluoro-5-methylbenzene 3-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

3-bromo-5-methylaniline Suppliers

Global Suppliers ( 135)
Supplier Tel Email Country ProdList Advantage
Alfa Aesar 400-6106006 saleschina@alfa-asia.com China 30103 84
Energy Chemical 400-0056266 sales8178@energy-chemical.com China 44850 61
Shijiazhuang Sdyano Fine Chemical Co., Ltd. 0311-89250318 13582355795 master@sjzsdyn.com China 2776 65
Wuhan Chemwish Technology Co., Ltd 86-027-67849912 sales@chemwish.com China 35884 56
JinYan Chemicals(ShangHai) Co.,Ltd. 13817811078 sales@jingyan-chemical.com China 9963 60
Jia Xing Isenchem Co.,Ltd 0573-85285100 18627885956 isenchem@163.com China 9389 66
Shanghai Longsheng chemical Co.,Ltd. 58099637 13585536065 sales@shlschem.com China 9880 59
Shanghai Harvest Chemical Industrial Co., Ltd. 15721252604 17321035817 sales@harvest-chem.com China 2829 64
Nanjing Chemlin Chemical Co., Ltd 025-83697070 13770331960 info@chemlin.com.cn China 16305 64
Shanghai Hanhong Scientific Co.,Ltd. 021-54306202 13764082696 info@hanhongsci.com China 42917 64
Supplier Advantage
Alfa Aesar 84
Energy Chemical 61
Shijiazhuang Sdyano Fine Chemical Co., Ltd. 65
Wuhan Chemwish Technology Co., Ltd 56
JinYan Chemicals(ShangHai) Co.,Ltd. 60
Jia Xing Isenchem Co.,Ltd 66
Shanghai Longsheng chemical Co.,Ltd. 59
Shanghai Harvest Chemical Industrial Co., Ltd. 64
Nanjing Chemlin Chemical Co., Ltd 64
Shanghai Hanhong Scientific Co.,Ltd. 64

View Latest Price from 3-bromo-5-methylaniline manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
3-bromo-5-methylaniline pictures 2019-09-03 3-bromo-5-methylaniline
74586-53-1
 $7.00 1KG 98% Career Henan Chemical Co

3-bromo-5-methylaniline Spectrum

3-bromo-5-methylaniline(74586-53-1)1HNMR

74586-53-1 (3-bromo-5-methylaniline) Related Search:

3-Bromo-5-nitrotoluene 5-Amino-3-bromobenzonitrile 3-Bromo-5-ethyl-benzenamine Benzenamine, 3-bromo-5-(difluoromethyl)- 3-Amino-5-bromotoluene, HCl
tert-butyl 3-bromo-5-methylphenylcarbamate

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3-bromo-5-methylaniline 3-Bromo-5-methylbenzenamine 3-Amino-5-bromotoluene, 5-Bromo-m-toluidine 3-AMino-5-broMotoluene BenzenaMine,3-broMo-5-Methyl- 3-Bromo-5-methylaniline,98% 74586-53-1 277-932-1