2-Bromo-n,n,4-trimethylaniline
- CAS No.
- 23667-06-3
- Chemical Name:
- 2-Bromo-n,n,4-trimethylaniline
- Synonyms
- 2-Bromo-n,n,4-trimethylaniline;2-bromo-N,N,4-trimethylbenzeneamine;Benzenamine, 2-bromo-N,N,4-trimethyl-
- CBNumber:
- CB7110304
- Molecular Formula:
- C9H12BrN
- Molecular Weight:
- 214.1
- MDL Number:
- MFCD07780654
- MOL File:
- Mol file
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302 |
| Precautionary statements | P280-P305+P351+P338 |
2-Bromo-n,n,4-trimethylaniline price More Price(18)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS47871 | 2-Bromo-N,N,4-trimethylaniline 97% | 23667-06-3 | 1g | $84 | 2026-06-04 | Buy |
| Activate Scientific | AS47871 | 2-Bromo-N,N,4-trimethylaniline 97% | 23667-06-3 | 5g | $291 | 2026-06-04 | Buy |
| aablocks | AA002NZF | 2-Bromo-N,N,4-trimethylaniline 98% | 23667-06-3 | 1g | $25 | 2026-05-28 | Buy |
| aablocks | AA002NZF | 2-Bromo-N,N,4-trimethylaniline 98% | 23667-06-3 | 5g | $115 | 2026-05-28 | Buy |
| aablocks | AA002NZF | 2-Bromo-N,N,4-trimethylaniline 98% | 23667-06-3 | 10g | $218 | 2026-05-28 | Buy |
2-Bromo-n,n,4-trimethylaniline Chemical Properties,Uses,Production
Synthesis
99-97-8
23667-06-3
General procedure for the synthesis of 2-bromo-N,N,4-trimethylaniline from N,N-dimethyl-p-toluidine: In a round-bottomed flask, N,N-dimethyl-p-toluidine (1 mmol) was mixed with 48% aqueous hydrobromic acid (1 mL) in dimethyl sulfoxide (DMSO, 1 mL). The reaction mixture was stirred at the indicated temperature for 1-4 hours. After completion of the reaction, it was cooled to room temperature and the pH of the reaction solution was adjusted to 7-8 with 4 M aqueous sodium hydroxide.Subsequently, the reaction mixture was extracted twice with ethyl acetate (EtOAc) and the organic phases were combined. The organic phase was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford the target product 2-bromo-N,N,4-trimethylaniline.
References
[1] Journal of Chemical Research, 2014, vol. 38, # 10, p. 593 - 596
[2] Synthesis, 2009, # 21, p. 3672 - 3676
[3] Synthetic Communications, 2010, vol. 40, # 19, p. 2954 - 2962
[4] Tetrahedron Letters, 2007, vol. 48, # 45, p. 7969 - 7973
[5] Chemische Berichte, 1908, vol. 41, p. 2117
2-Bromo-n,n,4-trimethylaniline Preparation Products And Raw materials
2-Bromo-n,n,4-trimethylaniline Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
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