10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
![10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Structure](CAS/20150408/GIF/4014-77-1.gif)
- CAS No.
- 4014-77-1
- Chemical Name:
- 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
- Synonyms
- 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol;Licarbazepine Impurity 5;Oxcarbazepine Impurity 27;10,11-dihydro-5H-dibenzo[b,f]azepin-10-o;5H-Dibenz[b,f]azepin-10-ol, 10,11-dihydro-;6,11-dihydro-5H-benzo[b][1]benzazepin-5-ol
- CBNumber:
- CB72604465
- Molecular Formula:
- C14H13NO
- Molecular Weight:
- 211.26
- MDL Number:
- MFCD22377561
- MOL File:
- 4014-77-1.mol
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H332-H335 |
| Precautionary statements | P261-P280-P305+P351+P338 |
10,11-dihydro-5H-dibenzo[b,f]azepin-10-o price More Price(25)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Synthonix | D57612 | 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% | 4014-77-1 | 250mg | $240 | 2026-05-06 | Buy |
| Synthonix | D57612 | 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% | 4014-77-1 | 100mg | $390 | 2026-05-06 | Buy |
| Synthonix | D57612 | 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% | 4014-77-1 | 1g | $610 | 2026-05-06 | Buy |
| Synthonix | D57612 | 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% | 4014-77-1 | 5g | $1790 | 2026-05-06 | Buy |
| aablocks | AA00D5UH | 10，11-Dihydro-5H-dibenzo[b，f]azepin-10-ol 98%(HPLC) | 4014-77-1 | 100mg | $143 | 2026-05-28 | Buy |
10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Chemical Properties, Uses, Production
Synthesis
![10-Oxo-10,11-Dihydro-5H-dibenz[b,f]azepine](/CAS/GIF/21737-58-6.gif)
21737-58-6
![10,11-dihydro-5H-dibenzo[b,f]azepin-10-o](/CAS/20150408/GIF/4014-77-1.gif)
4014-77-1
The general procedure for the synthesis of 10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol from 5H-dibenzo[b,f]azepin-10(11H)-one was as follows: 5H-dibenzo[b,f]azepin-10(11H)-one (350.0 g, 1.67 mol) was suspended in water (0.7 L) and methanol (2.8 L) in a mixed solvents. Sodium borohydride (76 g, 2.0 mol) was added in batches over 10 min without cooling and the reaction mixture was stirred continuously at 45 °C for 1 h. The reaction was completed by the addition of acetone (1.0 g, 2.0 mol). Upon completion of the reaction, acetone (350 mL) was added cautiously to quench the reaction and the reaction mixture was subsequently concentrated to a smaller volume. The target product was precipitated by the addition of water (700 mL) and the precipitate was collected and dried at 60-65 °C to afford (S)-10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol (315 g, 89.0% yield) as an off-white solid with a purity of >98%.
References
[1] Tetrahedron Letters, 2013, vol. 54, # 22, p. 2841 - 2844
10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Preparation Products And Raw materials
Raw materials
Preparation Products
10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Hangzhou Molcore Biopharmatech Co.,Ltd | 400-711-5280 86-571-81025280 | sales@molcore.com | China | 9957 | 58 |
| Aikon International Limited | 025-66061636 19370895928 | qqyang@aikonchem.com | China | 15810 | 58 |
| 3A Chemicals | 400-668-9898 | service@3achem.com | China | 20535 | 58 |
| Cool Pharm, Ltd | 021-58581007 18019463053 | sales@coolpharm.com | China | 9999 | 58 |
| Labnetwork lnc. | +86-27-50766799 +86-18062016861 | contact@labnetwork.com | China | 19981 | 58 |
| Shanghai Lanle Bird Industrial Co., Ltd. | 15021845385 | 765325601@qq.com | China | 3607 | 58 |
| Zhejiang Lianshuo Biotechnology Co., Ltd. | 18616526224 | lianshuo@vip.126.com | China | 9605 | 58 |
| Standardpharm Co. Ltd. | 86-714-3992388 | overseasales1@yongstandards.com | United States | 14320 | 58 |
| Shanghai Kaiwei Chemical Technology Co., Ltd. | 021-58461859 15821823057 | service@aiviche.com | China | 49299 | 58 |
View Latest Price from 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
![10,11-dihydro-5H-dibenzo[b,f]azepin-10-o pictures](/ProductImageEN/2024-07/Small/e31ed0b3-48ba-45f2-9885-ae28fec4e09f.png) |
2026-08-07 | 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
4014-77-1
|
$1.00-2.00 | 1KG | 99% | 100000KG | Shaanxi Dideu Medichem Co. Ltd |
-
- 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
4014-77-1
- $1.00-2.00
- 99%
- Shaanxi Dideu Medichem Co. Ltd
