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ChemicalBook >> CAS DataBase List >>10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Structure
10,11-dihydro-5H-dibenzo[b,f]azepin-10-o structure
CAS No.
4014-77-1
Chemical Name:
10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
Synonyms
10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol;Licarbazepine Impurity 5;Oxcarbazepine Impurity 27;10,11-dihydro-5H-dibenzo[b,f]azepin-10-o;5H-Dibenz[b,f]azepin-10-ol, 10,11-dihydro-;6,11-dihydro-5H-benzo[b][1]benzazepin-5-ol
CBNumber:
CB72604465
Molecular Formula:
C14H13NO
Molecular Weight:
211.26
MDL Number:
MFCD22377561
MOL File:
4014-77-1.mol
Last updated:2026-05-28 04:58:25
Product description Number Pack Size Price
10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% D57612 250mg $240
10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% D57612 100mg $390
10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% D57612 1g $610
10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% D57612 5g $1790
10，11-Dihydro-5H-dibenzo[b，f]azepin-10-ol 98%(HPLC) AA00D5UH 100mg $143
Request For Quotation

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H332-H335
Precautionary statements  P261-P280-P305+P351+P338

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o price More Price(31)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Synthonix D57612 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% 4014-77-1 250mg $240 2026-05-06 Buy
Synthonix D57612 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% 4014-77-1 100mg $390 2026-05-06 Buy
Synthonix D57612 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% 4014-77-1 1g $610 2026-05-06 Buy
Synthonix D57612 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 98% 4014-77-1 5g $1790 2026-05-06 Buy
aablocks AA00D5UH 10，11-Dihydro-5H-dibenzo[b，f]azepin-10-ol 98%(HPLC) 4014-77-1 100mg $143 2026-05-28 Buy
Product number Packaging Price Buy
D57612 250mg $240 Buy
D57612 100mg $390 Buy
D57612 1g $610 Buy
D57612 5g $1790 Buy
AA00D5UH 100mg $143 Buy

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Chemical Properties,Uses,Production

Synthesis

10-Oxo-10,11-Dihydro-5H-dibenz[b,f]azepine

21737-58-6

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

4014-77-1

The general procedure for the synthesis of 10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol from 5H-dibenzo[b,f]azepin-10(11H)-one was as follows: 5H-dibenzo[b,f]azepin-10(11H)-one (350.0 g, 1.67 mol) was suspended in water (0.7 L) and methanol (2.8 L) in a mixed solvents. Sodium borohydride (76 g, 2.0 mol) was added in batches over 10 min without cooling and the reaction mixture was stirred continuously at 45 °C for 1 h. The reaction was completed by the addition of acetone (1.0 g, 2.0 mol). Upon completion of the reaction, acetone (350 mL) was added cautiously to quench the reaction and the reaction mixture was subsequently concentrated to a smaller volume. The target product was precipitated by the addition of water (700 mL) and the precipitate was collected and dried at 60-65 °C to afford (S)-10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol (315 g, 89.0% yield) as an off-white solid with a purity of >98%.

References

[1] Tetrahedron Letters, 2013, vol. 54, # 22, p. 2841 - 2844

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Preparation Products And Raw materials

Raw materials

10-Oxo-10,11-Dihydro-5H-dibenz[b,f]azepine Water Methanol Sodium borohydride

Preparation Products

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Suppliers

Global( 34)Suppliers
Supplier Tel Email Country ProdList Advantage
Shaanxi Dideu Medichem Co. Ltd 		+86-29-81139210 17389186172 1077@dideu.com China 3796 58
Standardpharm Co. Ltd. 		86-714-3992388 overseasales1@yongstandards.com United States 14332 58
Labnetwork lnc. 		+86-27-50766799 +8618062016861 contact@labnetwork.com China 19987 58
Coresyn Pharmatech Co., Ltd. 		+86-571-86626709 +86-18157142896 cbc@coresyn.com China 9984 58
Aladdin Scientific 		tp@aladdinsci.com United States 52923 58
Amadis Chemical Company Limited 		571-89925085 sales@amadischem.com China 131956 58
Hangzhou Molcore Biopharmatech Co.,Ltd 400-711-5280 86-571-81025280 sales@molcore.com China 9967 58
Aikon International Limited 025-66061636 19370895928 qqyang@aikonchem.com China 15812 58
3A Chemicals 400-668-9898 service@3achem.com China 20557 58
Shanghai Jizhi Biochemical Technology Co. Ltd. 021-4009004166/18616739031 18616739031 3007523370@qq.com China 52678 58
Supplier Advantage
Shaanxi Dideu Medichem Co. Ltd 		58
Standardpharm Co. Ltd. 		58
Labnetwork lnc. 		58
Coresyn Pharmatech Co., Ltd. 		58
Aladdin Scientific 		58
Amadis Chemical Company Limited 		58
Hangzhou Molcore Biopharmatech Co.,Ltd 58
Aikon International Limited 58
3A Chemicals 58
Shanghai Jizhi Biochemical Technology Co. Ltd. 58

View Lastest Price from 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
10,11-dihydro-5H-dibenzo[b,f]azepin-10-o pictures 2025-12-12 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
4014-77-1
 $1.00-2.00 1KG 99% 100000KG Shaanxi Dideu Medichem Co. Ltd

4014-77-1(10,11-dihydro-5H-dibenzo[b,f]azepin-10-o)Related Search:

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10,11-dihydro-5H-dibenzo[b,f]azepin-10-o 6,11-dihydro-5H-benzo[b][1]benzazepin-5-ol Licarbazepine Impurity 5 5H-Dibenz[b,f]azepin-10-ol, 10,11-dihydro- Oxcarbazepine Impurity 27 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol 4014-77-1