(3-Methoxy-pyridin-2-yl)-methanol
- CAS No.
- 51984-46-4
- Chemical Name:
- (3-Methoxy-pyridin-2-yl)-methanol
- Synonyms
- 3-Methoxy-2-PyridineMethanol;3-methoxy-2-pyridyl)methanol;2-Pyridinemethanol, 3-methoxy-;(3-Methoxy-pyridin-2-yl)-methanol;2-(Hydroxymethyl)-3-methoxypyridine
- CBNumber:
- CB8674807
- Molecular Formula:
- C7H9NO2
- Molecular Weight:
- 139.15
- MDL Number:
- MFCD08234494
- MOL File:
- 51984-46-4.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302 |
| Precautionary statements | P280-P305+P351+P338 |
(3-Methoxy-pyridin-2-yl)-methanol price More Price(44)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS111181 | (3-Methoxypyridin-2-yl)methanol 97% | 51984-46-4 | 1g | $238 | 2026-06-04 | Buy |
| Activate Scientific | AS111181 | (3-Methoxypyridin-2-yl)methanol 97% | 51984-46-4 | 5g | $882 | 2026-06-04 | Buy |
| Matrix Scientific | 179451 | (3-Methoxypyridin-2-yl)-methanol | 51984-46-4 | 250.00mg | $43 | 2026-05-18 | Buy |
| Matrix Scientific | 179451 | (3-Methoxypyridin-2-yl)-methanol | 51984-46-4 | 1.00g | $150 | 2026-05-18 | Buy |
| Matrix Scientific | 179451 | (3-Methoxypyridin-2-yl)-methanol | 51984-46-4 | 5.00g | $711 | 2026-05-18 | Buy |
(3-Methoxy-pyridin-2-yl)-methanol Chemical Properties, Uses, Production
Synthesis
31224-43-8
124-41-4
51984-46-4
GENERAL STEPS: To a round-bottomed flask containing 3-fluoropyridine-2-aldehyde (400 mg, 3.20 mmol) was added a methanolic solution of sodium methanolate (15 mL, 7.50 mmol, 0.5 M). The reaction mixture was stirred at 80 °C for 4 hours. Upon completion of the reaction, the mixture was cooled to 0 °C in an ice bath, followed by the addition of sodium borohydride (90 mg, 2.38 mmol) and continued stirring at 0 °C for 20 min. After termination of the reaction, ice water was added to the mixture. The solvent was removed by concentration under reduced pressure and the resulting residue was purified by ISCO medium pressure liquid chromatography (MPLC) with an elution gradient of 40-100% ethyl acetate/hexane to afford (3-methoxypyridin-2-yl)methanol as a white solid (200 mg, 45.0% yield). The product was characterized by 1H NMR (DMSO-d6): δ 8.11 (dd, 1H), 7.41 (dd, 1H), 7.31 (dd, 1H), 4.83 (t, 1H), 4.54 (d, 2H), 3.82 (s, 3H). Mass spectrometry (MS) showed the molecular ion peak (M+H)+ m/z = 140.
References
[1] Patent: WO2009/27746, 2009, A1. Location in patent: Page/Page column 115
(3-Methoxy-pyridin-2-yl)-methanol Preparation Products And Raw materials
Raw materials
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Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai Ennopharm Co., Ltd. | +86 (21) 6435-5022 | China | 4263 | 65 | |
| SynAsst Chemical. | 021-60343070 | China | 12731 | 55 | |
| ShangHai AmK Pharmaceutical Technology Co., Ltd. | 微信 18019252918 18019252918 | sale@amkchem.com | China | 14982 | 55 |
| Hangzhou Milestone Pharmtech Co., Ltd. | 0571-82896630 18969958410 | sales_hz@milestonepharmtech.com | China | 4906 | 55 |
| JW & Y Pharmlab Co., Ltd. | 021-64340559 | xinyu_shi@jwypharmlab.com.cn | China | 11999 | 58 |
| ShangHai Movin Pharmaceutical Co., Ltd. | 13681854265 | info@moenpharm.com | China | 488 | 55 |
| Shanghai YuanYe Biotechnology Co., Ltd. | 15026964105 | 2881489226@qq.com | China | 89667 | 60 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Shanghai Anmike Chemical Co. Ltd. | 微信 18019252918 18019252918 | sale@amkchem.com | China | 9988 | 55 |
| Sichuan BoYou Biotechnology Co., Ltd. | 028-65791793 18140026355 | 568470422@qq.com | China | 9961 | 58 |
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