3-FLUORO-5-FORMYL-2-METHOXYPYRIDINE
- CAS No.
- 884494-73-9
- Chemical Name:
- 3-FLUORO-5-FORMYL-2-METHOXYPYRIDINE
- Synonyms
- 3-FLUORO-5-FORMYL-2-METHOXYPYRIDINE;5-FLUORO-6-METHOXY-PYRIDINE-3-CARBALDEHYDE;5-Fluoro-6-methoxy-3-pyridinecarboxaldehyde;3-Pyridinecarboxaldehyde, 5-fluoro-6-methoxy-;5-fluoro-6-methoxypyridine-3-carbaldehyde - [F87722]
- CBNumber:
- CB9111350
- Molecular Formula:
- C7H6FNO2
- Molecular Weight:
- 155.13
- MDL Number:
- MFCD04112587
- MOL File:
- Mol file
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H332-H335 |
| Precautionary statements | P261-P280-P305+P351+P338 |
| Hazard Codes | Xn |
| Risk Statements | 22 |
| HS Code | 2933399990 |
3-FLUORO-5-FORMYL-2-METHOXYPYRIDINE price More Price(9)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | PC201349 | 5-Fluoro-6-methoxynicotinaldehyde 98% | 884494-73-9 | 1g | $301 | 2021-12-16 | Buy |
| Matrix Scientific | 119595 | 5-Fluoro-6-methoxynicotinaldehyde 95+% | 884494-73-9 | 250mg | $490 | 2021-12-16 | Buy |
| Apolloscientific | PC201349 | 5-Fluoro-6-methoxynicotinaldehyde 98% | 884494-73-9 | 250mg | $128 | 2021-12-16 | Buy |
| Matrix Scientific | 119595 | 5-Fluoro-6-methoxynicotinaldehyde 95+% | 884494-73-9 | 1g | $1224 | 2021-12-16 | Buy |
| AK Scientific | Z5255 | 5-Fluoro-6-methoxynicotinaldehyde | 884494-73-9 | 1g | $1702 | 2021-12-16 | Buy |
3-FLUORO-5-FORMYL-2-METHOXYPYRIDINE Chemical Properties,Uses,Production
Synthesis
959616-65-0
884494-73-9
Dess-Martin periodinane (DMP, 27.37 g, 64.4 mmol) was added batchwise to a stirred solution of (5-fluoro-6-methoxypyridin-3-yl)methanol (6.8 g, 43.83 mmol) in dichloromethane (DCM, 150 mL) at 0 °C. The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, the reaction mixture was filtered through diatomaceous earth and washed with DCM (3 x 50 mL). The combined organic phases were washed sequentially with saturated aqueous NaHCO3 solution (200 mL), water (100 mL) and brine (150 mL), dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by column chromatography (silica gel 60-120 mesh, 0-15% petroleum ether solution of ethyl acetate) to obtain 5-fluoro-6-methoxynicotinaldehyde (6.0 g, 89% yield) as a white solid.
References
[1] Patent: EP2022793, 2009, A1. Location in patent: Page/Page column 73
[2] Patent: WO2015/158427, 2015, A1. Location in patent: Page/Page column 85
[3] Patent: EP2022793, 2009, A1. Location in patent: Page/Page column 73
3-FLUORO-5-FORMYL-2-METHOXYPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
3-FLUORO-5-FORMYL-2-METHOXYPYRIDINE Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| Jinan Carbotang Biotech Co.,Ltd. | +8615866703830 | figo.gao@foxmail.com | China | 8497 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
| CD Chemical Group Limited | +8615986615575 | info@codchem.com | China | 20342 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 | market18@leapchem.com | China | 43339 | 58 |
| Suzhou ARTK Medchem Co., Ltd. | +86-512-68323658 +86-18168183658 | sales1@artkmedchem.com | China | 39002 | 58 |
| Cochemical Co. Ltd. | +86-029-86115547 +86-17791676824 | sales@cochemical.com | China | 3952 | 58 |
| Allfluoro pharmaceutical co. ltd. | +86-400-0216110 +86-15958047586 | sales@allfluoro.com | China | 11385 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
