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tert-Butyl 3-bromobenzylcarbamate

tert-Butyl 3-bromobenzylcarbamate Structure
tert-Butyl 3-bromobenzylcarbamate structure
CAS No.
171663-13-1
Chemical Name:
tert-Butyl 3-bromobenzylcarbamate
Synonyms
N-Boc-3-broMobenzylaMine;Tert-Butyl 3-Bromobenzylcarbamat;tert-Butyl 3-bromobenzylcarbamate;1-(Boc-aMinoMethyl)-3-broMobenzene;tert-butyl N-[(3-bromophenyl)methyl]carbamate;(3-BROMO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER;N-[(3-Bromophenyl)methyl]-carbamic acid tert-butyl ester;N-[(3-Bromophenyl)Methyl]-Carbamic Acid 1,1-Dimethylethyl Ester;Carbamic acid, N-[(3-bromophenyl)methyl]-, 1,1-dimethylethyl ester
CBNumber:
CB9823305
Molecular Formula:
C12H16BrNO2
Molecular Weight:
286.16
MDL Number:
MFCD08703139
MOL File:
171663-13-1.mol
MSDS File:
SDS
Last updated:2026-09-12 18:56:36
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tert-Butyl 3-bromobenzylcarbamate Properties

Melting point 59-60 °C
Boiling point 374.3±25.0 °C(Predicted)
Density 1.319±0.06 g/cm3(Predicted)
storage temp. 2-8°C
form solid
pka 12.15±0.46(Predicted)
color White

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H302
Precautionary statements  P280-P305+P351+P338
Hazard Codes  Xn
Risk Statements  22
HS Code  2924297099

tert-Butyl 3-bromobenzylcarbamate price More Price(40)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Biosynth WGA66313 tert-Butyl 3-bromobenzylcarbamate 171663-13-1 25g $454.25 2026-06-05 Buy
Biosynth WGA66313 tert-Butyl 3-bromobenzylcarbamate 171663-13-1 50g $779 2026-06-05 Buy
Biosynth WGA66313 tert-Butyl 3-bromobenzylcarbamate 171663-13-1 100g $1103 2026-06-05 Buy
Apolloscientific OR962712 tert-Butyl 3-bromobenzylcarbamate 98% 171663-13-1 1g $21 2026-06-04 Buy
Apolloscientific OR962712 tert-Butyl 3-bromobenzylcarbamate 98% 171663-13-1 5g $62 2026-06-04 Buy
Product number Packaging Price Buy
WGA66313 25g $454.25 Buy
WGA66313 50g $779 Buy
WGA66313 100g $1103 Buy
OR962712 1g $21 Buy
OR962712 5g $62 Buy

tert-Butyl 3-bromobenzylcarbamate Chemical Properties, Uses, Production

Synthesis

Di-tert-butyl dicarbonate

24424-99-5

3-Bromobenzylamine hydrochloride

39959-54-1

TERT-BUTYL 3-BROMOBENZYLCARBAMATE

171663-13-1

The general procedure for the synthesis of 1-(Boc-aminomethyl)-3-bromobenzene from 3-bromobenzylamine hydrochloride and di-tert-butyl dicarbonate was as follows: to 250 mL of dichloromethane were added 25 g (110 mmol) of 3-bromobenzylamine hydrochloride and 24.5 g (110 mmol) of di-tert-butyl dicarbonate followed by 15.6 mL (110 mmol) of triethylamine. The reaction mixture was stirred at room temperature for 16 hours. Upon completion of the reaction, the reaction mixture was washed with water and the organic and aqueous phases were separated by sedimentation. The organic phase was dried over anhydrous sodium sulfate and the solvent was subsequently evaporated to give 32.4 g (100% yield) of tert-butyl (3-bromobenzyl)carbamate in crystalline form.

References

[1] Patent: US2009/12129, 2009, A1. Location in patent: Page/Page column 21
[2] Patent: WO2006/18325, 2006, A1. Location in patent: Page/Page column 28 - 29
[3] Patent: US2016/332999, 2016, A1. Location in patent: Paragraph 0420; 0421
[4] Patent: WO2018/5794, 2018, A2. Location in patent: Page/Page column 94
[5] Organic Process Research and Development, 2011, vol. 15, # 6, p. 1247 - 1255

tert-Butyl 3-bromobenzylcarbamate Preparation Products And Raw materials

Raw materials

Di-tert-butyl dicarbonate 3-Bromobenzylamine hydrochloride 3-Bromobenzylamine Triethylamine Dichloromethane

Preparation Products

(3-Bromobenzyl)methylamine

tert-Butyl 3-bromobenzylcarbamate Suppliers

Global Suppliers ( 78)
Supplier Tel Email Country ProdList Advantage
Shandong Fande Pharmaceutical Technology Co., Ltd. 0531-00000000 15552883993 3180453864@qq.com China 109 58
Energy Chemical 400-0056266 sales8178@energy-chemical.com China 44850 61
Accela ChemBio Co.,Ltd. 021-50795510 4000665055 marketing@accelachem.com China 10972 64
Shanghai Sunway Pharmaceutical Technology Co., Ltd 13761987713 hxzheng@sunwaypharm.cn China 8663 57
Nanjing Norris-Pharm Technology Co., Ltd 13901585132 sales@norris-pharm.com China 8869 55
Shanghai Jian Chao Chemical Technology Co., Ltd. 150-2103-5486 18017383231 983544897@qq.com China 9335 55
Shanghai Sheepchem Co., Ltd. +86 (21) 6715-7650 sheepchem@163.com China 993 60
Shanghai Raise Chemical Technology Co.,Ltd 15026594951 rs@raise-chem.com China 4904 55
Amatek Scientific Co. Ltd. 0512-56316828 4008675858 sales@amateksci.com China 9848 55
Bide Pharmatech Ltd. 400-164-7117 18317119277 product02@bidepharm.com China 40000 60
Supplier Advantage
Shandong Fande Pharmaceutical Technology Co., Ltd. 58
Energy Chemical 61
Accela ChemBio Co.,Ltd. 64
Shanghai Sunway Pharmaceutical Technology Co., Ltd 57
Nanjing Norris-Pharm Technology Co., Ltd 55
Shanghai Jian Chao Chemical Technology Co., Ltd. 55
Shanghai Sheepchem Co., Ltd. 60
Shanghai Raise Chemical Technology Co.,Ltd 55
Amatek Scientific Co. Ltd. 55
Bide Pharmatech Ltd. 60

View Latest Price from tert-Butyl 3-bromobenzylcarbamate manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
TERT-BUTYL 3-BROMOBENZYLCARBAMATE pictures 2019-07-06 TERT-BUTYL 3-BROMOBENZYLCARBAMATE
171663-13-1
 $1.00 1KG 98% 200kg Career Henan Chemical Co

tert-Butyl 3-bromobenzylcarbamate Spectrum

TERT-BUTYL 3-BROMOBENZYLCARBAMATE(171663-13-1)1HNMR

171663-13-1 (tert-Butyl 3-bromobenzylcarbamate) Related Search:

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[(3-Bromo-4-fluorophenyl)methyl]-carbamic acid tert-butyl ester 4-Boc-7-bromo-2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepine 4-Boc-7-bromo-1,2,3,5-tetrahydro-benzo[e][1,4]diazepine-3-carboxylic acid 3-methyl ester tert-Butyl 3-bromobenzylcarbamate (R)-N-Boc-3-bromo-beta-phenylalanine
5-Bromo-3,4-dihydro-1H-isoquinoline-2-carboxylic acid tert-butyl ester tert-Butyl 7-bromo-3,4-dihydroisoquinoline-2(1H)-carboxylate 3-(3-Bromo-phenyl)-3-tert-butoxycarbonylamino-propionic acid (R)-2-(3-Bromo-phenyl)-piperazine-1-carboxylic acid tert-butyl ester (S)-N-(tert-Butoxycarbonyl)-3-amino-3-(3,5-dibromophenyl)propionic acid
2-(3-Bromophenyl)piperazine-1-carboxylic acid tert-butyl ester (3-bromophenyl)[(tert-butoxycarbonyl)amino]acetic acid (S)-(3-Bromo-phenyl)-tert-butoxycarbonylamino-acetic acid

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(3-BROMO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER 1-(Boc-aMinoMethyl)-3-broMobenzene N-Boc-3-broMobenzylaMine Carbamic acid, N-[(3-bromophenyl)methyl]-, 1,1-dimethylethyl ester N-[(3-Bromophenyl)Methyl]-Carbamic Acid 1,1-Dimethylethyl Ester tert-butyl N-[(3-bromophenyl)methyl]carbamate N-[(3-Bromophenyl)methyl]-carbamic acid tert-butyl ester Tert-Butyl 3-Bromobenzylcarbamat tert-Butyl 3-bromobenzylcarbamate 171663-13-1 amine|alkyl bromide| carboxylic ester