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| | 3-Acetyl-1-methylpyrrole Basic information | | Synthesis |
| | 3-Acetyl-1-methylpyrrole Chemical Properties |
| Boiling point | 148-150 °C15 mm Hg(lit.) | | density | 1.038 g/mL at 25 °C(lit.) | | refractive index | n20/D 1.538(lit.) | | Fp | >230 °F | | pka | -5.84±0.70(Predicted) | | form | liquid | | Specific Gravity | 1.061.038 | | InChI | 1S/C7H9NO/c1-6(9)7-3-4-8(2)5-7/h3-5H,1-2H3 | | InChIKey | SZYIVZGXCXFXDN-UHFFFAOYSA-N | | SMILES | CC(=O)c1ccn(C)c1 | | LogP | 0.968 (est) | | CAS DataBase Reference | 932-62-7(CAS DataBase Reference) |
| Hazard Codes | Xi | | Risk Statements | 36/37/38 | | Safety Statements | 26-37/39 | | WGK Germany | 3 | | HS Code | 2933998090 | | Storage Class | 10 - Combustible liquids | | Hazard Classifications | Eye Irrit. 2
Skin Irrit. 2
STOT SE 3 |
| | 3-Acetyl-1-methylpyrrole Usage And Synthesis |
| Synthesis | 
To a 25 mL suspension of 2-butanone containing tetrabutylammonium bromide (0.3 g, 1 mmol) and K2CO3 (1.6 g, 12 mmol) under stirring, 3-acetylpyrrole (1.1 g, 10 mmol) and methyl bromoethane (11 mmol) were added. The mixture was heated at 60 °C for 12 hours, and then the reaction was cooled to room temperature. The solvent was removed under reduced pressure. The residue was absorbed with H₂O/Et₂O (1:1, 50 mL), the organic layer was separated, dried (Na₂SO₄), and evaporated to give 3-acetyl-1-methylpyrrole. | | Uses | The enthalpy of formation of 3-acetyl-1-methylpyrrole in the condensed and gas phases was studied. | | Synthesis Reference(s) | The Journal of Organic Chemistry, 46, p. 839, 1981 DOI: 10.1021/jo00318a002 | | General Description | The enthalpy of formation of 3-acetyl-1-methylpyrrole in the condensed and gas phases was studied. |
| | 3-Acetyl-1-methylpyrrole Preparation Products And Raw materials |
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