Fructone

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CAS:6413-10-1
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  • 2026-05-19
  • CAS:6413-10-1
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Fructone Basic information
Product Name:Fructone
Synonyms:2-(2-methyl-1,3-dioxolan-2-yl)acetic acid ethyl ester;fructone,Ethyl acetoacetate ethylene glycol ketal;Ethyl 2-(2-methyl-1,3-dioxolan-2-yl);ethyl 2-(2-methyl-1,3-dioxolan-2-yl)ethanoate;ETHYLACETOACETATE ETHYLENE GLYCOL KETAL;ETHYLACETOACETATE ETHYLENE KETAL;ETHYL METHYL DIOXOLANE ACETATE;ETHYL-2-METHYL-1,3-DIOXOLANE-2-ACETATE
CAS:6413-10-1
MF:C8H14O4
MW:174.19
EINECS:229-114-0
Product Categories:organic chemical;6413-10-1
Mol File:6413-10-1.mol
Fructone Structure
Fructone Chemical Properties
Boiling point 90 °C
density 1.0817 (rough estimate)
vapor pressure 1.08hPa at 20℃
refractive index 1.4310-1.4350
FEMA 4477 | ETHYL ACETOACETATE ETHYLENEGLYCOL KETAL
Fp 93.00°C
storage temp. Keep in dark place,Sealed in dry,Room Temperature
form clear liquid
color Colorless to Almost colorless
Odorat 100.00 %. sweet fruity apple green tropical plum woody
Odor Typefruity
biological sourcesynthetic
Water Solubility 124.8g/L at 20℃
JECFA Number1969
Major Applicationflavors and fragrances
Cosmetics Ingredients FunctionsPERFUMING
InChI1S/C8H14O4/c1-3-10-7(9)6-8(2)11-4-5-12-8/h3-6H2,1-2H3
InChIKeyXWEOGMYZFCHQNT-UHFFFAOYSA-N
SMILESO=C(OCC)CC1(C)OCCO1
LogP0.8 at 35℃
CAS DataBase Reference6413-10-1(CAS DataBase Reference)
NIST Chemistry ReferenceEthyl acetoacetate ethylene acetal(6413-10-1)
EPA Substance Registry System1,3-Dioxolane-2-acetic acid, 2-methyl-, ethyl ester (6413-10-1)
Safety Information
Hazard Codes Xi
WGK Germany WGK 2
RTECS JH6762500
TSCA TSCA listed
HS Code 2932.99.9090
Storage Class10 - Combustible liquids
MSDS Information
Fructone Usage And Synthesis
Chemical Properties Ethyl (2-Methyl-[1,3]dioxolan-2-yl)-acetate is not found in nature. It is a colorless liquid, d2041.084–1.092, n20D 1.431–1.435, with a strong, fruity, apple-like, slightly green odor. It can be prepared by acetalization of ethyl acetoacetate with ethylene glycol.
Very slightly soluble in water, soluble in alcohol and Propylene glycol, miscible with most perfume oils.
Usesflavors and fragrances
Trade nameFructone (IFF), Jasmaprunat (Symrise)
Synthesis
Ethyl acetoacetate

141-97-9

Ethylene glycol

107-21-1

Fructone

6413-10-1

Ethyl acetoacetate (39.0 g, 0.3 mol), ethylene glycol (55.8 g, 0.9 mol), and toluene (200 mL) were added to a 250 mL three-necked, round-bottomed flask fitted with a mechanical stirrer, thermometer, Dean-Stark manifold, and reflux condenser tube. Subsequently, p-toluenesulfonic acid monohydrate (0.2 g, catalytic amount) was added as a catalyst. The reaction mixture was heated to reflux and the water generated during the reaction was removed via a Dean-Stark water separator. After completion of the reaction, the solvent was removed under reduced pressure by rotary evaporator. The residue was distilled under reduced pressure and the fractions with boiling points of 96-99 °C were collected to give 47.6 g of the colorless oily product malate in 91% yield. The infrared spectrum of the product (KBr pressed sheet, cm1) showed characteristic absorption peaks: 2984, 2890, 1736, 1370, 1049.

References[1] Journal of Chemical Research - Part S, 1997, # 1, p. 26 - 27
[2] Journal of Organic Chemistry, 1989, vol. 54, # 15, p. 3625 - 3634
[3] Journal of Catalysis, 2000, vol. 196, # 2, p. 345 - 351
[4] Tetrahedron Letters, 2011, vol. 52, # 51, p. 7004 - 7007
[5] RSC Advances, 2016, vol. 6, # 47, p. 41404 - 41409
Fructone Preparation Products And Raw materials
Raw materialsEthyl acetoacetate-->Ethylene glycol-->Benzene-->Toluene-->p-Toluenesulfonic acid monohydrate
Preparation Products2-Methyl-1,3-dioxolane-2-ethanol
Tag:Fructone(6413-10-1) Related Product Information
Bromocyclopentane Ethyl 4-bromoacetoacetate 1,3-Dioxolane Ethyl 4-chloroacetoacetate Cyclopentane Ethyl 4,4,4-trifluoroacetoacetate Ethyl acetoacetate Ethyl 2-methylacetoacetate Ethyl acetate Methyl acetoacetate Ammonium acetate Ethyl 2-chloroacetoacetate Cyclopentyl chloride Tocopheryl acetate Methylcyclopentane Acetoxyacetic acid Glatiramer acetate Vinyl acetate