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| | 1H-Indole-6-carboxylicacid,hydrazide(9CI) Basic information |
| | 1H-Indole-6-carboxylicacid,hydrazide(9CI) Chemical Properties |
| density | 1.353±0.06 g/cm3(Predicted) | | storage temp. | Keep in dark place,Inert atmosphere,Room temperature | | pka | 12.95±0.30(Predicted) |
| | 1H-Indole-6-carboxylicacid,hydrazide(9CI) Usage And Synthesis |
| Synthesis | GENERAL PROCEDURE: Methyl indole-6-carboxylate (5 mmol) was slowly added to hydrazine hydrate (3 mL) at room temperature. Subsequently, the reaction mixture was subjected to microwave irradiation at 300 W power for 5-8 min. The reaction process was monitored in real time by thin layer chromatography (TLC). After the reaction was complete, the mixture was cooled to room temperature and the intermediate 1H-indole-6-carboxylic acid hydrazine was precipitated in 83-98% yield. | | References | [1] Journal of Chemical Research, 2015, vol. 39, # 5, p. 296 - 299 |
| | 1H-Indole-6-carboxylicacid,hydrazide(9CI) Preparation Products And Raw materials |
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