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2,7-Diacetylfluorene

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2,7-Diacetylfluorene manufacturers

2,7-Diacetylfluorene Basic information
Product Name:2,7-Diacetylfluorene
Synonyms:2,6-PYRIDINEDIMETHANOL;Ethanone, 1,1'-(9H-fluorene-2,7-diyl)bis-;1-(7-ACETYL-9H-FLUOREN-2-YL)ETHAN-1-ONE;2,7-Diacetylfluorene>;1,1'-(9H-Fluorene-2,7-diyl)bis(ethan-1-one);1,1'-(9H-Fluorene-2,7-diyl)bis(ethan-1-one) - [F93985];2,7-DIACETYLFLUORENE
CAS:961-27-3
MF:C17H14O2
MW:250.29
EINECS:
Product Categories:Fluorenes;Fluorenes & Fluorenones
Mol File:961-27-3.mol
2,7-Diacetylfluorene Structure
2,7-Diacetylfluorene Chemical Properties
Melting point 173 °C
Boiling point 459.6±38.0 °C(Predicted)
density 1.183
storage temp. -20°C Freezer
solubility Chloroform (Slightly), Ethyl Acetate (Slightly, Sonicated)
form Solid
color Pale Yellow
InChIInChI=1S/C17H14O2/c1-10(18)12-3-5-16-14(7-12)9-15-8-13(11(2)19)4-6-17(15)16/h3-8H,9H2,1-2H3
InChIKeyRIRYGERFWHUZBT-UHFFFAOYSA-N
SMILESC1C2=C(C=CC(C(=O)C)=C2)C2=C1C=C(C(=O)C)C=C2
CAS DataBase Reference961-27-3(CAS DataBase Reference)
Safety Information
Hazard Codes Xi
Hazard Note Irritant
HS Code 2914409000
MSDS Information
2,7-Diacetylfluorene Usage And Synthesis
Uses2,7-Diacetylfluorene is used as a reactant in the synthesis of (dioxaborine)fluorene derivatives for light-emitting diodes (LEDs).
SynthesisAluminum chloride (440 g) suspended in anhydrous 1,2-dichloroethane (500 ml) was stirred and treated dropwise with acetic anhydride (162 ml, 175 g) at 0C. The resulting solution was then added to a solution of fluorene (125 g) in 1,2-dichloroethane (700 ml) at 0C with stirring. After addition, half of the dichloroethane was removed under reduced pressure and the residue was poured into a mixture of ice and 2N hydrochloric acid. The resulting solid was collected by filtration, washed with water, dried and recrystallized from acetone to give 2,7-diacetylfluorene, m.p. 205C 177-180.
2,7-Diacetylfluorene Preparation Products And Raw materials
Tag:2,7-Diacetylfluorene(961-27-3) Related Product Information
4,4'-Biphenyldicarboxaldehyde 4-Acetylbiphenyl 4'-Methylbiphenyl-4-carbaldehyde 3',4'-Dimethylacetophenone 2-Acetylfluorene 4,4'-Diacetylbiphenyl 2-METHYLFLUORENE 2,6-Pyridinedimethanol ,98%,2,6-PYRIDINEDIMETHANOL 5-hydroxy-6-methyl-3,4-pyridinedimethanol dipalmitate 2,7-Diacetylfluorene Pyridoxine hydrochloride Metadoxine Pyridoxine Pirbuterol 2-Fluorenecarboxaldehyde 2,4,6-Trimethyl-3,5-pyridinedimethanol 2,4-Pyridinedimethanol 5-Oxo-DL-proline·5-Hydroxy-6-methyl-3,4-pyridinedimethanol