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| | 1-Bromo-2-chloro-4-fluoro-5-nitrobenzene Basic information |
| Product Name: | 1-Bromo-2-chloro-4-fluoro-5-nitrobenzene | | Synonyms: | 1-broMo-2-chloro-4-fluoro-5-nitrobenzene;5-bromo-4-chloro-2-fluoronitrobenzene;YVDJBLFLBBBGMD-UHFFFAOYSA-N;Benzene, 1-bromo-2-chloro-4-fluoro-5-nitro-;2-Fluoro-4-Chloro-5-Bromobenzene | | CAS: | 111010-08-3 | | MF: | C6H2BrClFNO2 | | MW: | 254.44 | | EINECS: | | | Product Categories: | | | Mol File: | 111010-08-3.mol |  |
| | 1-Bromo-2-chloro-4-fluoro-5-nitrobenzene Chemical Properties |
| Melting point | 65-65.5 °C | | Boiling point | 290.0±35.0 °C(Predicted) | | density | 1.904±0.06 g/cm3(Predicted) | | storage temp. | Sealed in dry,Room Temperature | | form | powder | | color | Faint to light yellow |
| | 1-Bromo-2-chloro-4-fluoro-5-nitrobenzene Usage And Synthesis |
| Synthesis |
To a mixture of 4-chloro-2-fluoronitrobenzene (1.00 g), silver sulfate (1.95 g), and concentrated sulfuric acid (5 ml), bromine (0.32 ml) was added under ice cooling, and the resulting mixture was stirred at 0 C. for 30 min, then at room temperature for 1 h. The reaction mixture was put into ice water and subjected to extraction with ether. The organic layer was washed with water, a saturated aqueous sodium hydrogen carbonate solution, and a saturated aqueous sodium chloride solution sequentially, dried with anhydrous sodium sulfate and concentrated under reduced pressure to give 1.38 g of 1-Bromo-2-chloro-4-fluoro-5-nitrobenzene (yield, 95%).
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| | 1-Bromo-2-chloro-4-fluoro-5-nitrobenzene Preparation Products And Raw materials |
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