2-Sulfobenzoic acid monoammonium salt

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2-Sulfobenzoic acid monoammonium salt Basic information
Application
Product Name:2-Sulfobenzoic acid monoammonium salt
Synonyms:2-sulfo-benzoicacimonoammoniumsalt;Benzoicacid,2-sulfo-,monoammoniumsalt;AMMONIUM ACID SULFOBENZOATE;AMMONIUM O-SULFOBENZOATE;2-SULFOBENZOIC ACID AMMONIUM SALT;O-SULFOBENZOIC ACID, AMMONIUM SALT;O-SULFOBENZOIC ACID MONOAMMONIUM SALT;ammonium hydrogen 2-sulphobenzoate
CAS:6939-89-5
MF:C7H9NO5S
MW:219.22
EINECS:230-077-8
Product Categories:
Mol File:6939-89-5.mol
2-Sulfobenzoic acid monoammonium salt Structure
2-Sulfobenzoic acid monoammonium salt Chemical Properties
Melting point 274-277°C
storage temp. Store below +30°C.
form powder to crystal
color White to Almost white
CAS DataBase Reference6939-89-5(CAS DataBase Reference)
EPA Substance Registry SystemBenzoic acid, 2-sulfo-, monoammonium salt (6939-89-5)
Safety Information
WGK Germany WGK 3 highly water endangering
TSCA TSCA listed
HS Code 2916 39 90
MSDS Information
2-Sulfobenzoic acid monoammonium salt Usage And Synthesis
ApplicationBecause it contains carboxyl and sulfonyl groups, 2-sulfonylsporin ammonium salt can perform various functions such as monodentate, bidentate, chelate, and bridging, and can also act as a donor and acceptor for forming hydrogen bonds. Therefore, the chemistry of 2-sulfonylsporin ammonium salt has been extensively studied.
Synthesis0.25 mmol of ammonia, 0.112 g (0.5 mmol) of sodium 2-sulfobenzoate (3-NaHsb), 0.078 g (0.50 mmol) of 2,2-bipyridine (2,2-bipy), and 20 mL of water were added to 30 mL of Teflon tubing sealed in a stainless steel reactor, and the reaction was carried out for 1 d in an oven at 423 K. The solution was cooled down to room temperature. A dark red solution was obtained and filtered; the filtrate was slowly evaporated at room temperature and dark red bulk crystals were obtained in about 3 months in 54% yield (147 mg of 2-sulfosporin ammonium salt). Elemental analysis (based on the chemical formula C7H9NO5S) showed that the experimental values matched the theoretically calculated values.
Purification Methodso-Sulfobenzoic acid (monoammonium salt) [6939-89-5] M 219.5. Crystallise the salt from water.
2-Sulfobenzoic acid monoammonium salt Preparation Products And Raw materials
Raw materialsSaccharin-->Saccharin sodium
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