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| | 5-Bromo-2-nitrophenylacetic acid Basic information |
| | 5-Bromo-2-nitrophenylacetic acid Chemical Properties |
| storage temp. | Sealed in dry,Room Temperature | | Appearance | Light yellow to yellow Solid |
| | 5-Bromo-2-nitrophenylacetic acid Usage And Synthesis |
| Synthesis | 2-(5-bromo-2-nitrophenyl)acetonitrile was used as starting material, which was dissolved in a solvent mixture of acetic acid (AcOH) and concentrated hydrochloric acid (HCl) (1:5, v/v), followed by the reaction under reflux conditions for 4 hours. Upon completion of the reaction, the reaction mixture was extracted using ethyl acetate, the organic phase was separated and dried with anhydrous sodium sulfate (Na2SO4), and finally the solvent was removed by rotary evaporator to obtain the target product 2-(5-bromo-2-nitrophenyl)acetic acid. | | References | [1] Archiv der Pharmazie (Weinheim, Germany), 1989, vol. 322, p. 483 - 487
[2] Tetrahedron Letters, 2014, vol. 56, # 1, p. 89 - 94 |
| | 5-Bromo-2-nitrophenylacetic acid Preparation Products And Raw materials |
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