|
|
| | N-Ethoxycarbonylmethyl-oxalamic acid ethyl ester Basic information |
| Product Name: | N-Ethoxycarbonylmethyl-oxalamic acid ethyl ester | | Synonyms: | N-Ethoxycarbonylmethyl-oxalamic acid ethyl ester;N-EthoxycarboMylMethyl-oxalaMic acid ethyl ester;(CarboxyMethyl)oxaMic Acid Diethyl Ester;N-(2-Ethoxy-2-oxoacetyl)glycine ethyl ester;Glycine, N-(2-ethoxy-2-oxoacetyl)-, ethyl ester;Ethyl 2-((2-ethoxy-2-oxoethyl);2-[(2-ethoxy-2-oxoethyl)amino]-2-oxoacetic acid ethyl ester | | CAS: | 29655-79-6 | | MF: | C8H13NO5 | | MW: | 203.19 | | EINECS: | | | Product Categories: | | | Mol File: | 29655-79-6.mol |  |
| | N-Ethoxycarbonylmethyl-oxalamic acid ethyl ester Chemical Properties |
| storage temp. | Sealed in dry,Room Temperature | | Cosmetics Ingredients Functions | HAIR CONDITIONING |
| | N-Ethoxycarbonylmethyl-oxalamic acid ethyl ester Usage And Synthesis |
| Uses | (Carboxymethyl)oxamic Acid Diethyl Ester, is an intermediate in various chemical synthesis. It is used in the preparation of 5-alkoxyoxazoles, used in Diels-Alder process. | | Synthesis | Example 2 II: Compound 4 was prepared using ethyl glycinate hydrochloride and ethyl oxalyl chloride monoethyl ester as starting materials with reference to the literature (J. Heterocycl. Chem. 1995, 32, 1693-1702).Subsequently, the reduction reaction was carried out using the NaBH4/LiCl system in ethanol solution. Further oxidation by Dess-Martin oxidizer gave the target aldehyde 6 in 25% overall yield (two-step reaction). | | References | [1] Synthetic Communications, 2000, vol. 30, # 17, p. 3171 - 3180 [2] Patent: WO2007/124546, 2007, A1. Location in patent: Page/Page column 63 [3] Chemische Berichte, 1897, vol. 30, p. 590 [4] Journal of the American Chemical Society, 1997, vol. 119, # 1, p. 86 - 93 [5] Organic Process Research and Development, 2004, vol. 8, # 2, p. 192 - 200 |
| | N-Ethoxycarbonylmethyl-oxalamic acid ethyl ester Preparation Products And Raw materials |
|