2-Bromo-6-fluorobenzoyl chloride

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2-Bromo-6-fluorobenzoyl chloride manufacturers
2-Bromo-6-fluorobenzoyl chloride Basic information
Product Name:2-Bromo-6-fluorobenzoyl chloride
Synonyms:Benzoyl chloride, 2-bromo-6-fluoro-;2-bromo-6-fluorobenzeneformylchloro;2-Bromo-6-fluorobenzoyl chloride
CAS:1020718-20-0
MF:C7H3BrClFO
MW:237.45
EINECS:
Product Categories:Fluorine series
Mol File:Mol File
2-Bromo-6-fluorobenzoyl chloride Structure
2-Bromo-6-fluorobenzoyl chloride Chemical Properties
Boiling point 236℃
density 1.742
Fp 97℃
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
form liquid
color Colourless
Safety Information
HS Code 2916399090
MSDS Information
2-Bromo-6-fluorobenzoyl chloride Usage And Synthesis
Synthesis
2-Bromo-6-fluorobenzoic acid

2252-37-1

2-BROMO-6-FLUOROBENZOYL CHLORIDE

1020718-20-0

General method: 2-bromo-6-fluorobenzoic acid (1.0 mmol) was mixed with excess thionyl chloride (5 mL) and reacted at reflux for 2 hours. After completion of the reaction, the excess thionyl chloride was removed by vacuum concentration to give 2-bromo-6-fluorobenzoyl chloride in quantitative yield.

References[1] Chinese Chemical Letters, 2013, vol. 24, # 8, p. 673 - 676
[2] Patent: EP2123644, 2009, A1. Location in patent: Page/Page column 59
[3] Journal of the American Chemical Society, 2010, vol. 132, # 32, p. 11278 - 11287
[4] Synlett, 2013, vol. 24, # 19, p. 2575 - 2580
[5] Journal of the American Chemical Society, 2017, vol. 139, # 30, p. 10228 - 10231
2-Bromo-6-fluorobenzoyl chloride Preparation Products And Raw materials
Raw materials2-Bromo-6-fluorobenzoic acid
Tag:2-Bromo-6-fluorobenzoyl chloride(1020718-20-0) Related Product Information
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