N-(4-DIMETHYLAMINO-3,5-DINITROPHENYL)MALEIMIDE(3475-74-9) 13C NMR
Product NameN-(4-DIMETHYLAMINO-3,5-DINITROPHENYL)MALEIMIDE
CAS3475-74-9
Molecular FormulaC12H10N4O6
Molecular Weight306.23
InChIInChI=1S/C12H10N4O6/c1-13(2)12-8(15(19)20)5-7(6-9(12)16(21)22)14-10(17)3-4-11(14)18/h3-6H,1-2H3
InChIKey QPYAUURPGVXHFK-UHFFFAOYSA-N
SmilesN1(C2=CC([N+]([O-])=O)=C(N(C)C)C([N+]([O-])=O)=C2)C(=O)C=CC1=O
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MassMS-NW-6380 N-(4-dimethylamino-3,5-dinitrophenyl)maleimide C12H10N4O6 (Mass of molecular ion: 306)
Source Temperature: 200 °C Sample Temperature: 180 °C Direct, 75 eV
15.0 19.1 17.0 1.9 18.0 6.0 26.0 24.3 27.0 4.4 28.0 6.1 29.0 2.5 30.0 6.6 31.0 1.0 37.0 1.7 38.0 5.1 39.0 14.0 40.0 3.8 41.0 5.4 42.0 47.1 43.0 7.8 44.0 4.3 45.0 1.1 50.0 4.2 51.0 7.1 52.0 8.0 53.0 11.7 54.0 56.7 55.0 6.0 56.0 1.2 61.0 4.4 62.0 6.3 63.0 17.6 64.0 10.0 65.0 9.5 66.0 26.1 67.0 5.0 68.0 1.7 72.0 1.7 74.0 1.6 75.0 5.3 76.0 12.8 77.0 16.1 78.0 9.8 79.0 4.6 80.0 9.9 81.0 2.2 82.0 56.2 83.0 3.4 86.0 1.9 87.0 3.3 88.0 10.8 89.0 11.4 90.0 19.5 91.0 10.3 92.0 8.0 93.0 7.7 94.0 2.2 98.0 1.8 100.0 1.7 101.0 2.1 102.0 6.4 103.0 11.1 104.0 15.3 105.0 8.8 106.0 5.9 107.0 3.0 108.0 1.4 114.0 1.6 115.0 5.9 116.0 24.6 117.0 22.2 118.0 19.0 119.0 12.7 120.0 14.1 121.0 3.8 122.0 1.2 128.0 3.4 129.0 6.5 130.0 12.4 131.0 17.3 132.0 18.0 133.0 7.1 134.0 4.3 135.0 1.6 141.0 1.1 142.0 4.4 143.0 10.6 144.0 23.0 145.0 23.7 146.0 26.5 147.0 9.6 148.0 5.6 149.0 3.1 150.0 1.1 153.0 2.6 155.0 2.0 156.0 3.4 157.0 9.2 158.0 19.1 159.0 27.0 160.0 12.5 161.0 4.8 162.0 1.5 167.0 1.3 168.0 1.4 169.0 2.1 170.0 3.3 171.0 8.8 172.0 23.7 173.0 22.2 174.0 8.0 175.0 15.4 176.0 2.7 183.0 1.1 184.0 3.0 185.0 8.1 186.0 15.4 187.0 7.2 188.0 4.0 189.0 2.3 190.0 1.2 198.0 5.4 199.0 13.0 200.0 9.0 201.0 16.7 202.0 6.0 203.0 2.7 212.0 4.2 213.0 60.0 214.0 27.5 215.0 8.1 216.0 2.9 226.0 4.9 227.0 2.3 228.0 7.0 229.0 13.2 230.0 4.8 231.0 5.0 242.0 3.2 243.0 16.8 244.0 7.6 245.0 1.6 247.0 2.9 258.0 1.0 259.0 43.0 260.0 8.0 261.0 12.1 262.0 1.9 272.0 3.7 273.0 1.6 274.0 1.4 275.0 1.5 289.0 100.0 290.0 15.8 291.0 2.6 305.0 4.0 306.0 66.4 307.0 10.3 308.0 2.1
parameter in CDCl3
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1H NMR 300 MHz C12 H10 N4 O6 0.044 g : 0.5 ml CDCl3 N-(4-dimethylamino-3,5-dinitrophenyl)maleimide 
Parameter ppm Hz
D(A) 7.982 D(B) 6.919 D(C) 2.838
Hz ppm Int.2394.61 7.982 333 2075.71 6.919 333 851.39 2.838 1000
in CDCl3
KBr disc
nujol mull
