1120-36-1

1-十四烯(1120-36-1)红外图谱(IR1)

产品名称:1-十四烯

CAS:1120-36-1

分子式:C14H28

分子量: 196.37

InChI:InChI=1S/C14H28/c1-3-5-7-9-11-13-14-12-10-8-6-4-2/h3H,1,4-14H2,2H3

InChIKey: HFDVRLIODXPAHB-UHFFFAOYSA-N

Smiles:C=CCCCCCCCCCCCC

Mass

MS-NW-5130          
1-tetradecene
C14H28              (Mass of molecular ion:    196)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0      17.5
      28.0       1.2
      29.0      37.3
      36.0       1.3
      39.0      16.5
      40.0       3.3
      41.0      79.8
      42.0      22.0
      43.0     100.0
      44.0       3.4
      53.0       6.6
      54.0      13.1
      55.0      92.2
      56.0      78.1
      57.0      91.1
      58.0       4.2
      65.0       1.1
      66.0       1.2
      67.0      13.0
      68.0      14.9
      69.0      75.9
      70.0      76.3
      71.0      36.8
      72.0       2.1
      79.0       1.1
      81.0       5.7
      82.0      17.9
      83.0      77.7
      84.0      44.2
      85.0      17.8
      86.0       1.2
      95.0       1.9
      96.0       7.5
      97.0      54.5
      98.0      24.3
      99.0       3.4
     110.0       3.6
     111.0      23.9
     112.0      14.9
     113.0       1.9
     124.0       1.7
     125.0      10.0
     126.0       9.0
     127.0       1.2
     139.0       3.0
     140.0       3.7
     153.0       1.4
     154.0       3.4
     168.0       3.5
     196.0       4.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₄ H₂₈	0.04 ml : 0.5 ml CDCl₃
1-tetradecene

    Assign.     Shift(ppm)

      A             5.79
      B             4.98
      C             4.92
      D             2.02
      E             1.26
      F             0.89

     Hz     ppm     Int.

    453.25   5.061     44
    446.44   4.985     39
    445.19   4.971     30
    436.44   4.874     47
    435.25   4.860     33
    179.38   2.003     31
    179.19   2.001     31
    113.06   1.263   1000
     84.13   0.940     39
     82.44   0.921     32
     80.94   0.904     32
     78.88   0.881    109

in CDCl3