15945-07-0

2,4,5-三氯苯磺酰氯(15945-07-0)核磁图(¹³CNMR)

产品名称:2,4,5-三氯苯磺酰氯

CAS:15945-07-0

分子式:C6H2Cl4O2S

分子量: 279.96

InChI:InChI=1S/C6H2Cl4O2S/c7-3-1-5(9)6(2-4(3)8)13(10,11)12/h1-2H

InChIKey: WNVVRCKTQSCPAC-UHFFFAOYSA-N

Smiles:C1(S(Cl)(=O)=O)=CC(Cl)=C(Cl)C=C1Cl

Mass

MS-NW-1919          
2,4,5-trichlorobenzenesulfonyl chloride
C6H2Cl4O2S          (Mass of molecular ion:    278)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      28.0       1.9
      35.0       1.0
      36.0       1.5
      37.0       5.3
      38.0       1.4
      45.0       1.0
      47.0       1.2
      48.0       3.0
      49.0       2.2
      50.0       3.1
      54.0       1.6
      60.0       1.4
      61.0       4.2
      62.0       3.1
      64.0       3.9
      69.0       2.1
      71.0       1.4
      71.5       4.1
      72.0       6.1
      72.5       2.8
      73.0      11.3
      74.0      26.7
      75.0       1.8
      79.0       1.9
      83.0       1.6
      84.0      11.5
      85.0       2.1
      86.0       3.8
      94.0       1.0
      96.0       1.5
      97.0       3.7
      99.0       1.1
     107.0       5.0
     108.0      18.3
     109.0      23.4
     110.0       6.9
     111.0       7.2
     118.0       1.9
     119.0       2.1
     120.0       1.3
     121.0       1.4
     121.5       1.9
     122.5       1.9
     143.0      26.8
     144.0      14.9
     145.0      18.1
     146.0       9.6
     147.0       3.4
     148.0       1.6
     167.0       4.4
     169.0       4.2
     171.0       1.3
     176.0       1.2
     178.0       1.5
     179.0      66.7
     180.0       6.0
     181.0      62.5
     182.0       5.2
     183.0      20.5
     184.0       1.6
     185.0       2.2
     195.0      20.4
     196.0       1.4
     197.0      19.4
     198.0       1.3
     199.0       6.9
     201.0       1.4
     214.0       4.8
     216.0       6.2
     218.0       3.0
     227.0       1.2
     229.0       1.2
     243.0      99.2
     244.0       7.3
     245.0     100.0
     246.0       7.3
     247.0      35.3
     248.0       2.6
     249.0       4.9
     278.0      28.9
     279.0       2.1
     280.0      38.3
     281.0       3.0
     282.0      19.6
     283.0       1.4
     284.0       4.7
     360.0       1.1

parameter in CDCl3

¹H NMR	300 MHz
C₆ H₂ Cl₄ O₂ S	0.047 g : 0.5 ml CDCl₃
2,4,5-trichlorobenzenesulfonyl chloride

    Parameter     ppm  Hz

      D(A)         8.226
      D(B)         7.763

     Hz     ppm     Int.

   2467.80   8.226   1000
   2328.90   7.763   1000

in CDCl3

CCl4 solution

KBr disc

nujol mull

4880 A,100M,powder

更多供应商

Clearsynth Labs Limited

安耐吉化学&3A（安徽泽升科技有限公司）

武汉易泰科技有限公司上海分公司

Capot Chemical Co., Ltd

2,4,5-三氯苯磺酰氯(15945-07-0)核磁图(13CNMR)

2,4,5-三氯苯磺酰氯(15945-07-0)核磁图(¹³CNMR)