16532-02-8

溴乙基二甲基氯硅烷(16532-02-8)核磁图(¹HNMR)

产品名称:溴乙基二甲基氯硅烷

CAS:16532-02-8

分子式:C3H8BrClSi

分子量: 187.54

InChI:InChI=1S/C3H8BrClSi/c1-6(2,5)3-4/h3H2,1-2H3

InChIKey: CAURZYXCQQWBJO-UHFFFAOYSA-N

Smiles:[Si](CBr)(Cl)(C)C

Mass

MS-NW-4937          
(bromomethyl)chlorodimethylsilane
C3H8BrClSi          (Mass of molecular ion:    186)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      27.0       1.9
      28.0       1.6
      29.0       3.1
      42.0       1.8
      43.0       4.1
      53.0       1.2
      63.0       9.0
      64.0       1.0
      65.0       9.0
      67.0       2.5
      77.0       1.4
      78.0       1.0
      79.0       2.3
      92.0       2.9
      93.0     100.0
      94.0       8.3
      95.0      35.0
      96.0       2.6
      97.0       1.1
     107.0       1.6
     109.0       1.9
     123.0       4.9
     124.0       1.0
     125.0       4.8
     143.0      10.9
     144.0       1.5
     145.0      13.7
     147.5       3.9
     152.0       1.8
     153.5       2.0
     157.0       1.3
     159.0       1.5
     171.0       4.9
     173.0       6.1
     175.0       1.7
     186.0       4.8
     188.0       6.3
     190.0       1.7
     197.0       2.4
     199.0       2.5
     225.0       2.3
     227.0       2.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₃ H₈ Br Cl Si	0.04 ml : 0.5 ml CDCl₃
(bromomethyl)chlorodimethylsilane

    Assign.     Shift(ppm)

      A             2.638
      B             0.572
     
     J(A,SI-29)=4.3HZ
     J(B,SI-29)=7.3HZ

     Hz     ppm     Int.

    236.31   2.639    297
     54.81   0.612     47
     51.25   0.573   1000
     49.31   0.551     63
     47.69   0.533     51

in CDCl3

liquid film

溴乙基二甲基氯硅烷(16532-02-8)核磁图(1HNMR)

溴乙基二甲基氯硅烷(16532-02-8)核磁图(¹HNMR)