18480-23-4

烯丙基三苯基氯化膦(18480-23-4)核磁图(¹³CNMR)

分子式:C21H20ClP

分子量: 338.81

InChI:InChI=1S/C21H20P.ClH/c1-2-18-22(19-12-6-3-7-13-19,20-14-8-4-9-15-20)21-16-10-5-11-17-21;/h2-17H,1,18H2;1H/q+1;/p-1

InChIKey: FKMJROWWQOJRJX-UHFFFAOYSA-M

Smiles:[P+](CC=C)(C1C=CC=CC=1)(C1=CC=CC=C1)C1C=CC=CC=1.[Cl-]

¹HNMR

¹³CNMR

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₁ H₂₀ Cl P	0.038 g : 0.5 ml CDCl₃
allyltriphenylphosphonium chloride

    Assign.     Shift(ppm)

      A             7.83
      B             7.72
      C             5.73
      D             5.554
      E             5.399
      F             4.744

     Hz     ppm     Int.

   3143.92   7.867    607
   3138.55   7.854    292
   3136.72   7.849    866
   3135.13   7.845    846
   3131.84   7.837    739
   3131.47   7.836    745
   3129.52   7.831    450
   3127.20   7.825    547
   3125.61   7.821    777
   3123.90   7.817   1000
   3122.80   7.814    755
   3119.63   7.806    368
   3118.65   7.804    401
   3094.85   7.744    680
   3093.38   7.741    422
   3091.80   7.737    651
   3087.16   7.725    881
   3085.21   7.720    611
   3084.11   7.718    600
   3081.91   7.712    337
   3079.96   7.707    402
   3076.05   7.697    302
   2303.71   5.765     42
   2298.46   5.752     43
   2296.51   5.747     34
   2295.90   5.745     35
   2293.95   5.740     76
   2288.70   5.727     78
   2286.87   5.723     89
   2283.94   5.715     39
   2281.49   5.709     90
   2279.66   5.705     51
   2279.42   5.704     51
   2279.05   5.703     50
   2276.86   5.698     75
   2274.54   5.692     38
   2271.61   5.684     74
   2269.78   5.680     38
   2264.65   5.667     34
   2229.00   5.578    134
   2228.03   5.575    135
   2223.75   5.565    127
   2222.78   5.562    125
   2212.04   5.535     79
   2211.06   5.533     80
   2206.79   5.522     80
   2205.81   5.520     79
   2165.04   5.418    126
   2164.31   5.416    127
   2160.64   5.407    128
   2159.91   5.405    125
   2155.03   5.393    107
   2154.30   5.391    108
   2150.63   5.382    105
   2149.78   5.380    103
   1907.23   4.773    225
   1900.15   4.755    216
   1891.72   4.734    223
   1887.94   4.724     36
   1884.64   4.716    211

in CDCl3