2,4,6-三甲基-1,3-苯二胺(3102-70-3)核磁图(¹³CNMR)

Mass

MS-NW-7894          
2,4,6-trimethyl-m-phenylenediamine
C9H14N2             (Mass of molecular ion:    150)

   Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       1.8
      27.0       1.6
      28.0       3.8
      30.0       1.3
      39.0       3.7
      41.0       2.2
      42.0       3.0
      51.0       1.8
      52.0       2.2
      53.0       2.5
      54.0       3.0
      61.0       3.4
      63.0       1.1
      65.0       3.5
      66.0       2.7
      67.0       4.9
      67.5       1.3
      73.0       1.4
      74.0       4.4
      74.5       1.0
      75.0       7.6
      77.0       4.1
      78.0       1.3
      79.0       2.6
      80.0       1.4
      91.0       3.2
      92.0       1.1
      93.0       2.1
      94.0       2.4
      95.0       1.0
     103.0       1.6
     104.0       1.2
     105.0       3.2
     106.0       5.1
     107.0       5.9
     108.0       3.5
     109.0       1.8
     110.0       1.0
     117.0       3.4
     118.0       5.9
     119.0       1.3
     120.0       3.0
     121.0       2.0
     122.0       7.3
     123.0       1.1
     130.0       1.8
     131.0       1.2
     132.0       8.8
     133.0       8.3
     134.0       5.7
     135.0      37.2
     136.0       3.6
     147.0       1.2
     148.0       1.7
     149.0      63.3
     150.0     100.0
     151.0      10.6

Assign. Shift(ppm) A 6.43 B 4.06 C 1.94 D 1.866

     Hz     ppm     Int.

    575.63   6.428    116
    363.63   4.061    112
    182.00   2.033     23
    181.31   2.025     24
    173.94   1.943   1000
    167.25   1.868    577