7417-18-7

1-(2-甲氧基苯基)乙醇(7417-18-7)核磁图(¹³CNMR)

产品名称:1-(2-甲氧基苯基)乙醇

CAS:7417-18-7

分子式:C9H12O2

分子量: 152.19

InChI:InChI=1S/C9H12O2/c1-11-9-5-3-2-4-8(9)6-7-10/h2-5,10H,6-7H2,1H3

InChIKey: XLDRDNQLEMMNNH-UHFFFAOYSA-N

Smiles:C1(CCO)=CC=CC=C1OC

Mass

MS-NW-5454          
o-methoxyphenethyl alcohol
C9H12O2             (Mass of molecular ion:    152)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.2
      18.0       1.2
      27.0       2.6
      28.0       2.0
      29.0       1.7
      31.0       3.5
      38.0       1.4
      39.0       7.8
      41.0       1.8
      50.0       3.0
      51.0       8.3
      52.0       4.6
      53.0       2.0
      62.0       1.4
      63.0       4.6
      64.0       1.4
      65.0      14.8
      66.0       1.1
      77.0      10.8
      78.0       8.1
      79.0       3.3
      89.0       3.8
      90.0       2.4
      91.0     100.0
      92.0       9.2
      93.0       7.7
     103.0       1.3
     105.0       1.2
     107.0       7.2
     108.0       1.6
     119.0       2.1
     120.0       2.2
     121.0      97.3
     122.0      26.4
     123.0       2.3
     134.0       1.1
     152.0      46.9
     153.0       5.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₂ O₂	0.04 ml : 0.5 ml CDCl₃
o-methoxyphenethyl alcohol

    Assign.     Shift(ppm)

      A             7.20
      B             7.14
      C             6.88
      D             6.84
      E             3.78
      F             3.78
      G             2.88
      J             2.18

     Hz     ppm     Int.

    651.19   7.271     22
    646.13   7.215     39
    644.81   7.200     64
    642.63   7.176     74
    638.19   7.126     28
    636.50   7.107    119
    623.19   6.959     46
    621.81   6.943     80
    616.06   6.879     80
    614.94   6.867    129
    608.44   6.794     60
    607.25   6.781     40
    345.81   3.862     84
    345.31   3.856     83
    338.94   3.785   1000
    332.56   3.714    122
    263.94   2.948     90
    257.44   2.875    148
    250.81   2.801     63
    195.56   2.184    275

in CDCl3