3-Chloro-6-nitro (1H)indazole
- CAS No.
- 50593-68-5
- Chemical Name:
- 3-Chloro-6-nitro (1H)indazole
- Synonyms
- NSC84179;3-CHLORO-6-NITROINDAZOLE;3-chloro-6-nitro-1h-indazol;3-Chloro-6-nitro (1H)indazole;1H-Indazole, 3-chloro-6-nitro-;3-Chloro-6-nitro-1H-indazole ,97%
- CBNumber:
- CB0673031
- Molecular Formula:
- C7H4ClN3O2
- Molecular Weight:
- 197.58
- MDL Number:
- MFCD00010741
- MOL File:
- 50593-68-5.mol
- MSDS File:
- SDS
- TDS File:
- TDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| Hazard Codes | Xi |
| HazardClass | IRRITANT |
| HS Code | 29339900 |
3-Chloro-6-nitro (1H)indazole price More Price(41)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR14098 | 3-Chloro-6-nitro-1H-indazole ≥95% | 50593-68-5 | 250mg | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR14098 | 3-Chloro-6-nitro-1H-indazole ≥95% | 50593-68-5 | 1g | $51 | 2026-06-04 | Buy |
| Apolloscientific | OR14098 | 3-Chloro-6-nitro-1H-indazole ≥95% | 50593-68-5 | 5g | $241 | 2026-06-04 | Buy |
| Matrix Scientific | 047046 | 3-Chloro-6-nitro-1H-indazole | 50593-68-5 | 500.00mg | $181 | 2026-05-18 | Buy |
| Matrix Scientific | 047046 | 3-Chloro-6-nitro-1H-indazole | 50593-68-5 | 1.00g | $228 | 2026-05-18 | Buy |
3-Chloro-6-nitro (1H)indazole Chemical Properties, Uses, Production
Chemical Properties
Yellow solid
Synthesis
7597-18-4
50593-68-5
General procedure for the synthesis of 3-chloro-6-nitro-1H-indazole from 6-nitro-1H-indazole: 6-nitro-1H-indazole (5.0 g, 31 mmol) was added to an aqueous (150 mL) solution of sodium hydroxide (5.0 g), and the mixture was heated until a red color solution formed. The reaction mixture was cooled in an ice water bath for 15 minutes, followed by the slow addition of sodium hypochlorite solution (60 mL, 5.25%, 45 mmol). The reaction mixture was stirred continuously at 0 °C for 5 h. Upon completion of the reaction, the pH was adjusted with dilute hydrochloric acid to 7. The reaction mixture was extracted with ethyl acetate, the organic layers were combined and washed with distilled water, followed by concentration of the organic phase under reduced pressure. The residue was purified by fast column chromatography to afford the target product 3-chloro-6-nitro-1H-indazole (5.5 g, 92% yield). The structure of the product was confirmed by 1H NMR (300 MHz, DMSO-d6): δ 7.93 (m, 1H), 8.02 (m, 1H), 8.50 (m, 1H), 14.01 (s, 1H); the mass spectrum (DCI/NH3) showed m/z 197 [M+H]+.
References
[1] Patent: US2005/277638, 2005, A1. Location in patent: Page/Page column 49
[2] Journal of Chemical Research, Miniprint, 1990, # 11, p. 2601 - 2615
[3] Heterocycles, 1995, vol. 41, # 3, p. 487 - 496
[4] Justus Liebigs Annalen der Chemie, 1927, vol. 451, p. 285,302
3-Chloro-6-nitro (1H)indazole Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Wuhan Chemwish Technology Co., Ltd | 86-027-67849912 | sales@chemwish.com | China | 35884 | 56 |
| China DongFan Chemical Co.,LTD | 86-0571-85151182 | China | 5681 | 66 | |
| Nantong MYBio-pharm. Co., Ltd. | 0513-85921823 18662920231 | sales@ntminyanmedical.com | China | 4563 | 58 |
| Chengdu HuaXia Chemical Reagent Co. Ltd | 400-1166-196 13458535857 | cdhxsj@163.com | China | 13323 | 58 |
| ShangHai AmK Pharmaceutical Technology Co., Ltd. | 微信 18019252918 18019252918 | sale@amkchem.com | China | 14982 | 55 |
| Bellen Chemistry Co., Ltd. | 010-60400365-8001 15910885229 | service@bellenchem.com | China | 4514 | 60 |
| Accela ChemBio Inc. | +1(858) 699-3322 | marketing@accelachem.com | United States | 6022 | 65 |
| Shanghai YuanYe Biotechnology Co., Ltd. | 15026964105 | 2881489226@qq.com | China | 89667 | 60 |
| Changzhou Hopschain Chemical Co.,Ltd. | 85528066 13775048983 | sales@hopschem.com | China | 31548 | 55 |
View Latest Price from 3-Chloro-6-nitro (1H)indazole manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-07-06 | 3-CHLORO-6-NITRO (1H)INDAZOLE
50593-68-5
|
$1.00 | 1KG | 97% | 200KG | Career Henan Chemical Co |
-
- 3-CHLORO-6-NITRO (1H)INDAZOLE
50593-68-5
- $1.00
- 97%
- Career Henan Chemical Co
50593-68-5 (3-Chloro-6-nitro (1H)indazole) Related Search:
1of4
