1-(2'-Bromophenyl)ethylamine
- CAS No.
- 113899-55-1
- Chemical Name:
- 1-(2'-Bromophenyl)ethylamine
- Synonyms
- 1-(2-BROMOPHENYL)ETHANAMINE;1-(2'-Bromophenyl)ethylamine;2-bromo-α-methylBenzenemethanamine;Benzenemethanamine, 2-bromo-α-methyl-;2-Bromo-alpha-methylbenzenemethanamine;Benzenemethanamine, 2-bromo-.alpha.-methyl-
- CBNumber:
- CB0699897
- Molecular Formula:
- C8H10BrN
- Molecular Weight:
- 200.08
- MDL Number:
- MFCD05215385
- MOL File:
- 113899-55-1.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
1-(2'-Bromophenyl)ethylamine price More Price(48)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS64014 | 1-(2-Bromophenyl)ethanamine 97% | 113899-55-1 | 1g | $103 | 2026-06-04 | Buy |
| Activate Scientific | AS64014 | 1-(2-Bromophenyl)ethanamine 97% | 113899-55-1 | 5g | $461 | 2026-06-04 | Buy |
| Matrix Scientific | 132428 | 1-(2-Bromophenyl)ethanamine | 113899-55-1 | 250.00mg | $33 | 2026-05-18 | Buy |
| Matrix Scientific | 132428 | 1-(2-Bromophenyl)ethanamine | 113899-55-1 | 1.00g | $76 | 2026-05-18 | Buy |
| Matrix Scientific | 132428 | 1-(2-Bromophenyl)ethanamine | 113899-55-1 | 5.00g | $216 | 2026-05-18 | Buy |
1-(2'-Bromophenyl)ethylamine Chemical Properties,Uses,Production
Synthesis
27760-49-2
113899-55-1
Under nitrogen protection, sodium borohydride (3.1 g, 86 mmol) and titanium tetrachloride (1 M in toluene, 43 mL, 43 mmol) were dissolved in 40 mL of anhydrous 1,2-dimethoxyethane and the solution was cooled to 0 °C. Subsequently, 1-(2-bromophenyl)ethanone oxime (4.6 g, 21.5 mmol) was slowly added dropwise to the above cooled solution. After the dropwise addition was completed, the reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the reaction was quenched with 200 mL of water and the mixture was adjusted to alkaline with ammonium hydroxide. The crude product was extracted with a solvent mixture of toluene and ethyl acetate to separate the organic and aqueous layers. The organic layer was dried with anhydrous sodium sulfate and subsequently concentrated under reduced pressure to give the crude product 1-(2-bromophenyl)ethylamine (4.0 g, 100% yield). Mass spectrum (electrospray ionization) m/z 200/202 [M + 1]+.
References
[1] Patent: WO2008/144223, 2008, A2. Location in patent: Page/Page column 11
1-(2'-Bromophenyl)ethylamine Preparation Products And Raw materials
Raw materials
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Preparation Products
1-(2'-Bromophenyl)ethylamine Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Candia Thamtech Company Limited | 0371-86615086 18203638366 0371-86159066 13526786601 | China | 2011 | 60 | |
| 9ding chemical ( Shanghai) Limited | 4009209199 | sales@9dingchem.com | China | 18201 | 56 |
| SynAsst Chemical. | 021-60343070 | China | 12731 | 55 | |
| CEG Chemical Science&Technology Co., Ltd. | Mobile:13665161512 | China | 1784 | 58 | |
| Amatek Scientific Co. Ltd. | 0512-56316828 4008675858 | sales@amateksci.com | China | 9849 | 55 |
| Shanghai Carlow Chemicals Co., Ltd. | 21-33526724 18930996265 | info@carlowchem.com | China | 1996 | 58 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| LABTER PHARMATECH(BEIJING) CO.,LTD | 010-56330744 18310155299 | sales@labter.com.cn | China | 19999 | 55 |
| JW & Y Pharmlab Co., Ltd. | 021-64340559 | xinyu_shi@jwypharmlab.com.cn | China | 11999 | 58 |
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