ChemicalBook >> CAS DataBase List >>1,10-Dibromodecane

1,10-Dibromodecane

CAS No.
4101-68-2
Chemical Name:
1,10-Dibromodecane
Synonyms
,w-Dibromodecane;Dibromodecane,95%;1,10-DIBROMODECANE;1,10-dibromo-decan;TIMTEC-BB SBB008900;Decene, 1,10-dibromo;Decane, 1,10-dibromo-;1,10-DECANE DIBROMIDE;DECAMETHYLENE BROMIDE;1,10-Dibromodecane,97%
CBNumber:
CB3322169
Molecular Formula:
C10H20Br2
Molecular Weight:
300.07
MDL Number:
MFCD00000222
MOL File:
4101-68-2.mol
MSDS File:
SDS
Last updated:2026-01-13 11:17:25
Product description Number Pack Size Price
1,10-Dibromodecane 97% D39800 100g $124
1,10-Dibromodecane >95.0%(GC) D0179 25g $30
1,10-Dibromodecane >95.0%(GC) D0179 100g $104
1,10-Dibromodecane D448868 10g $75
1,10-Dibromodecane D448868 1g $45
More product size

1,10-Dibromodecane Properties

Melting point 25-27 °C (lit.)
Boiling point 160 °C/15 mmHg (lit.)
Density 1.335 g/mL at 25 °C (lit.)
refractive index n20/D 1.4912(lit.)
Flash point 26°C
storage temp. Sealed in dry,Room Temperature
form Crystalline Low Melting Solid
color Beige to brown
Specific Gravity 1.335
Water Solubility insoluble
BRN 506156
Dielectric constant 6.5599999999999996
InChI 1S/C10H20Br2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2
InChIKey GTQHJCOHNAFHRE-UHFFFAOYSA-N
SMILES BrCCCCCCCCCCBr
CAS DataBase Reference 4101-68-2(CAS DataBase Reference)
NIST Chemistry Reference Decane, 1,10-dibromo-(4101-68-2)
EPA Substance Registry System Decane, 1,10-dibromo- (4101-68-2)
UNSPSC Code 12352100
NACRES NA.22

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P305+P351+P338
PPE Eyeshields, Gloves, type N95 (US)
Hazard Codes  C,Xi
Risk Statements  20/21/22-36/37/38
Safety Statements  22-24/25-36-26
WGK Germany  3
TSCA  TSCA listed
HS Code  29049090
Storage Class 11 - Combustible Solids
NFPA 704
1
0 0

1,10-Dibromodecane price More Price(29)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich D39800 1,10-Dibromodecane 97% 4101-68-2 100g $124 2025-07-31 Buy
TCI Chemical D0179 1,10-Dibromodecane >95.0%(GC) 4101-68-2 25g $30 2025-07-31 Buy
TCI Chemical D0179 1,10-Dibromodecane >95.0%(GC) 4101-68-2 100g $104 2025-07-31 Buy
TRC D448868 1,10-Dibromodecane 4101-68-2 10g $75 2021-12-16 Buy
TRC D448868 1,10-Dibromodecane 4101-68-2 1g $45 2021-12-16 Buy
Product number Packaging Price Buy
D39800 100g $124 Buy
D0179 25g $30 Buy
D0179 100g $104 Buy
D448868 10g $75 Buy
D448868 1g $45 Buy

1,10-Dibromodecane Chemical Properties,Uses,Production

Chemical Properties

beige to brown crystalline low melting mass

Uses

1,10-Dibromodecane is used as an alkylating agent and as synthetic organic intermediate.

Synthesis

1,10-Decanediol

112-47-0

1,10-Dibromodecane

4101-68-2

The general procedure for the synthesis of 1,10-dibromodecane from 1,10-decanediol is as follows: 1,10-decanediol (1 eq.), 48% aqueous hydrobromic acid (ca. 3 eq./hydroxyl), and octane (ca. 7:1 volume-to-weight ratio to the diol) were added to a single-necked, round-bottomed flask and assembled with a fractionating column/Dean-Stark trap. The reaction mixture was placed in a heated oil bath (145-150°C) with rapid magnetic stirring. The aqueous (lower) layer at the initial boiling point (89-92°C) was condensed and gently separated, and subsequently collected at about half the theoretical volume of water; at this point the temperature of the azeotrope (still at head temperature) began to rise. The condenser was set to full reflux for a few hours, then turned back on and the aqueous-phase material continued to be collected for 1 hour (top temperature 96-100°C). The final volume of the aqueous phase distillate reaches 90-100% of the theoretical value (up to 24% hydrobromic acid in the high boiling distillate). When the octane phase (which is light tan in color) contains dibromides and brominated streptanols (e.g., 6 band 6c), it is washed with cold 85% v/v sulfuric acid (10 mL first, then 5 mL) to remove all color and brominated streptanols. For all three dibromides (3b, 4b, 6b), the neutralized octane solution was passed through a Vigreux column under reduced pressure to remove the solvent, and the residue (which was confirmed to be essentially pure by 1H NMR) was purified by Kugelrohr distillation. Trace amounts of 4-methyltetrahydropyran were detected prior to distillation of 4b.

References

[1] Tetrahedron Letters, 2015, vol. 56, # 4, p. 630 - 632
[2] Green Chemistry, 2014, vol. 16, # 2, p. 836 - 843
[3] Journal of Organic Chemistry, 2015, vol. 80, # 11, p. 5386 - 5394
[4] Journal of the American Chemical Society, 1936, vol. 58, p. 488
[5] Journal of the Chemical Society, 1958, p. 2068

112-47-0
4101-68-2
Synthesis of 1,10-Dibromodecane from 1,10-Decanediol
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View Lastest Price from 1,10-Dibromodecane manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1,10-Dibromodecane pictures 2026-02-13 1,10-Dibromodecane
4101-68-2
US $0.00 / KG 1KG ≥98.5% 20 Tons/Month Yancheng Longshen Chemical Co.,Ltd.
1,10-Dibromodecane pictures 2025-09-25 1,10-Dibromodecane
4101-68-2
US $100.00-1.00 / KG 1KG 99% g-kg-tons, free sample is available Henan Fengda Chemical Co., Ltd
1,10-Dibromodecane pictures 2025-06-27 1,10-Dibromodecane
4101-68-2
US $0.00 / KG 1KG 99% 500000kg Hebei Chuanghai Biotechnology Co., Ltd
Dibromodecane,95% TIMTEC-BB SBB008900 DECAMETHYLENE BROMIDE DECAMETHYLENE DIBROMIDE 1,10-DIBROMODECANE 1,10-DECAMETHYLENE BROMIDE 1,10-DECAMETHYLENE DIBROMIDE 1,10-DECANE DIBROMIDE Decane, 1,10-dibromo- 1,10-Dibromodecane,97% 1,10-Dibromodecane,Decamethylene dibromide 1,10-DibroModecane, 97% 100ML 1,10-DibroModecane, 97% 25ML 1,10-DibroModecane, 97% 500ML 1,10-Decamethylene Bromide 1,10-Decamethylene Dibromide 1,10-1,10-dibroModecane 1,10-DibroModecane, 99%+ ,w-Dibromodecane 1,10-dibromo-decan Decene, 1,10-dibromo 1,10-Dibromodecane, 97%, for synthesis 1,10-Dibromodecane > 1,10-Dibromodecane ISO 9001:2015 REACH 4101-68-2 C10H20Br2 BrCH210Br 4101682 Halogenated Hydrocarbons Organic Building Blocks Monofunctional & 伪,蠅-Bifunctional Alkanes 伪,蠅-Bifunctional Alkanes 伪,蠅-Dibromoalkanes Alkyl Building Blocks DIBROMOALKANE Bromine Compounds alpha,omega-Bifunctional Alkanes alpha,omega-Dibromoalkanes Monofunctional & alpha,omega-Bifunctional Alkanes