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1,10-Dibromodecane

1,10-Dibromodecane Structure
1,10-Dibromodecane structure
CAS No.
4101-68-2
Chemical Name:
1,10-Dibromodecane
Synonyms
DECAMETHYLENE DIBROMIDE;,w-Dibromodecane;Dibromodecane,95%;1,10-DIBROMODECANE;1,10-dibromo-decan;TIMTEC-BB SBB008900;Decene, 1,10-dibromo;DECAMETHYLENE BROMIDE;Decane, 1,10-dibromo-;1,10-DECANE DIBROMIDE
CBNumber:
CB3322169
Molecular Formula:
C10H20Br2
Molecular Weight:
300.07
MDL Number:
MFCD00000222
MOL File:
4101-68-2.mol
MSDS File:
SDS
Last updated:2026-05-28 03:29:11
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1,10-Dibromodecane Properties

Melting point 25-27 °C (lit.)
Boiling point 160 °C/15 mmHg (lit.)
Density 1.335 g/mL at 25 °C (lit.)
refractive index n20/D 1.4912(lit.)
Flash point 26°C
storage temp. Sealed in dry,Room Temperature
form Crystalline Low Melting Solid
Specific Gravity 1.335
color Beige to brown
Water Solubility insoluble
BRN 506156
Dielectric constant 6.5599999999999996
InChI 1S/C10H20Br2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2
InChIKey GTQHJCOHNAFHRE-UHFFFAOYSA-N
SMILES BrCCCCCCCCCCBr
CAS DataBase Reference 4101-68-2(CAS DataBase Reference)
NIST Chemistry Reference Decane, 1,10-dibromo-(4101-68-2)
EPA Substance Registry System Decane, 1,10-dibromo- (4101-68-2)
UNSPSC Code 12352100
NACRES NA.22

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P305+P351+P338
PPE Eyeshields, Gloves, type N95 (US)
Hazard Codes  C,Xi
Risk Statements  20/21/22-36/37/38
Safety Statements  22-24/25-36-26
WGK Germany  3
TSCA  TSCA listed
HS Code  29049090
Storage Class 11 - Combustible Solids
REACH Registrations Active
NFPA 704
1
0 0

1,10-Dibromodecane price More Price(43)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich D39800 1,10-Dibromodecane 97% 4101-68-2 100g $132 2026-04-30 Buy
TCI Chemical D0179 1,10-Dibromodecane >95.0%(GC) 4101-68-2 25g $27 2026-04-30 Buy
TCI Chemical D0179 1,10-Dibromodecane >95.0%(GC) 4101-68-2 100g $94 2026-04-30 Buy
AK Scientific J99517 1,10-Dibromodecane 97% 4101-68-2 5g $13 2026-06-04 Buy
AK Scientific J99517 1,10-Dibromodecane 97% 4101-68-2 25g $23 2026-06-04 Buy
Product number Packaging Price Buy
D39800 100g $132 Buy
D0179 25g $27 Buy
D0179 100g $94 Buy
J99517 5g $13 Buy
J99517 25g $23 Buy

1,10-Dibromodecane Chemical Properties,Uses,Production

Chemical Properties

beige to brown crystalline low melting mass

Uses

1,10-Dibromodecane is used as an alkylating agent and as synthetic organic intermediate.

Synthesis

1,10-Decanediol

112-47-0

1,10-Dibromodecane

4101-68-2

The general procedure for the synthesis of 1,10-dibromodecane from 1,10-decanediol is as follows: 1,10-decanediol (1 eq.), 48% aqueous hydrobromic acid (ca. 3 eq./hydroxyl), and octane (ca. 7:1 volume-to-weight ratio to the diol) were added to a single-necked, round-bottomed flask and assembled with a fractionating column/Dean-Stark trap. The reaction mixture was placed in a heated oil bath (145-150°C) with rapid magnetic stirring. The aqueous (lower) layer at the initial boiling point (89-92°C) was condensed and gently separated, and subsequently collected at about half the theoretical volume of water; at this point the temperature of the azeotrope (still at head temperature) began to rise. The condenser was set to full reflux for a few hours, then turned back on and the aqueous-phase material continued to be collected for 1 hour (top temperature 96-100°C). The final volume of the aqueous phase distillate reaches 90-100% of the theoretical value (up to 24% hydrobromic acid in the high boiling distillate). When the octane phase (which is light tan in color) contains dibromides and brominated streptanols (e.g., 6 band 6c), it is washed with cold 85% v/v sulfuric acid (10 mL first, then 5 mL) to remove all color and brominated streptanols. For all three dibromides (3b, 4b, 6b), the neutralized octane solution was passed through a Vigreux column under reduced pressure to remove the solvent, and the residue (which was confirmed to be essentially pure by 1H NMR) was purified by Kugelrohr distillation. Trace amounts of 4-methyltetrahydropyran were detected prior to distillation of 4b.

References

[1] Tetrahedron Letters, 2015, vol. 56, # 4, p. 630 - 632
[2] Green Chemistry, 2014, vol. 16, # 2, p. 836 - 843
[3] Journal of Organic Chemistry, 2015, vol. 80, # 11, p. 5386 - 5394
[4] Journal of the American Chemical Society, 1936, vol. 58, p. 488
[5] Journal of the Chemical Society, 1958, p. 2068

1,10-Dibromodecane synthesis

112-47-0
4101-68-2
Synthesis of 1,10-Dibromodecane from 1,10-Decanediol

1,10-Dibromodecane Preparation Products And Raw materials

Raw materials

Hydrogen bromide Decylene glycol 1,10-Decanediol Water n-Octane
7-Bromo-1-heptene Diethyl sebacate 11-Bromoundecanoic acid 1,9-Decadiene

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Preparation Products

12-Mercaptododecanoic acid Decane Tetradecanoic acid, 14-bromo-, methyl ester 9-DECEN-1-OL 1-Bromo-10-phenyldecane
10-Bromodecanol Ethyl 8-bromooctanoate

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1,10-Dibromodecane Suppliers

Global( 340)Suppliers
Supplier Tel Email Country ProdList Advantage
Qingdao Daopu Chemical Technology Co., LTD 15315511583 332054974@qq.com China 51 58
J & K SCIENTIFIC LTD. 18210857532 18210857532 jkinfo@jkchemical.com China 96815 76
Meryer (Shanghai) Chemical Technology Co., Ltd. 4006356688 18621169109 market03@meryer.com China 40202 62
future industrial shanghai co., ltd 400-0066400 13621662912 sales@jonln.com China 1989 65
Alfa Aesar 400-6106006 saleschina@alfa-asia.com China 30103 84
TCI (Shanghai) Development Co., Ltd. 021-67121386 Sales-CN@TCIchemicals.com China 24512 81
Ark Pharm, Inc. 847-367-3680 sales@arkpharminc.com United States 1669 56
Energy Chemical 400-0056266 sales8178@energy-chemical.com China 44850 61
Capot Chemical Co., Ltd +86 (0) 571 85 58 67 18 China 18187 66
Shanghai Longsheng chemical Co.,Ltd. 58099637 13585536065 sales@shlschem.com China 9880 59
Supplier Advantage
Qingdao Daopu Chemical Technology Co., LTD 58
J & K SCIENTIFIC LTD. 76
Meryer (Shanghai) Chemical Technology Co., Ltd. 62
future industrial shanghai co., ltd 65
Alfa Aesar 84
TCI (Shanghai) Development Co., Ltd. 81
Ark Pharm, Inc. 56
Energy Chemical 61
Capot Chemical Co., Ltd 66
Shanghai Longsheng chemical Co.,Ltd. 59

View Lastest Price from 1,10-Dibromodecane manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1,10-Dibromodecane pictures 2026-09-12 1,10-Dibromodecane
4101-68-2
 1KG ≥98.5% 20 Tons/Month Yancheng Longshen Chemical Co.,Ltd.
1,10-Dibromodecane pictures 2026-09-02 1,10-Dibromodecane
4101-68-2
 $1.00-100.00 1KG 99% Henan Fengda Chemical Co., Ltd
1,10-dibromodecane pictures 2026-05-28 1,10-dibromodecane
4101-68-2
 $1.00 1KG 99.% 50 ton Hebei Chuanghai Biotechnology Co,.LTD

1,10-Dibromodecane Spectrum

1,10-Dibromodecane(4101-68-2)MS1,10-Dibromodecane(4101-68-2)1HNMR1,10-Dibromodecane(4101-68-2)13CNMR1,10-Dibromodecane(4101-68-2)IR11,10-Dibromodecane(4101-68-2)IR21,10-Dibromodecane(4101-68-2)IR31,10-Dibromodecane(4101-68-2)Raman

4101-68-2(1,10-Dibromodecane)Related Search:

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Dibromodecane,95% TIMTEC-BB SBB008900 DECAMETHYLENE BROMIDE 1,10-DIBROMODECANE 1,10-DECAMETHYLENE BROMIDE 1,10-DECAMETHYLENE DIBROMIDE 1,10-DECANE DIBROMIDE Decane, 1,10-dibromo- 1,10-Dibromodecane,97% 1,10-Dibromodecane,Decamethylene dibromide 1,10-DibroModecane, 97% 100ML 1,10-DibroModecane, 97% 25ML 1,10-DibroModecane, 97% 500ML 1,10-Decamethylene Bromide 1,10-Decamethylene Dibromide 1,10-1,10-dibroModecane 1,10-DibroModecane, 99%+ ,w-Dibromodecane 1,10-dibromo-decan Decene, 1,10-dibromo 1,10-Dibromodecane, 97%, for synthesis 1,10-Dibromodecane > 1,10-Dibromodecane ISO 9001：2015 REACH DECAMETHYLENE DIBROMIDE 4101-68-2 C10H20Br2 BrCH210Br 4101682 Halogenated Hydrocarbons Organic Building Blocks Monofunctional & 伪,蠅-Bifunctional Alkanes 伪,蠅-Bifunctional Alkanes 伪,蠅-Dibromoalkanes Alkyl Building Blocks DIBROMOALKANE Bromine Compounds alpha,omega-Bifunctional Alkanes alpha,omega-Dibromoalkanes Monofunctional & alpha,omega-Bifunctional Alkanes