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2-Iodo-5-methoxyaniline

2-Iodo-5-methoxyaniline Structure
2-Iodo-5-methoxyaniline structure
CAS No.
153898-63-6
Chemical Name:
2-Iodo-5-methoxyaniline
Synonyms
2-Iodo-5-methoxyaniline;2-Iodo-5-methoxybenzenamine;2-Iodo-5-methoxy-phenylamine;BenzenaMine, 2-iodo-5-Methoxy-;1H-Pyrazol-5-amine,1-(3-methylethyl)-
CBNumber:
CB4130950
Molecular Formula:
C7H8INO
Molecular Weight:
249.05
MDL Number:
MFCD08458361
MOL File:
153898-63-6.mol
MSDS File:
SDS
Last updated:2026-09-12 18:52:20
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2-Iodo-5-methoxyaniline Properties

Melting point 33-36 °C(Solv: ethyl acetate (141-78-6))
Boiling point 298.4±30.0 °C(Predicted)
Density 1.807±0.06 g/cm3(Predicted)
storage temp. Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka 2.11±0.10(Predicted)
Appearance White to light brown Solid
InChI InChI=1S/C7H8INO/c1-10-5-2-3-6(8)7(9)4-5/h2-4H,9H2,1H3
InChIKey CYDBBGSUZRDOPE-UHFFFAOYSA-N
SMILES C1(N)=CC(OC)=CC=C1I

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P305+P351+P338

2-Iodo-5-methoxyaniline price More Price(35)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Usbiological 280733 2-Iodo-5-methoxyaniline Asreported 153898-63-6 250mg $389 2026-06-03 Buy
Usbiological 280733 2-Iodo-5-methoxyaniline Asreported 153898-63-6 500mg $545 2026-06-03 Buy
Usbiological 280733 2-Iodo-5-methoxyaniline Asreported 153898-63-6 1g $736 2026-06-03 Buy
Usbiological 280733 2-Iodo-5-methoxyaniline Asreported 153898-63-6 2g $992 2026-06-03 Buy
Usbiological 280733 2-Iodo-5-methoxyaniline Asreported 153898-63-6 5g $1380 2026-06-03 Buy
Product number Packaging Price Buy
280733 250mg $389 Buy
280733 500mg $545 Buy
280733 1g $736 Buy
280733 2g $992 Buy
280733 5g $1380 Buy

2-Iodo-5-methoxyaniline Chemical Properties, Uses, Production

Synthesis

4-IODO-3-NITROANISOLE

58755-70-7

2-IODO-5-METHOXYANILINE

153898-63-6

General procedure for the synthesis of 2-iodo-5-methoxyaniline from 4-iodo-3-nitroanisole: To a 100 mL methanol solution of 4-iodo-3-nitroanisole (5 g, 17.9 mmol) was added FeCl3 (50 mg, 0.3 mmol) and activated carbon (40 mg). The mixture was heated to reflux and hydrazine hydrate (1.75 g, 35 mmol) was added slowly and dropwise. After keeping the reaction at reflux for 8 h, it was cooled to room temperature and the reaction mixture was filtered through diatomaceous earth. The filtrate was concentrated and purified by column chromatography (eluent: hexane solution of 10% ethyl acetate) to afford 4.05 g of the target product 2-iodo-5-methoxyaniline as a light yellow oil (91% yield).1H NMR (300 MHz, CDCl3) δ 7.47 (1H, d, J = 8.7 Hz), 6.31 (1H, d, J = 2.8 Hz), 6.13 (1H, d, J = 2.8 Hz) 6.13 (1H, dd, J = 2.8, 8.7 Hz), 3.73 (3H, s).

References

[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 32, p. 7354 - 7358
[2] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[3] Patent: WO2003/106462, 2003, A1. Location in patent: Page 110
[4] Tetrahedron Letters, 2008, vol. 49, # 2, p. 363 - 366
[5] Angewandte Chemie - International Edition, 2010, vol. 49, # 48, p. 9262 - 9265

2-Iodo-5-methoxyaniline Preparation Products And Raw materials

Raw materials

4-Iodo-3-nitroanisole Methanol HYDRAZINE

Preparation Products

2-Amino-4-methoxy-benzoic acid D-Tryptophan, 6-methoxy-, ethyl ester 2-Ethynyl-5-methoxyaniline

2-Iodo-5-methoxyaniline Suppliers

Global Suppliers ( 97)
Supplier Tel Email Country ProdList Advantage
Shanghai Titan Enterprise Development Co., Ltd 16621224781 syy@titansci.com China 2893 58
Adamas Reagent, Ltd. 400-6009262 15618770481 yhx@titansci.com China 14098 59
Shanghai Hanhong Scientific Co.,Ltd. 021-54306202 13764082696 info@hanhongsci.com China 42917 64
Shanghai yirong biology science and technology co., ltd 18049974220 3060526242@qq.com China 999 60
Chengdu HappySyn Pharmaceutical Technology Co., Ltd. 85114309 18982182443 yangli@happysyn.com China 2284 55
Hangzhou Sage Chemical Co., Ltd. +86057186818502 13588463833 info@sagechem.com China 10265 58
Nanjing JinruiJiuAn Biotechnology Co., Ltd. 025-58196018 800028039 sales@fartop.net China 2227 55
Shanghai Topbiochem Technology Co., Ltd 021-58170097 info@topbiochem.com China 9510 58
Shanghai Topbiochem Technology Co., Ltd +86-21-60341587 sales@topbiochem.com China 6166 58
Shanghai Raise Chemical Technology Co.,Ltd +86-021-50935922 China 7854 55
Supplier Advantage
Shanghai Titan Enterprise Development Co., Ltd 58
Adamas Reagent, Ltd. 59
Shanghai Hanhong Scientific Co.,Ltd. 64
Shanghai yirong biology science and technology co., ltd 60
Chengdu HappySyn Pharmaceutical Technology Co., Ltd. 55
Hangzhou Sage Chemical Co., Ltd. 58
Nanjing JinruiJiuAn Biotechnology Co., Ltd. 55
Shanghai Topbiochem Technology Co., Ltd 58
Shanghai Topbiochem Technology Co., Ltd 58
Shanghai Raise Chemical Technology Co.,Ltd 55

View Latest Price from 2-Iodo-5-methoxyaniline manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2-IODO-5-METHOXYANILINE pictures 2020-02-01 2-IODO-5-METHOXYANILINE
153898-63-6
 $1.00 1KG 98% 200kgs Career Henan Chemical Co

2-Iodo-5-methoxyaniline Spectrum

2-IODO-5-METHOXYANILINE(153898-63-6)1HNMR

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BenzenaMine, 2-iodo-5-Methoxy- 2-Iodo-5-methoxy-phenylamine 2-Iodo-5-methoxybenzenamine 1H-Pyrazol-5-amine,1-(3-methylethyl)- 2-Iodo-5-methoxyaniline 153898-63-6