2-IODO-5-METHOXYANILINE
- CAS No.
- 153898-63-6
- Chemical Name:
- 2-IODO-5-METHOXYANILINE
- Synonyms
- 2-IODO-5-METHOXYANILINE;2-Iodo-5-methoxybenzenamine;2-Iodo-5-methoxy-phenylamine;BenzenaMine, 2-iodo-5-Methoxy-;1H-Pyrazol-5-amine,1-(3-methylethyl)-
- CBNumber:
- CB4130950
- Molecular Formula:
- C7H8INO
- Molecular Weight:
- 249.05
- MDL Number:
- MFCD08458361
- MOL File:
- 153898-63-6.mol
| Product description | Number | Pack Size | Price |
| 2-Iodo-5-methoxyaniline | I708655 | 50mg | $45 |
| 2-Iodo-5-methoxyaniline | W3349 | 5g | $444 |
| 2-IODO-5-METHOXYANILINE 95.00% | HCH0049825 | 1G | $852.55 |
| 2-IODO-5-METHOXYANILINE 95.00% | HCH0049825 | 2.5G | $1227.82 |
| 2-IODO-5-METHOXYANILINE 95.00% | HCH0049825 | 5G | $1548.26 |
| More product size | |||
| Melting point | 33-36 °C(Solv: ethyl acetate (141-78-6)) |
|---|---|
| Boiling point | 298.4±30.0 °C(Predicted) |
| Density | 1.807±0.06 g/cm3(Predicted) |
| storage temp. | Keep in dark place,Inert atmosphere,Store in freezer, under -20°C |
| pka | 2.11±0.10(Predicted) |
| Appearance | White to light brown Solid |
| InChI | InChI=1S/C7H8INO/c1-10-5-2-3-6(8)7(9)4-5/h2-4H,9H2,1H3 |
| InChIKey | CYDBBGSUZRDOPE-UHFFFAOYSA-N |
| SMILES | C1(N)=CC(OC)=CC=C1I |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
2-IODO-5-METHOXYANILINE price More Price(22)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | I708655 | 2-Iodo-5-methoxyaniline | 153898-63-6 | 50mg | $45 | 2021-12-16 | Buy |
| AK Scientific | W3349 | 2-Iodo-5-methoxyaniline | 153898-63-6 | 5g | $444 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0049825 | 2-IODO-5-METHOXYANILINE 95.00% | 153898-63-6 | 1G | $852.55 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0049825 | 2-IODO-5-METHOXYANILINE 95.00% | 153898-63-6 | 2.5G | $1227.82 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0049825 | 2-IODO-5-METHOXYANILINE 95.00% | 153898-63-6 | 5G | $1548.26 | 2021-12-16 | Buy |
2-IODO-5-METHOXYANILINE Chemical Properties,Uses,Production
Synthesis
58755-70-7
153898-63-6
General procedure for the synthesis of 2-iodo-5-methoxyaniline from 4-iodo-3-nitroanisole: To a 100 mL methanol solution of 4-iodo-3-nitroanisole (5 g, 17.9 mmol) was added FeCl3 (50 mg, 0.3 mmol) and activated carbon (40 mg). The mixture was heated to reflux and hydrazine hydrate (1.75 g, 35 mmol) was added slowly and dropwise. After keeping the reaction at reflux for 8 h, it was cooled to room temperature and the reaction mixture was filtered through diatomaceous earth. The filtrate was concentrated and purified by column chromatography (eluent: hexane solution of 10% ethyl acetate) to afford 4.05 g of the target product 2-iodo-5-methoxyaniline as a light yellow oil (91% yield).1H NMR (300 MHz, CDCl3) δ 7.47 (1H, d, J = 8.7 Hz), 6.31 (1H, d, J = 2.8 Hz), 6.13 (1H, d, J = 2.8 Hz) 6.13 (1H, dd, J = 2.8, 8.7 Hz), 3.73 (3H, s).
References
[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 32, p. 7354 - 7358
[2] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[3] Patent: WO2003/106462, 2003, A1. Location in patent: Page 110
[4] Tetrahedron Letters, 2008, vol. 49, # 2, p. 363 - 366
[5] Angewandte Chemie - International Edition, 2010, vol. 49, # 48, p. 9262 - 9265
2-IODO-5-METHOXYANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29795 | 58 |
| Hubei Ipure Biology Co., Ltd | +8613367258412 | ada@ipurechemical.com | China | 10236 | 58 |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | sales@win-winchemical.com | China | 14343 | 58 |
| CR Corporation Limited | +8613062833949 | fred.wen@crcorporation.cn | China | 8645 | 58 |
| Changzhou Fullone Chemical Co., Ltd. | +86-13328197671 +86-13861172460 | sales@borenchem.cn | China | 1055 | 58 |
| Changzhou Anxuan Chemical Co., Ltd | +86-0519-89882563 +86-18961279162 | andy@anxuanchem.com | China | 4327 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25356 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +8613336024896 | CB@aromsyn.com | China | 19183 | 58 |
View Lastest Price from 2-IODO-5-METHOXYANILINE manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-02-01 | 2-IODO-5-METHOXYANILINE
153898-63-6
|
US $1.00 / KG | 1KG | 98% | 200kgs | Career Henan Chemical Co |
-
- 2-IODO-5-METHOXYANILINE
153898-63-6
- US $1.00 / KG
- 98%
- Career Henan Chemical Co
