1,3-DibroMo-5-isopropoxybenzene
- CAS No.
- 1112210-82-8
- Chemical Name:
- 1,3-DibroMo-5-isopropoxybenzene
- Synonyms
- 3,5-Dibromoisopropoxybenzene;1,3-DibroMo-5-isopropoxybenzene;1,3-dibromo-5-propan-2-yloxybenzene;Benzene, 1,3-dibromo-5-(1-methylethoxy)-
- CBNumber:
- CB42651963
- Molecular Formula:
- C9H10Br2O
- Molecular Weight:
- 293.98
- MDL Number:
- MFCD12547881
- MOL File:
- 1112210-82-8.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319 |
| Precautionary statements | P261-P305+P351+P338 |
| HS Code | 2909303890 |
1,3-DibroMo-5-isopropoxybenzene price More Price(23)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR471673 | 1,3-Dibromo-5-isopropoxybenzene 97% | 1112210-82-8 | 1g | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR471673 | 1,3-Dibromo-5-isopropoxybenzene 97% | 1112210-82-8 | 5g | $33 | 2026-06-04 | Buy |
| Apolloscientific | OR471673 | 1,3-Dibromo-5-isopropoxybenzene 97% | 1112210-82-8 | 25g | $160 | 2026-06-04 | Buy |
| Apolloscientific | OR471673 | 1,3-Dibromo-5-isopropoxybenzene 97% | 1112210-82-8 | 100g | $509 | 2026-06-04 | Buy |
| Activate Scientific | AS47488 | 1,3-Dibromo-5-isopropoxybenzene 97% | 1112210-82-8 | 5g | $33 | 2026-06-04 | Buy |
1,3-DibroMo-5-isopropoxybenzene Chemical Properties, Uses, Production
Synthesis
1435-51-4
67-63-0
1112210-82-8
Synthesis of Intermediate Ia: 60% NaH mineral oil dispersion (1.89 g, 47.25 mmol) was slowly added dropwise to anhydrous DMF (20 mL) at 0 °C and protected by inert atmosphere. Isopropanol (3.62 mL, 47.25 mmol) was then added and the mixture was stirred at 0 °C for 15 min. Next, a solution of 1,3-dibromo-5-fluorobenzene (1.98 mL, 15.75 mmol) in anhydrous DMF (20 mL) was added dropwise at the same temperature. The reaction mixture was brought to room temperature and stirred continuously for 16 hours. Upon completion of the reaction, the reaction was quenched by slow addition of saturated NaHCO3 solution and the crude product was extracted twice with ether (Et2O). The organic layers were combined, washed sequentially with saturated NaHCO3 solution three times and saturated NaCl solution once, dried over anhydrous MgSO4 and concentrated to give yellow oil Ia in quantitative yield.1H NMR (300 MHz, CDCl3) δ 7.11 (t, J = 1.4 Hz, 1H), 6.97 (d, J = 1.5 Hz, 2H), 4.61- 4.40 (m, 1H), 1.32 (d, J = 6.0 Hz, 6H).
References
[1] Patent: WO2013/14170, 2013, A1. Location in patent: Page/Page column 62; 63
1,3-DibroMo-5-isopropoxybenzene Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14098 | 59 |
| SynAsst Chemical. | 021-60343070 | China | 12731 | 55 | |
| Shanghai ShiXian Chemical Technology Co., Ltd. | 13764359345 | 990877971@qq.com | China | 1921 | 50 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| AAB-PHARMA LIMITED | 025-66800956 18800000000 | sales@njdmchem.com | China | 4200 | 50 |
| Shanghai CR Corporation Limited | 13917420128 13062833949 | fred.wen@crcorporation.cn | China | 9775 | 58 |
| Aikon International Limited | 025-58859352 13913916777 | dt3@aikonchem.com | China | 15490 | 58 |
| 3A Chemicals | 400-668-9898 | service@3achem.com | China | 20535 | 58 |
| Shanghai SPAR pharmaceutical technology co., LTD | 021-000000 | admin@jingshipharmatech.com | China | 9919 | 58 |
| Shanghai Jizhi Biochemical Technology Co. Ltd. | 021-4009004166/18616739031 18616739031 | 3007523370@qq.com | China | 40000 | 58 |
