3-Methoxy-5-nitrobenzaldehyde
- CAS No.
- 354512-22-4
- Chemical Name:
- 3-Methoxy-5-nitrobenzaldehyde
- Synonyms
- 3-Methoxy-5-nitrobenzaldehyde;Benzaldehyde, 3-methoxy-5-nitro-
- CBNumber:
- CB4787943
- Molecular Formula:
- C8H7NO4
- Molecular Weight:
- 181.15
- MDL Number:
- MFCD09038015
- MOL File:
- 354512-22-4.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302 |
| Precautionary statements | P280-P305+P351+P338 |
3-Methoxy-5-nitrobenzaldehyde price More Price(21)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Synthonix | M48516 | 3-Methoxy-5-nitrobenzaldehyde 95+% | 354512-22-4 | 250mg | $120 | 2026-05-06 | Buy |
| Synthonix | M48516 | 3-Methoxy-5-nitrobenzaldehyde 95+% | 354512-22-4 | 1g | $470 | 2026-05-06 | Buy |
| Synthonix | M48516 | 3-Methoxy-5-nitrobenzaldehyde 95+% | 354512-22-4 | 5g | $1280 | 2026-05-06 | Buy |
| Synthonix | M48516 | 3-Methoxy-5-nitrobenzaldehyde 95+% | 354512-22-4 | 10g | $2220 | 2026-05-06 | Buy |
| aablocks | AA00CAG3 | 3-Methoxy-5-Nitrobenzaldehyde 95% | 354512-22-4 | 100mg | $234 | 2026-05-28 | Buy |
3-Methoxy-5-nitrobenzaldehyde Chemical Properties, Uses, Production
Synthesis
354525-36-3
354512-22-4
Step 3. (3-methoxy-5-nitrophenyl)methanol (75 g, 0.41 mol) was dissolved in dichloromethane (1.5 L) and cooled below 10°C. Under stirring, pyridinium dichromate (382 g, 1.02 mol) and silica gel (382 g) were added in batches. After addition, the reaction mixture was brought to room temperature and stirring was continued for 3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (Expanding agent: petroleum ether/ethyl acetate = 3:1, Rf = 0.6) to confirm the complete conversion of the raw material. Upon completion of the reaction, the crude product was purified by fast column chromatography (eluent: dichloromethane) to afford 3-methoxy-5-nitrobenzaldehyde as a yellow solid (170 g, 76% yield in 3 batches).
References
[1] Patent: WO2013/148365, 2013, A1. Location in patent: Paragraph 0095
[2] Journal of Medicinal Chemistry, 2004, vol. 47, # 11, p. 2897 - 2905
[3] MedChemComm, 2018, vol. 9, # 8, p. 1293 - 1304
3-Methoxy-5-nitrobenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
3-Methoxy-5-nitrobenzaldehyde Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Beijing Wuyunyongchang Science and Technology Co., Ltd. | 15210642910 | moon5.1days@126.com | China | 202 | 56 |
| Shanghai Tombiopharma Chemical Co. Ltd. | 13391076197 | tombiopharma@163.com | China | 4986 | 55 |
| Hotechem Shanghai Co., Ltd., | 021-34621078 13120882795 | 465106944@qq.com | China | 859 | 56 |
| SuZhou ShiYa Biopharmaceuticals, Inc. | 0512-0512-52358471 17715136450 | sales@shiyabiopharm.com | China | 9814 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Shanghai Pingguo Pharmaceutical Co., Ltd. | 021-20432229 | 2412110556@qq.com | China | 6016 | 55 |
| Sichuan BoYou Biotechnology Co., Ltd. | 028-65791793 18140026355 | 568470422@qq.com | China | 9961 | 58 |
| Wuxi AppTec | 022-59987777 13552403979 | jia_guoqiang@wuxiapptec.com | China | 22344 | 58 |
| Aikon International Limited | 025-66113011 19370895928 | qzhang@aikonchem.com | China | 15390 | 58 |
| Fan De(Beijing) Biotechnology Co., Ltd. | 15911056312 | liming@bio-fount.com | China | 9718 | 58 |
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