5-CHLORO-3-IODO-1H-INDAZOLE
- CAS No.
- 351456-45-6
- Chemical Name:
- 5-CHLORO-3-IODO-1H-INDAZOLE
- Synonyms
- 351456-46-5;5-CHLORO-3-IODOINDAZOLE;5-chloro-3-iodo-2H-indazole;5-CHLORO-3-IODO-1H-INDAZOLE;1H-Indazole, 5-chloro-3-iodo-
- CBNumber:
- CB5322673
- Molecular Formula:
- C7H4ClIN2
- Molecular Weight:
- 278.48
- MDL Number:
- MFCD06739146
- MOL File:
- 351456-45-6.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 5-Chloro-3-iodo-1H-indazole | OR60117 | 1g | $70 |
| 5-Chloro-3-iodo-1H-indazole | FC51611 | 250mg | $87.5 |
| 5-Chloro-3-iodo-1H-indazole | FC51611 | 500mg | $140 |
| 5-CHLORO-3-IODO-1H-INDAZOLE 95.00% | HCH0013556 | 250MG | $220.5 |
| 5-Chloro-3-iodo-1H-indazole | OR60117 | 500mg | $38 |
| More product size | |||
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| Hazard Codes | Xn |
| Risk Statements | 22 |
| HazardClass | IRRITANT |
| HS Code | 2933998090 |
5-CHLORO-3-IODO-1H-INDAZOLE price More Price(21)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR60117 | 5-Chloro-3-iodo-1H-indazole | 351456-45-6 | 1g | $70 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC51611 | 5-Chloro-3-iodo-1H-indazole | 351456-45-6 | 250mg | $87.5 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC51611 | 5-Chloro-3-iodo-1H-indazole | 351456-45-6 | 500mg | $140 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0013556 | 5-CHLORO-3-IODO-1H-INDAZOLE 95.00% | 351456-45-6 | 250MG | $220.5 | 2021-12-16 | Buy |
| Apolloscientific | OR60117 | 5-Chloro-3-iodo-1H-indazole | 351456-45-6 | 500mg | $38 | 2021-12-16 | Buy |
5-CHLORO-3-IODO-1H-INDAZOLE Chemical Properties,Uses,Production
Synthesis
698-26-0
351456-45-6
General procedure for the synthesis of 3-iodo-5-chloroindazole from 5-chloro-1H-indazole: the direct iodination reaction was carried out by referring to the method previously reported by Bocchi [28] with slight modifications. The procedure was as follows: 5-chloro-1H-indazole (3 g, 25.4 mmol), iodine (12.7 g, 50.03 mmol) and potassium hydroxide (5.34 g, 95.25 mmol) were dissolved in DMF (7 mL) and the reaction was stirred for 3 h at room temperature. Upon completion of the reaction, the reaction was quenched with saturated sodium bisulfite solution (150 mL), at which time a precipitate was generated. The precipitate was collected by vacuum filtration and washed with water three times (30 mL each). The resulting solid was dried in a vacuum oven at 30 °C overnight to give 6.17 g of the light yellow solid product 3-iodo-5-chloroindazole. Yield: 100%; Melting point: 136-138 °C (literature value:[36] 134-136 °C); IR (KBr) ν (cm^-1): 3086 (NH); 424 (C-I). 1H-NMR δ (ppm): 13.50 (1H, s, H-1); 7.55 (1H, d, J=8.6 Hz, H-7); 7.45- 7.40 (2H, m, H-6 and H-4); 7.19 (1H, dd, J=7.5Hz, H-5).13C-NMR δ (ppm): 140.41; 127.22; 126.79; 121.23; 120.39; 110.51; 93.49. HRMS calculated value C7H4ClIN2: 277.9107 , measured value: 277.9109.
References
[1] Molecules, 2018, vol. 23, # 8,
[2] Patent: WO2017/98328, 2017, A2. Location in patent: Paragraph 00208
[3] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 9, p. 2793 - 2800
5-CHLORO-3-IODO-1H-INDAZOLE Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Capot Chemical Co.,Ltd. | +86-（0）57185586718; +8613336195806 | sales@capot.com | China | 29735 | 60 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49975 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29799 | 58 |
| Zhejiang J&C Biological Technology Co.,Limited | +1-2135480471 | sales@sarms4muscle.com | China | 10473 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25356 | 58 |
| RR Scientific LLC | +86-13917743231 | sales@rrscientific.com | United States | 878 | 58 |
| GIHI CHEMICALS CO.,LIMITED | +8618058761490 | info@gihichemicals.com | China | 49948 | 58 |
| Xiamen Work-For-World Medicine Co.,Ltd. | +8615921822462 | co@wfwmed.com | China | 447 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52924 | 58 |
View Lastest Price from 5-CHLORO-3-IODO-1H-INDAZOLE manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
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2020-01-14 | 5-CHLORO-3-IODO-1H-INDAZOLE
351456-45-6
|
US $9.80 / KG | 1g | ≥99% | 100kg | Career Henan Chemical Co |
-
- 5-CHLORO-3-IODO-1H-INDAZOLE
351456-45-6
- US $9.80 / KG
- ≥99%
- Career Henan Chemical Co
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