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5-bromo-2-nitrobenzenamine

5-bromo-2-nitrobenzenamine Structure
5-bromo-2-nitrobenzenamine structure
CAS No.
5228-61-5
Chemical Name:
5-bromo-2-nitrobenzenamine
Synonyms
5-bromo-2-nitroanline;5-bromo-2-nitrobenzenamine;2-Amino-4-bromonitrobenzene;3-Amino-4-nitrobromobenzene;(5-BroMo-2-nitrophenyl)aMine;BenzenaMine, 5-broMo-2-nitro-
CBNumber:
CB71559911
Molecular Formula:
C6H5BrN2O2
Molecular Weight:
217.02
MDL Number:
MFCD09056836
MOL File:
5228-61-5.mol
MSDS File:
SDS
Last updated:2026-05-28 03:19:48
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5-bromo-2-nitrobenzenamine Properties

Melting point 151-152 °C
Boiling point 331.9±22.0 °C(Predicted)
Density 1.812±0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2–8 °C
form solid
pka -1.53±0.25(Predicted)
color Light yellow to yellow
InChI InChI=1S/C6H5BrN2O2/c7-4-1-2-6(9(10)11)5(8)3-4/h1-3H,8H2
InChIKey RMIFLIVHJLREFJ-UHFFFAOYSA-N
SMILES C1(N)=CC(Br)=CC=C1[N+]([O-])=O

SAFETY

Risk and Safety Statements

Symbol(GHS)  Skull and Crossbones (GHS06)
GHS06
Signal word  Danger
Hazard statements  H301+H311+H331-H315-H319
Precautionary statements  P501-P261-P270-P271-P264-P280-P337+P313-P305+P351+P338-P361+P364-P332+P313-P301+P310+P330-P302+P352+P312-P304+P340+P311-P403+P233-P405
HS Code  2921420090

5-bromo-2-nitrobenzenamine price More Price(49)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Activate Scientific AS39351 5-Bromo-2-nitroaniline 98% 5228-61-5 5g $21 2026-06-04 Buy
Apolloscientific OR61286 5-Bromo-2-nitroaniline ≥95% 5228-61-5 1g $21 2026-06-04 Buy
Apolloscientific OR61286 5-Bromo-2-nitroaniline ≥95% 5228-61-5 5g $24 2026-06-04 Buy
Activate Scientific AS39351 5-Bromo-2-nitroaniline 98% 5228-61-5 25g $47 2026-06-04 Buy
Apolloscientific OR61286 5-Bromo-2-nitroaniline ≥95% 5228-61-5 25g $35 2026-06-04 Buy
Product number Packaging Price Buy
AS39351 5g $21 Buy
OR61286 1g $21 Buy
OR61286 5g $24 Buy
AS39351 25g $47 Buy
OR61286 25g $35 Buy

5-bromo-2-nitrobenzenamine Chemical Properties, Uses, Production

Synthesis

1-Bromo-4-nitrobenzene

586-78-7

5-bromo-2-nitrobenzenamine

5228-61-5

General procedure for the synthesis of 2-nitro-5-bromoaniline from 1-bromo-4-nitrobenzene: Step 1: Synthesis of 5-bromo-2-nitroaniline (142) [0745] To a solution of ethylene glycol dimethyl ether (170 mL) containing potassium tert-butoxide (21.92 g, 195 mmol) and copper(I) chloride (2.36 g, 23.8 mmol) was added dropwise a solution of 1-bromo-4-nitrobenzene (141, 8.69 g, 43.0 mmol) in DMF (45 mL) at 0 °C and protected by nitrogen, the time of dropwise addition was 50 min. After the dropwise addition, the cooling bath was removed and the reaction mixture was continued to be stirred at room temperature for 4 hours. After completion of the reaction, the reaction solution was diluted with dichloromethane, washed sequentially with aqueous ammonium chloride, dried over anhydrous magnesium sulfate, filtered and concentrated to give the target compound 142 (7.85 g, 84% yield). [0746] 1H NMR (CDCl3) δ (ppm): 7.98 (d, J = 9.2 Hz, 1H), 7.02 (d, J = 2.0 Hz, 1H), 6.82 (dd, J = 9.2, 2.0 Hz, 1H), 6.12 (bs, 2H).

References

[1] Patent: WO2007/118137, 2007, A1. Location in patent: Page/Page column 109-110
[2] Journal of the Chemical Society - Perkin Transactions 1, 1999, # 11, p. 1437 - 1444
[3] Patent: WO2016/89830, 2016, A1. Location in patent: Page/Page column 43
[4] Patent: WO2016/89797, 2016, A1. Location in patent: Page/Page column 65
[5] Patent: WO2016/89833, 2016, A1. Location in patent: Page/Page column 42

5-bromo-2-nitrobenzenamine Preparation Products And Raw materials

Raw materials

3'-Bromoacetanilide 3-Bromo-4-nitroaniline 1-Bromo-4-nitrobenzene 2,4-Dibromo-1-nitrobenzene Methoxyamine Hydrochloride
Sulfuric acid 2-Fluoro-4-bromonitrobenzene 1,2-Dimethoxyethane 3-Bromoaniline Acetic acid

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Preparation Products

3,5-Dibromoaniline 4-Bromo-3-nitrobenzene-1,2-diamine 1,2-Diamino-3-chlorobenzene 5-broMobenzo[c][1,2,5]oxadiazole oxide

5-bromo-2-nitrobenzenamine Suppliers

Global Suppliers ( 126)
Supplier Tel Email Country ProdList Advantage
Shanghai Harvest Chemical Industrial Co., Ltd. 15721252604 17321035817 sales@harvest-chem.com China 2829 64
Energy Chemical 400-0056266 sales8178@energy-chemical.com China 44850 61
Shijiazhuang Sdyano Fine Chemical Co., Ltd. 0311-89250318 13582355795 master@sjzsdyn.com China 2776 65
Jia Xing Isenchem Co.,Ltd 0573-85285100 18627885956 isenchem@163.com China 9389 66
Accela ChemBio Co.,Ltd. 021-50795510 4000665055 marketing@accelachem.com China 10972 64
Shanghai Hanhong Scientific Co.,Ltd. 021-54306202 13764082696 info@hanhongsci.com China 42917 64
Shandong Xiya Chemical Co., Ltd 13355009207 13355009207 3007715519@qq.com China 18722 57
Shanghai Sunway Pharmaceutical Technology Co., Ltd 13761987713 hxzheng@sunwaypharm.cn China 8663 57
T&W GROUP 021-61551611 13296011611 contact@trustwe.com China 9884 58
Chiba Pharmaceutical Science and technology Co, Ltd. 0531-81313138 13066006660 chibapharm@foxmail.com China 3996 55
Supplier Advantage
Shanghai Harvest Chemical Industrial Co., Ltd. 64
Energy Chemical 61
Shijiazhuang Sdyano Fine Chemical Co., Ltd. 65
Jia Xing Isenchem Co.,Ltd 66
Accela ChemBio Co.,Ltd. 64
Shanghai Hanhong Scientific Co.,Ltd. 64
Shandong Xiya Chemical Co., Ltd 57
Shanghai Sunway Pharmaceutical Technology Co., Ltd 57
T&W GROUP 58
Chiba Pharmaceutical Science and technology Co, Ltd. 55

View Latest Price from 5-bromo-2-nitrobenzenamine manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
5-bromo-2-nitrobenzenamine pictures 2020-01-08 5-bromo-2-nitrobenzenamine
5228-61-5
 $1.00 1KG 99.0% 100kg Career Henan Chemical Co

5-bromo-2-nitrobenzenamine Spectrum

5-bromo-2-nitrobenzenamine(5228-61-5)1HNMR

5228-61-5 (5-bromo-2-nitrobenzenamine) Related Search:

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5-bromo-2-nitrobenzenamine 2-Amino-4-bromonitrobenzene (5-BroMo-2-nitrophenyl)aMine BenzenaMine, 5-broMo-2-nitro- 5-bromo-2-nitroanline 3-Amino-4-nitrobromobenzene 5228-61-5