1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID
- CAS No.
- 1779-10-8
- Chemical Name:
- 1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID
- Synonyms
- LABOTEST-BB LT00455402;6-Naphthaleneethanamine;4,7-Dibrom-3-hydroxy-2-naphthoesure;Isoxazole,3-(bromomethyl)-10-methyl-;4,7-DIBROMO-3-HYDROXY-2-NAPHTHOIC ACID;1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARB&;1,6-DIBROMO-2-NAPHTHOL-3-CARBOXYLIC ACID;4,7-Dibromo-3-hydroxy-2-naphthoicAcid>4,7-Dibromo-3-hydroxy-2-naphthoic acid 97%;4,7-dibromo-3-hydroxy-2-naphthalenecarboxylicaci
- CBNumber:
- CB7213566
- Molecular Formula:
- C11H6Br2O3
- Molecular Weight:
- 345.97
- MDL Number:
- MFCD00046367
- MOL File:
- 1779-10-8.mol
- MSDS File:
- SDS
| Melting point | 251-255 °C (lit.) |
|---|---|
| Boiling point | 427.6±45.0 °C(Predicted) |
| Density | 2.073±0.06 g/cm3(Predicted) |
| storage temp. | Sealed in dry,Room Temperature |
| form | powder to crystal |
| pka | 2.38±0.30(Predicted) |
| color | Light yellow to Yellow to Green |
| BRN | 2378969 |
| CAS DataBase Reference | 1779-10-8(CAS DataBase Reference) |
| EPA Substance Registry System | 2-Naphthalenecarboxylic acid, 4,7-dibromo-3-hydroxy- (1779-10-8) |
| UNSPSC Code | 12352100 |
1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID price More Price(26)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 638528 | 1,6-Dibromo-2-hydroxynaphthalene-3-carboxylic acid 97% | 1779-10-8 | 5g | $49.1 | 2023-06-20 | Buy |
| TCI Chemical | D3646 | 4,7-Dibromo-3-hydroxy-2-naphthoic Acid >98.0%(GC)(T) | 1779-10-8 | 5g | $184 | 2025-07-31 | Buy |
| TRC | D425773 | 1,6-Dibromo-2-hydroxynaphthalene-3-carboxylic acid | 1779-10-8 | 500mg | $65 | 2021-12-16 | Buy |
| TRC | D425773 | 1,6-Dibromo-2-hydroxynaphthalene-3-carboxylic acid | 1779-10-8 | 100mg | $45 | 2021-12-16 | Buy |
| Usbiological | 411451 | 1,6-Dibromo-2-hydroxynaphthalene-3-carboxylic acid | 1779-10-8 | 100mg | $305 | 2021-12-16 | Buy |
1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID Chemical Properties,Uses,Production
Chemical Properties
Light yellow solid
Synthesis
92-70-6
1779-10-8
In a 1 L three-necked flask, 3-hydroxy-2-naphthalenecarboxylic acid (50 g, 0.27 mol) was dissolved in 600 mL of glacial acetic acid and stirred until completely dissolved. Another 100 mL of glacial acetic acid was taken to dilute the bromine (34 mL, 0.67 mol), and the diluted bromine solution was slowly added dropwise to the reaction solution, controlling the reaction temperature between 20-30 °C. After the dropwise addition was completed, the reaction system was heated up to 120 °C, and the reaction was refluxed for 3 hours. After the reaction was completed, the heating was stopped and the reaction solution was allowed to cool naturally to room temperature. The cooled reaction solution was slowly poured into 3000 mL of ice water, and a large amount of yellow solid was precipitated. The solid product was collected by filtration, and the filter cake was washed with water and dried in an oven to give 84 g of intermediate 2 in 91% yield.
References
[1] Patent: CN106866433, 2017, A. Location in patent: Paragraph 0075; 0076; 0077
[2] Patent: EP2573067, 2013, A1. Location in patent: Paragraph 0051; 0052
[3] Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 791
[4] Journal of Medicinal Chemistry, 1990, vol. 33, # 1, p. 171 - 178
[5] Journal of Medicinal Chemistry, 2008, vol. 51, # 15, p. 4685 - 4698
1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Capot Chemical Co.,Ltd. | +8613336195806 | sales@capot.com | China | 29734 | 60 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-2158073036 | info@dakenam.com | China | 12930 | 58 |
| Zhejiang ZETian Fine Chemicals Co. LTD | +8618957127338 | stella@zetchem.com | China | 2161 | 58 |
| Changzhou Ansciep Chemical Co., Ltd. | +86 519 86305871 | sales@ansciepchem.com | CHINA | 4241 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29800 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | sales@win-winchemical.com | China | 14360 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52846 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +8613336024896 | CB@aromsyn.com | China | 19183 | 58 |
View Lastest Price from 1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-08 | 1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID
1779-10-8
|
US $3.00 / KG | 1KG | 98% | 200KG | Career Henan Chemical Co |
-
- 1,6-DIBROMO-2-HYDROXYNAPHTHALENE-3-CARBOXYLIC ACID
1779-10-8
- US $3.00 / KG
- 98%
- Career Henan Chemical Co
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