3-(DIMETHYLAMINO)-1-PHENYL-2-PROPEN-1-ONE
- CAS No.
- 1201-93-0
- Chemical Name:
- 3-(DIMETHYLAMINO)-1-PHENYL-2-PROPEN-1-ONE
- Synonyms
- 3-(Dimethylamino)-1-phenylprop-2-en-1-one;NSC 601833;3-(Dimethylamino)acrylophenone;3-(Dimethylamino)phenylpropenone;3-Dimethylamino-1-phenylpropenone;3-(DIMETHYLAMINO)-1-PHENYL-2-PROPEN-1-ONE;2-Propen-1-one, 3-(dimethylamino)-1-phenyl-;3-(N,N-Dimethylamino)-1-phenyl-2-propen-1-one;(2E)-3-(Dimethylamino)-1-phenylprop-2-en-1-one;3 - (dimethylamino) - 1 - (2-phenyl) - 2-propene-1-one
- CBNumber:
- CB7425011
- Molecular Formula:
- C11H13NO
- Molecular Weight:
- 175.23
- MDL Number:
- MFCD00121193
- MOL File:
- 1201-93-0.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Product description | Number | Pack Size | Price |
| 3-DIMETHYLAMINO-1-PHENYL-2-PROPEN-1-ONE AldrichCPR | S447862 | 1 unit | $197 |
| 3-DIMETHYLAMINO-1-PHENYL-2-PROPEN-1-ONE AldrichCPR | S447862 | 1G | $179 |
| 3-(Dimethylamino)-1-phenyl-2-propen-1-one >98.0%(GC)(T) | D5384 | 1g | $65 |
| 3-(Dimethylamino)-1-phenyl-2-propen-1-one >98.0%(GC)(T) | D5384 | 5g | $197 |
| (2E)-3-(Dimethylamino)-1-phenylprop-2-en-1-one 98% | OR15176 | 1g | $21 |
| More product size | |||
| Melting point | 91-93°C |
|---|---|
| Boiling point | 260.0±32.0 °C(Predicted) |
| Density | 1.022±0.06 g/cm3(Predicted) |
| storage temp. | Sealed in dry,Room Temperature |
| solubility | soluble in Methanol |
| form | powder to crystal |
| pka | 6.63±0.70(Predicted) |
| color | White to Yellow to Green |
| λmax | 325nm(lit.) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS02 |
|---|---|
| Signal word | Warning |
| Hazard statements | H228 |
| Precautionary statements | P240-P210-P241-P280-P370+P378 |
| Hazard Codes | Xi |
| HazardClass | IRRITANT |
| HS Code | 2922390090 |
3-(DIMETHYLAMINO)-1-PHENYL-2-PROPEN-1-ONE price More Price(73)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | S447862 | 3-DIMETHYLAMINO-1-PHENYL-2-PROPEN-1-ONE AldrichCPR | 1201-93-0 | 1 unit | $197 | 2026-04-30 | Buy |
| Sigma-Aldrich | S447862 | 3-DIMETHYLAMINO-1-PHENYL-2-PROPEN-1-ONE AldrichCPR | 1201-93-0 | 1G | $179 | 2024-03-01 | Buy |
| TCI Chemical | D5384 | 3-(Dimethylamino)-1-phenyl-2-propen-1-one >98.0%(GC)(T) | 1201-93-0 | 1g | $65 | 2026-04-30 | Buy |
| TCI Chemical | D5384 | 3-(Dimethylamino)-1-phenyl-2-propen-1-one >98.0%(GC)(T) | 1201-93-0 | 5g | $197 | 2026-04-30 | Buy |
| Apolloscientific | OR15176 | (2E)-3-(Dimethylamino)-1-phenylprop-2-en-1-one 98% | 1201-93-0 | 1g | $21 | 2026-06-04 | Buy |
3-(DIMETHYLAMINO)-1-PHENYL-2-PROPEN-1-ONE Chemical Properties,Uses,Production
Definition
ChEBI: 3-(dimethylamino)-1-phenylprop-2-en-1-one is a carbonyl compound.
Synthesis Reference(s)
Chemistry Letters, 13, p. 1419, 1984
The Journal of Organic Chemistry, 45, p. 4522, 1980 DOI: 10.1021/jo01310a058
Synthesis
4637-24-5
98-86-2
1201-93-0
In a 100 mL dry round-bottomed flask, acetophenone (1.08 g, 9 mmol) and N,N-dimethylformamide dimethyl acetal (3.9 mL, 30 mmol) were added with 30 mL of xylene as solvent. The reaction mixture was refluxed at 140 °C for 12 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) and the heating was stopped after confirming the completion of the reaction. The solvent was removed by distillation under reduced pressure and the resulting crude product was purified by fast column chromatography to afford 3-(dimethylamino)-1-phenyl-2-propen-1-one (1.48 g, 97% yield) as a light yellow solid.
References
[1] RSC Advances, 2017, vol. 7, # 45, p. 28483 - 28488
[2] Patent: CN108383763, 2018, A. Location in patent: Paragraph 0044; 0046
[3] Patent: US2011/195993, 2011, A1. Location in patent: Page/Page column 10; 14
[4] Journal of Organic Chemistry, 1980, vol. 45, # 24, p. 4857 - 4860
[5] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 4, p. 1214 - 1217
3-(DIMETHYLAMINO)-1-PHENYL-2-PROPEN-1-ONE Preparation Products And Raw materials
Raw materials
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Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Wuhan Chemwish Technology Co., Ltd | 027-67849912 | sales@chemwish.com | CHINA | 10821 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +86-189 4982 3763 | sales@tnjchem.com | China | 34563 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +86-13336024896 | CB@aromsyn.com | China | 19183 | 58 |
| SUZHOU SENFEIDA CHEMICAL CO.,LTD | +86-0512-83500002 +86-15195660023 | 3899766280@qq.com | China | 26362 | 58 |
| Aceschem Inc. | +1-817863-6948 +1-（817）863-6948 | sales@aceschem.com | United States | 19632 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 57505 | 58 | |
| Wuhan Fortuna Chemical Co.,Ltd | +86-2759207851; +86-18007136271 | hk@fortunachem.com | China | 6006 | 58 |
| DAYANG CHEM (HANGZHOU) CO.,LTD | +86-88938639 +86-17705817739 | info@dycnchem.com | China | 53803 | 58 |
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