3-CHLORO-4-ISOPROPOXY-BENZOIC ACID
- CAS No.
- 213598-07-3
- Chemical Name:
- 3-CHLORO-4-ISOPROPOXY-BENZOIC ACID
- Synonyms
- 3-CHLORO-4-ISOPROPOXY-BENZOIC ACID;3-chloro-4-propan-2-yloxybenzoic Acid;3-Chloro-4-(1-methylethoxy)benzoic acid;Benzoic acid, 3-chloro-4-(1-methylethoxy)-
- CBNumber:
- CB7841404
- Molecular Formula:
- C10H11ClO3
- Molecular Weight:
- 214.65
- MDL Number:
- MFCD08703674
- MOL File:
- 213598-07-3.mol
- MSDS File:
- SDS
3-CHLORO-4-ISOPROPOXY-BENZOIC ACID price More Price(22)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | C598313 | 3-Chloro-4-isopropoxybenzoicAcid | 213598-07-3 | 100mg | $65 | 2021-12-16 | Buy |
| ChemScene | CS-M0439 | 3-chloro-4-isopropoxybenzoicacid | 213598-07-3 | 1g | $70 | 2021-12-16 | Buy |
| ChemScene | CS-M0439 | 3-chloro-4-isopropoxybenzoicacid | 213598-07-3 | 5g | $229 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC150050 | 3-Chloro-4-isopropoxybenzoicacid | 213598-07-3 | 250mg | $75 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC150050 | 3-Chloro-4-isopropoxybenzoicacid | 213598-07-3 | 500mg | $100 | 2021-12-16 | Buy |
3-CHLORO-4-ISOPROPOXY-BENZOIC ACID Chemical Properties,Uses,Production
Synthesis
916596-04-8
213598-07-3
Step 2: Synthesis of 3-chloro-4-isopropoxybenzoic acid (34). To a stirred solution of 3-chloro-4-isopropoxybenzonitrile (33, 57 g, 291 mmol) in ethanol (EtOH, 120 mL) was added an aqueous 12% potassium hydroxide (KOH) solution (300 mL), and the reaction mixture was heated to 100 °C and kept for 3 h. The reaction was carried out with the addition of aqueous potassium hydroxide (KOH). Upon completion of the reaction, the mixture was cooled to room temperature and acidified with hydrochloric acid (HCl) to pH 5. A yellow solid precipitated during the acidification process, which was collected by filtration, washed with water and dried. The resulting solid was mixed with hexane, stirred for 5 minutes and decanted to remove the hexane. The process was repeated once, and the solid was resuspended in hexane, filtered, and washed with hexane to give 3-chloro-4-isopropoxybenzoic acid (34) as a white solid (45 g, 72% yield).
References
[1] Patent: WO2017/4609, 2017, A1. Location in patent: Paragraph 0277
[2] Patent: WO2017/4608, 2017, A1. Location in patent: Paragraph 0153
3-CHLORO-4-ISOPROPOXY-BENZOIC ACID Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| Accela ChemBio Inc. | +1-858-6993322 | info@accelachem.com | United States | 21193 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49975 | 58 |
| Labnetwork lnc. | +86-27-50766799 +8618062016861 | contact@labnetwork.com | China | 19987 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Shanghai Boc Chemical Co.,Ltd | 021-34975603-808 18721111801 | sales@bocpharma.com | China | 1010 | 64 |
| Shanghai T&W Pharmaceutical Co., Ltd. | +86 21 61551611 | China | 9891 | 58 | |
| Haoyuan Chemexpress Co., Ltd. | 021-58950125 | info@chemexpress.com | China | 7552 | 61 |
| Bide Pharmatech Ltd. | 400-164-7117 13681763483 | product02@bidepharm.com | China | 42446 | 60 |
| Shanghai YuanQi Biotechnology Co., Ltd. | +86-2332782371 +86-18120098618 | sales@adobechem.com | China | 1250 | 50 |
