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2-Methoxy-5-Iodopyridine

2-Methoxy-5-Iodopyridine Structure
2-Methoxy-5-Iodopyridine structure
CAS No.
13472-61-2
Chemical Name:
2-Methoxy-5-Iodopyridine
Synonyms
2-Methoxy-5-Iodopyridine;5-lodo-2-methoxypyridine;Pyridine, 5-iodo-2-methoxy-;5-Iodo-2-methoxypyridine>5-Iodo-2-methoxypyridine 98%
CBNumber:
CB81033218
Molecular Formula:
C6H6INO
Molecular Weight:
235.02
MDL Number:
MFCD07781180
MOL File:
13472-61-2.mol
MSDS File:
SDS
TDS File:
TDS
Last updated:2026-07-21 11:58:00
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2-Methoxy-5-Iodopyridine Properties

Boiling point 237℃
Density 1.825
refractive index 1.6060 to 1.6100
Flash point 97℃
storage temp. Keep in dark place,Inert atmosphere,Room temperature
form Liquid
pka 1.38±0.10(Predicted)
color Clear colorless to pale yellow
Sensitive Light Sensitive

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P280a-P304+P340-P305+P351+P338-P405-P501a
HS Code  29333990
NFPA 704
1
2 0

2-Methoxy-5-Iodopyridine price More Price(53)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical I0925 5-Iodo-2-methoxypyridine >98.0%(GC) 13472-61-2 1g $67 2026-04-30 Buy
TCI Chemical I0925 5-Iodo-2-methoxypyridine >98.0%(GC) 13472-61-2 5g $209 2026-04-30 Buy
Usbiological 280947 5-Iodo-2-methoxypyridine Asreported 13472-61-2 500mg $333 2026-06-03 Buy
Usbiological 280947 5-Iodo-2-methoxypyridine Asreported 13472-61-2 1g $512 2026-06-03 Buy
Usbiological 280947 5-Iodo-2-methoxypyridine Asreported 13472-61-2 2g $699 2026-06-03 Buy
Product number Packaging Price Buy
I0925 1g $67 Buy
I0925 5g $209 Buy
280947 500mg $333 Buy
280947 1g $512 Buy
280947 2g $699 Buy

2-Methoxy-5-Iodopyridine Chemical Properties, Uses, Production

Synthesis

5-Bromo-2-methoxypyridine

13472-85-0

2-Methoxy-5-Iodopyridine

13472-61-2

The general procedure for the synthesis of 5-bromo-2-methoxypyridine from 5-bromo-2-methoxypyridine was as follows: n-butyllithium (1.5 M in hexane solution, 4.98 mL, 7.47 mmol) was slowly added to a solution of isopropylmagnesium chloride (1.61 M in THF, 4.64 mL, 7.47 mmol) in THF (20 mL) under ice bath cooling conditions. The reaction mixture was stirred for 5 min to form a yellow solution after which 5-bromo-2-methoxypyridine (1.405 g, 0.98 mL, 7.10 mmol, 95%) was added. The resulting solution was continued to be stirred at 0 °C for 45 min. Molecular iodine (3.79 g, 14.94 mmol) was then added and the reaction mixture was stirred at 0°C for 30 minutes and then at room temperature for 1 hour. Upon completion of the reaction, the reaction was quenched by the addition of aqueous ammonium chloride (5 mL) and the organic and aqueous phases were separated. The aqueous phase was extracted with ethyl acetate (2 x 75 mL), and the combined organic layers were dried with magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (ethyl acetate-heptane, 5-80%) to afford the target product 5-iodo-2-methoxypyridine.

References

[1] Synthesis, 2012, vol. 44, # 5, p. 735 - 746
[2] Synthesis (Germany), 2015, vol. 47, # 20, p. 3231 - 3240
[3] Journal of the American Chemical Society, 2015, vol. 137, # 33, p. 10480 - 10483

2-Methoxy-5-Iodopyridine Preparation Products And Raw materials

Raw materials

5-Bromo-2-methoxypyridine n-Butyllithium Hexane Tetrahydrofuran iodine
Isopropylmagnesium chloride

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Preparation Products

2-Methoxy-5-Iodopyridine Suppliers

Global Suppliers ( 99)
Supplier Tel Email Country ProdList Advantage
Meryer (Shanghai) Chemical Technology Co., Ltd. 4006356688 18621169109 market03@meryer.com China 40202 62
Alfa Aesar 400-6106006 saleschina@alfa-asia.com China 30103 84
TCI (Shanghai) Development Co., Ltd. 021-67121386 Sales-CN@TCIchemicals.com China 24512 81
Energy Chemical 400-0056266 sales8178@energy-chemical.com China 44850 61
Capot Chemical Co., Ltd +86 (0) 571 85 58 67 18 China 18187 66
Shandong Xiya Chemical Co., Ltd 13355009207 13355009207 3007715519@qq.com China 18722 57
Shanghai Sunway Pharmaceutical Technology Co., Ltd 13761987713 hxzheng@sunwaypharm.cn China 8663 57
Thermo Fisher Scientific 800-810-5118 cnchemical@thermofisher.com China 17752 75
TOKYO CHEMICAL INDUSTRY CO., LTD. 03-36680489 Sales-JP@TCIchemicals.com Japan 28364 80
TCI Europe 320-37350700 sales@tcieurope.eu Europe 23654 75
Supplier Advantage
Meryer (Shanghai) Chemical Technology Co., Ltd. 62
Alfa Aesar 84
TCI (Shanghai) Development Co., Ltd. 81
Energy Chemical 61
Capot Chemical Co., Ltd 66
Shandong Xiya Chemical Co., Ltd 57
Shanghai Sunway Pharmaceutical Technology Co., Ltd 57
Thermo Fisher Scientific 75
TOKYO CHEMICAL INDUSTRY CO., LTD. 80
TCI Europe 75

View Latest Price from 2-Methoxy-5-Iodopyridine manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
5-Iodo-2-methoxypyridine pictures 2026-08-25 5-Iodo-2-methoxypyridine
13472-61-2
 $10.00-50.00 1KG 99% ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
5-Iodo-2-methoxypyridine pictures 2022-01-26 5-Iodo-2-methoxypyridine
13472-61-2
 1KG 98.7% 100 tons Honest Joy Holdings Limited
2-Methoxy-5-Iodopyridine pictures 2020-01-08 2-Methoxy-5-Iodopyridine
13472-61-2
 $1.00 1KG 99.0% 100kg Career Henan Chemical Co

13472-61-2 (2-Methoxy-5-Iodopyridine) Related Search:

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2-Methoxy-5-Iodopyridine 5-Iodo-2-methoxypyridine 98% 5-Iodo-2-methoxypyridine> Pyridine, 5-iodo-2-methoxy- 5-lodo-2-methoxypyridine 13472-61-2 Pyridine