3-Fluoro-5-nitrobenzonitrile
- CAS No.
- 110882-60-5
- Chemical Name:
- 3-Fluoro-5-nitrobenzonitrile
- Synonyms
- 3-Cyano-5-fluoronitrobenzene;3-Fluoro-5-nitrobenzonitrile;3-fluoro-5-nitrobenzenitrile;Benzonitrile,3-fluoro-5-nitro-;3-FLUORO-5-NITROBENZONITRILE, 97% MIN.
- CBNumber:
- CB8175935
- Molecular Formula:
- C7H3FN2O2
- Molecular Weight:
- 166.11
- MDL Number:
- MFCD05864356
- MOL File:
- 110882-60-5.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302+H312+H332-H315-H319-H335 |
| Precautionary statements | P261-P280-P305+P351+P338 |
| HS Code | 2926907090 |
3-Fluoro-5-nitrobenzonitrile price More Price(29)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| SynQuest Laboratories | 4655-3-53 | 3-Fluoro-5-nitrobenzonitrile 97% | 110882-60-5 | 5g | $595 | 2026-05-22 | Buy |
| Matrix Scientific | 114183 | 3-Fluoro-5-nitrobenzonitrile | 110882-60-5 | 1.00g | $480 | 2026-05-18 | Buy |
| aablocks | AA007BZ7 | 3-Fluoro-5-nitrobenzonitrile 97% | 110882-60-5 | 250mg | $20 | 2026-05-28 | Buy |
| aablocks | AA007BZ7 | 3-Fluoro-5-nitrobenzonitrile 97% | 110882-60-5 | 1g | $24 | 2026-05-28 | Buy |
| aablocks | AA007BZ7 | 3-Fluoro-5-nitrobenzonitrile 98% | 110882-60-5 | 5g | $78 | 2026-05-28 | Buy |
3-Fluoro-5-nitrobenzonitrile Chemical Properties, Uses, Production
Synthesis
3819-88-3
557-21-1
110882-60-5
Step 1: Zinc cyanide (0.92 eq.) and tetrakis(triphenylphosphine)palladium (0.058 eq.) were sequentially added to a 1.0 eq. solution of 1-fluoro-3-iodo-5-nitrobenzene in anhydrous DMF (0.37 M) under nitrogen protection. The reaction mixture was heated to 80 °C and the reaction was stirred overnight. Subsequently, 0.023 equivalents of tetrakis(triphenylphosphine)palladium was added and the reaction continued to be stirred at 80°C for 6 hours. Upon completion of the reaction, the mixture was cooled to room temperature and diluted with 15 volumes of ethyl acetate (based on the amount of 1-fluoro-3-iodo-5-nitrobenzene). The organic phase was sequentially washed three times with water and once with saturated saline. The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography with 10% ether/hexane as eluent to give 3-fluoro-5-nitrobenzonitrile as a solid in 90% yield.
References
[1] Patent: US2006/14761, 2006, A1. Location in patent: Page/Page column 29
[2] Patent: WO2007/75377, 2007, A2. Location in patent: Page/Page column 52-53
[3] Patent: WO2007/70626, 2007, A2. Location in patent: Page/Page column 40
[4] Patent: WO2007/70683, 2007, A2. Location in patent: Page/Page column 83
[5] Patent: WO2007/78839, 2007, A2. Location in patent: Page/Page column 40-41
3-Fluoro-5-nitrobenzonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Wuhan Chemwish Technology Co., Ltd | 86-027-67849912 | sales@chemwish.com | China | 35884 | 56 |
| Capot Chemical Co., Ltd | +86 (0) 571 85 58 67 18 | China | 18187 | 66 | |
| Shanghai Sinch Parmaceuticals Tech. Co. Ltd. | +86-21-54098501 | sales@sinch.com.cn | China | 11592 | 64 |
| Shanghai Harvest Chemical Industrial Co., Ltd. | 15721252604 17321035817 | sales@harvest-chem.com | China | 2829 | 64 |
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42917 | 64 |
| Shanghai Aladdin Bio-Chem Technology Co.,LTD | 400-6206333 13167063860 | anhua.mao@aladdin-e.com | China | 29985 | 65 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| Xinyanhe Pharmatech Co.,Ltd | 0519-85252752 15366845260 | taihuaren@vip.163.com | China | 1032 | 58 |
| Tianjin Anhao Biological Technology Co., Ltd. | sales@ahpharmatech.com | China | 5734 | 55 |
View Latest Price from 3-Fluoro-5-nitrobenzonitrile manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-12-27 | 3-FLUORO-5-NITROBENZONITRILE
110882-60-5
|
$6.60 | 1KG | 97%-99% | 1kg-1000kg | Career Henan Chemical Co |
-
- 3-FLUORO-5-NITROBENZONITRILE
110882-60-5
- $6.60
- 97%-99%
- Career Henan Chemical Co
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