ChemicalBook >> CAS DataBase List >>3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97

3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97

CAS No.
19962-04-0
Chemical Name:
3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97
Synonyms
Neostigmine bromide Impurity L;Neostigmine bromide Impurity 4;3-Aminophenyl dimethylcarbamate;3-aminophenyl N,N-dimethylcarbamate;Cyclobutanecarboxylicacid,3,5-difluoro-;3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97;N,N-Dimethylcarbamic acid 3-aminophenyl ester;Carbamic acid, N,N-dimethyl-, 3-aminophenyl ester
CBNumber:
CB8506775
Molecular Formula:
C9H12N2O2
Molecular Weight:
180.2
MDL Number:
MFCD00052699
MOL File:
19962-04-0.mol
MSDS File:
SDS
Last updated:2026-07-06 17:03:36
Product description Number Pack Size Price
3-Aminophenyl dimethylcarbamate 97% AS46543 1g $181
3-Aminophenyl dimethylcarbamate 97% AS46543 5g $522
3-Aminophenyl dimethylcarbamate 295519 250.00mg $62
3-Aminophenyl dimethylcarbamate 295519 1.00g $124
3-Aminophenyl dimethylcarbamate 295519 5.00g $358
More product size

3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 Properties

Melting point 85-88 °C
Boiling point 198-202 °C(Press: 9 Torr)
Density 1.176±0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2–8 °C
pka 3.69±0.10(Predicted)
Appearance Light yellow to yellow Solid

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P305+P351+P338

3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 price More Price(30)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Activate Scientific AS46543 3-Aminophenyl dimethylcarbamate 97% 19962-04-0 1g $181 2026-06-04 Buy
Activate Scientific AS46543 3-Aminophenyl dimethylcarbamate 97% 19962-04-0 5g $522 2026-06-04 Buy
Matrix Scientific 295519 3-Aminophenyl dimethylcarbamate 19962-04-0 250.00mg $62 2026-05-19 Buy
Matrix Scientific 295519 3-Aminophenyl dimethylcarbamate 19962-04-0 1.00g $124 2026-05-19 Buy
Matrix Scientific 295519 3-Aminophenyl dimethylcarbamate 19962-04-0 5.00g $358 2026-05-19 Buy
Product number Packaging Price Buy
AS46543 1g $181 Buy
AS46543 5g $522 Buy
295519 250.00mg $62 Buy
295519 1.00g $124 Buy
295519 5.00g $358 Buy

3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 Chemical Properties,Uses,Production

Synthesis

4-nitrophenyl dimethylcarbamate

7244-70-4

3-Aminophenol

591-27-5

3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97

19962-04-0

GENERAL STEPS: To a dry 500 mL four-necked round-bottomed flask were added dimethyl sulfoxide (DMSO, 100 mL), 3-aminophenol (67.5 g) and sodium hydroxide (NaOH, 24.7 g). The reaction mixture was heated to 75-80 °C and maintained at this temperature for 4 hours. Subsequently, 4-nitrophenyl-N,N-dimethylcarbamate (100 g) and DMSO (100 mL) were added in batches at the same temperature. The reaction temperature was raised to 110-120 °C and the reaction was continued for 2 hours. The progress of the reaction was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction was quenched with 1% sodium hydroxide solution (1500 mL). Extraction was carried out with methylene chloride (MDC), the organic layer was separated, washed with water, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was recrystallized with toluene to obtain pure 3-aminophenyl dimethylcarbamate. Yield: 62 g (72.2% yield). Melting point: 83-85°C (literature value: 80-86°C, FR 1498834).

References

[1] Patent: WO2017/175238, 2017, A1. Location in patent: Page/Page column 31

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View Lastest Price from 3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
N,N-Dimethylcarbamic acid 3-aminophenyl ester pictures 2026-07-06 N,N-Dimethylcarbamic acid 3-aminophenyl ester
19962-04-0
1kg 98 1000kgs Shaanxi Dideu New Materials Co. Ltd

3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 Spectrum

N,N-Dimethylcarbamic acid 3-aminophenyl ester 3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 3-Aminophenyl dimethylcarbamate 3-aminophenyl N,N-dimethylcarbamate Carbamic acid, N,N-dimethyl-, 3-aminophenyl ester Neostigmine bromide Impurity 4 Cyclobutanecarboxylicacid,3,5-difluoro- Neostigmine bromide Impurity L 19962-04-0