3,4-Dibromoanisole
- CAS No.
- 62415-74-1
- Chemical Name:
- 3,4-Dibromoanisole
- Synonyms
- 4-Dibromoanisole;3,4-Dibromoanisol;1,2-Dibromo-4-methoxybenzene;Benzene, 1,2-dibromo-4-methoxy-;3,4-Dibromoanisole 94%, remainder predominantly isomer
- CBNumber:
- CB91106771
- Molecular Formula:
- C7H6Br2O
- Molecular Weight:
- 265.93
- MDL Number:
- MFCD00070786
- MOL File:
- 62415-74-1.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| HS Code | 2909309090 |
3,4-Dibromoanisole price More Price(38)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR400564 | 3,4-Dibromoanisole >98% | 62415-74-1 | 5g | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR400564 | 3,4-Dibromoanisole >98% | 62415-74-1 | 25g | $30 | 2026-06-04 | Buy |
| Apolloscientific | OR400564 | 3,4-Dibromoanisole >98% | 62415-74-1 | 100g | $113 | 2026-06-04 | Buy |
| Apolloscientific | OR400564 | 3,4-Dibromoanisole >98% | 62415-74-1 | 500g | $555 | 2026-06-04 | Buy |
| Activate Scientific | AS49143 | 1,2-Dibromo-4-methoxybenzene 95% | 62415-74-1 | 5g | $26 | 2026-06-04 | Buy |
3,4-Dibromoanisole Chemical Properties, Uses, Production
Synthesis
2398-37-0
62415-74-1
GENERAL METHODS: N-bromosuccinimide (NBS, 1.5 eq., 0.3 mmol), catalyst (10 mol%, 0.02 mmol) and acetonitrile (CH3CN, 1.0 mL) were sequentially added to the reaction tube, followed by m-bromoanisole (0.2 mmol). The reaction mixture was stirred at room temperature for 12 hours away from light. Upon completion of the reaction, the reaction was quenched by the addition of saturated sodium thiosulfate (Na2S2O3) aqueous solution (2 mL). The reaction mixture was extracted with ethyl acetate (3.5 mL). The organic phases were combined, washed with saturated saline (10 mL), dried over anhydrous sodium sulfate (Na2SO4) and filtered through a diatomaceous earth pad. The filtrate was concentrated under reduced pressure and the residue was purified by rapid chromatography on a silica gel column with the eluent of petroleum ether/dichloromethane (5:1, v/v) to afford the target product 3,4-dibromoanisole.
References
[1] Tetrahedron, 2017, vol. 73, # 50, p. 7105 - 7114
[2] Bulletin de la Societe Chimique de France, 1981, vol. 1, # 1-2, p. 42 - 48
[3] Synthetic Communications, 2000, vol. 30, # 12, p. 2091 - 2098
3,4-Dibromoanisole Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Energy Chemical | 400-0056266 | sales8178@energy-chemical.com | China | 44850 | 61 |
| Shijiazhuang Sdyano Fine Chemical Co., Ltd. | 0311-89250318 13582355795 | master@sjzsdyn.com | China | 2776 | 65 |
| Capot Chemical Co., Ltd | +86 (0) 571 85 58 67 18 | China | 18187 | 66 | |
| Shanghai Harvest Chemical Industrial Co., Ltd. | 15721252604 17321035817 | sales@harvest-chem.com | China | 2829 | 64 |
| Shanghai Sphchem Co., Ltd. | 021-56491756 13512199871 | 2819742715@qq.com | China | 3994 | 55 |
| Nanjing Norris-Pharm Technology Co., Ltd | 13901585132 | sales@norris-pharm.com | China | 8869 | 55 |
| Jiangsu Aikon Biopharmaceutical R&D co.,Ltd. | 025-66113011 13913916777 | cfzhang@aikonchem.com | China | 19902 | 55 |
| 9ding chemical ( Shanghai) Limited | 4009209199 | sales@9dingchem.com | China | 18201 | 56 |
| Shanghai Aladdin Bio-Chem Technology Co.,LTD | 400-6206333 13167063860 | anhua.mao@aladdin-e.com | China | 29977 | 65 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
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