9-(1-Naphthyl) carbazole
- CAS No.
- 22034-43-1
- Chemical Name:
- 9-(1-Naphthyl) carbazole
- Synonyms
- 9-(naphthalen-1-yl)-9H-carbazole;DYPR0399;9-Napthylcarbazole;9-(1-Naphthyl) carbazole;9-(1-Naphthyl)carbazole>9-naphthalen-1-ylcarbazole;9-(1-naphthalenyl)-9H-Carbazole;9H-Carbazole, 9-(1-naphthalenyl)-
- CBNumber:
- CB92686654
- Molecular Formula:
- C22H15N
- Molecular Weight:
- 293.36
- MDL Number:
- MFCD26127424
- MOL File:
- 22034-43-1.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Melting point | 126.0 to 131.0 °C |
|---|---|
| Boiling point | 503.7±23.0 °C(Predicted) |
| Density | 1.15±0.1 g/cm3(Predicted) |
| storage temp. | Sealed in dry,Room Temperature |
| form | powder to crystal |
| color | White to Almost white |
| λmax | 321nm(Cyclohexane)(lit.) |
| InChI | InChI=1S/C22H15N/c1-2-10-17-16(8-1)9-7-15-20(17)23-21-13-5-3-11-18(21)19-12-4-6-14-22(19)23/h1-15H |
| InChIKey | QSOAYCUFEQGHDN-UHFFFAOYSA-N |
| SMILES | N1(C2=C3C(C=CC=C3)=CC=C2)C2=C(C=CC=C2)C2=C1C=CC=C2 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319 |
| Precautionary statements | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 |
| HS Code | 2933.99.9701 |
9-(1-Naphthyl) carbazole price More Price(20)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemical | N1012 | 9-(1-Naphthyl)carbazole >98.0%(GC) | 22034-43-1 | 1g | $121 | 2026-04-30 | Buy |
| TCI Chemical | N1012 | 9-(1-Naphthyl)carbazole >98.0%(GC) | 22034-43-1 | 5g | $426 | 2026-04-30 | Buy |
| Chem-Impex | 42740 | 9-(1-Naphthyl)carbazole ≥98%(GC) | 22034-43-1 | 1G | $217.33 | 2026-05-19 | Buy |
| Chem-Impex | 42740 | 9-(1-Naphthyl)carbazole ≥98%(GC) | 22034-43-1 | 5G | $801.7 | 2026-05-19 | Buy |
| aablocks | AA00C1KO | 9-(Naphthalen-1-yl)-9H-carbazole 97% | 22034-43-1 | 1g | $8 | 2026-05-28 | Buy |
9-(1-Naphthyl) carbazole Chemical Properties, Uses, Production
Uses
9-(Naphthalen-1-yl)-9H-carbazole is a useful research chemical.
Synthesis
90-11-9
86-74-8
22034-43-1
[Example 8]; [0397] In this embodiment, the method for the synthesis of 2-{N-(1-naphthalenyl)-N-[9-(1-naphthalenyl)carbazol-3-yl]amino}-9,10-diphenylanthracene (abbreviation: 2NCNPA) is specifically described by the anthracene derivative of the present invention represented by structural formula (220). ; [Step 1] Synthesis of N,N-diethylnaphthalenyl-H-carbazol-S-amine (abbreviation: NCN) (i) Synthesis of 9-(1-naphthalenyl)carbazole. the scheme for the synthesis of 9-(1-naphthalenyl)carbazole is illustrated in (C-18). 21 g (0.1 mol) of 1-bromonaphthalene, 17 g (0.1 mol) of carbazole, 950 mg (5 mmol) of copper (I) iodide, 33 g (240 mmol) of potassium carbonate, and 660 mg (2.5 mmol) of 18-crown-6-ether were added to a 500 mL three-necked flask with nitrogen displacement. To this mixture was added 80 mL of 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone (abbreviation: DMPU), which was then stirred at 170 °C for 6 h under nitrogen protection. To this reaction mixture was added a further 10 g (50 mmol) of 1-bromonaphthalene, 2.0 g (10 mmol) of copper (I) iodide and 2.6 g (10 mmol) of 18-crown-6-ether and stirring was continued at 170 °C for 7.5 hours. Further 10 g (50 mmol) of 1-bromonaphthalene was added to this reaction mixture and stirring was continued at 180 °C for 6 hours. Upon completion of the reaction, about 200 mL of toluene and about 100 mL of 1 mol/L hydrochloric acid were added to this reaction mixture, and then the mixture was filtered through diatomaceous earth. The resulting filtrate was sequentially filtered through Florisil and diatomaceous earth. The organic and aqueous layers of the resulting filtrate were separated, and the organic layer was washed with 1 mol/L hydrochloric acid, then with water, and finally dried with magnesium sulfate. The suspension was filtered through Florisil and diatomaceous earth. The filtrate was concentrated to give an oil to which methanol was added and sonicated to precipitate solids. The precipitated solid was collected by filtration to give 22 g of 9-(1-naphthyl)carbazole as a white powder (75% yield).The Rf values (SiO2, eluent; hexane:ethyl acetate=10:1) for 9-(1-naphthyl)carbazole, 1-bromonaphthalene, and carbazole were 0.61, 0.74, and 0.24, respectively.
References
[1] Patent: WO2007/125934, 2007, A1. Location in patent: Page/Page column 168-169
[2] Patent: WO2009/72587, 2009, A1. Location in patent: Page/Page column 237-238
[3] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2006, vol. 63, # 1, p. 15 - 20
[4] Journal of Organic Chemistry, 2009, vol. 74, # 9, p. 3341 - 3349
9-(1-Naphthyl) carbazole Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Puyang Huicheng Electronic Material Co. Ltd. | 0393-0393-8910800 15039333257 | info@huichengchem.com | China | 588 | 64 |
| Suzhou Shanyang Pharmaceutical Technology Co., | 0512-63268889 18506119477 | 82169840@qq.com | China | 624 | 58 |
| Yurui (Shanghai) Chemical Co., Ltd. | 02150456736 18602143071 | Jenny@riyngroup.com | China | 500 | 30 |
| Harbin Jiekai new material Co., Ltd. | 15104587591; 18245017205 | sales@jiekaichem.com | China | 38 | 58 |
| TCI (Shanghai) Development Co., Ltd. | 021-67121386 | Sales-CN@TCIchemicals.com | China | 24512 | 81 |
| Jia Xing Isenchem Co.,Ltd | 0573-85285100 18627885956 | isenchem@163.com | China | 9389 | 66 |
| Beijing Green Guardee Technology CO,.LTD | 010- 89781189-8112 18511583708 | sales2@greenguardee.com | China | 294 | 56 |
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14098 | 59 |
| Shandong Xiya Chemical Co., Ltd | 13355009207 13355009207 | 3007715519@qq.com | China | 18722 | 57 |
| Spectrum Chemical Manufacturing Corp. | 021-021-021-67601398-809-809-809 15221380277 | marketing_china@spectrumchemical.com | China | 9643 | 60 |
View Latest Price from 9-(1-Naphthyl) carbazole manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2026-09-02 | 9-(1-Naphthyl) carbazole
22034-43-1
|
$1.00-200.00 | 1KG | 99%, 99.5% Sublimated | Henan Fengda Chemical Co., Ltd | ||
 |
2026-07-17 | 9-(Naphthalen-1-yl)-9H-carbazole
22034-43-1
|
1kg | 99.9% | 500kg | Changzhou Mascot Import & Export Co., Ltd | ||
 |
2026-06-30 | 9-(1-Naphthyl) carbazole
22034-43-1
|
1kg | 99% | 10000KGS | Shaanxi Dideu New Materials Co. Ltd |
-
- 9-(1-Naphthyl) carbazole
22034-43-1
- $1.00-200.00
- 99%, 99.5% Sublimated
- Henan Fengda Chemical Co., Ltd
-
- 9-(Naphthalen-1-yl)-9H-carbazole
22034-43-1
- 99.9%
- Changzhou Mascot Import & Export Co., Ltd
-
- 9-(1-Naphthyl) carbazole
22034-43-1
- $0.00
- 99%
- Shaanxi Dideu New Materials Co. Ltd
