2-Bromo-5-methoxybenzylamine
- CAS No.
- 887581-09-1
- Chemical Name:
- 2-Bromo-5-methoxybenzylamine
- Synonyms
- 2-Bromo-5-methoxybenzylamine;2-bromo-5-methxoxybenzylamine;(2-BROMO-5-METHOXYPHENYL)METHANAMINE;Benzenemethanamine,2-bromo-5-methoxy-
- CBNumber:
- CB9380246
- Molecular Formula:
- C8H10BrNO
- Molecular Weight:
- 216.08
- MDL Number:
- MFCD07786684
- MOL File:
- 887581-09-1.mol
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
2-Bromo-5-methoxybenzylamine price
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS117965 | (2-Bromo-5-methoxyphenyl)methanamine 97% | 887581-09-1 | 1g | $211 | 2026-06-04 | Buy |
| Activate Scientific | AS117965 | (2-Bromo-5-methoxyphenyl)methanamine 97% | 887581-09-1 | 5g | $660 | 2026-06-04 | Buy |
| Matrix Scientific | 213862 | 2-Bromo-5-methoxybenzylamine | 887581-09-1 | 100.00mg | $47 | 2026-05-18 | Buy |
| Matrix Scientific | 213862 | 2-Bromo-5-methoxybenzylamine | 887581-09-1 | 250.00mg | $57 | 2026-05-18 | Buy |
| Matrix Scientific | 213862 | 2-Bromo-5-methoxybenzylamine | 887581-09-1 | 1.00g | $100 | 2026-05-18 | Buy |
2-Bromo-5-methoxybenzylamine Chemical Properties,Uses,Production
Synthesis
138642-47-4
887581-09-1
Step A: Synthesis of 1-(2-bromo-5-methoxyphenyl)methanamine 2-Bromo-5-methoxybenzonitrile (10.0 g, 47.2 mmol) was dissolved in dry tetrahydrofuran (100 mL) in a flame-dried flask and cooled in an ice bath. A solution of borane-tetrahydrofuran complex (75 mL, 75 mmol, 1.0 M) was added slowly and dropwise over 30 min. The reaction mixture was stirred overnight at room temperature and then the reaction was slowly quenched with ice water and saturated aqueous sodium carbonate solution. Tetrahydrofuran was removed by distillation under reduced pressure and the residue was extracted with ethyl acetate (EtOAc) several times (3 times). The organic layers were combined, washed with water, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography to afford the target product 1-(2-bromo-5-methoxyphenyl)methanamine as a white powder (3.65 g, 36% yield). m/z = 216.9, 219.0 for C8H10BrNO ([M+H]+) by LCMS analysis.
References
[1] Patent: US2010/190804, 2010, A1. Location in patent: Page/Page column 75-76
[2] Patent: WO2004/14384, 2004, A2. Location in patent: Page/Page column 235-236; 239
2-Bromo-5-methoxybenzylamine Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
2-Bromo-5-methoxybenzylamine Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
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| LABTER PHARMATECH(BEIJING) CO.,LTD | 010-56330744 18310155299 | sales@labter.com.cn | China | 19999 | 55 |
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| Shanghai Jizhi Biochemical Technology Co. Ltd. | 021-4009004166/18616739031 18616739031 | 3007523370@qq.com | China | 40000 | 58 |
| Jiangsu aikang biomedical research and development co., LTD | 025-58859352 17714375163 | qzhang@aikonchem.com | China | 15525 | 58 |
