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BIS(2,4-DINITROPHENYL) CARBONATE

BIS(2,4-DINITROPHENYL) CARBONATE structure

CAS No.: 7497-12-3

Chemical Name:: BIS(2,4-DINITROPHENYL) CARBONATE

Synonyms: AI3-14991;BIS(2,4-DINITROPHENYL) CARBONATE;Phenol, 2,4-dinitro-, 1,1'-carbonate

CBNumber:: CB9387366

Molecular Formula:: C13H6N4O11

Molecular Weight:: 394.21

MDL Number:: MFCD00056106

MOL File:: 7497-12-3.mol

Last updated:2024-12-24 13:20:50

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BIS(2,4-DINITROPHENYL) CARBONATE Properties

Melting point	148 °C(Solv: benzene (71-43-2))
Boiling point	583.5±50.0 °C(Predicted)
Density	1.741±0.06 g/cm3(Predicted)
solubility	sol EtOAc, pyridine, DMF, CHCl3; moderately sol benzene; insol hexane; dec hot H2O, EtOH
color	yellow solid

BIS(2,4-DINITROPHENYL) CARBONATE price

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
aablocks	AA00G78Y	BIS(2,4-DINITROPHENYL) CARBONATE	7497-12-3	5g	$538	2026-05-28	Buy
American Custom Chemicals Corporation	CHM0028671	BIS(2,4-DINITROPHENYL) CARBONATE 95.00%	7497-12-3	10G	$1455.3	2021-12-16	Buy

Product number	Packaging	Price	Buy
AA00G78Y	5g	$538	Buy
CHM0028671	10G	$1455.3	Buy

BIS(2,4-DINITROPHENYL) CARBONATE Chemical Properties,Uses,Production

Description

Bis(2,4-dinitrophenyl)carbonate is used in the preparation of azapeptides.

Uses

Peptide and azapeptide coupling reagent that functions by activating amines, forming derivatives suitable for condensation with N-protected amino acids; converts carboxylic acids to activated esters.

Synthesis

Diphenyl carbonate (20 g) is added to a stirred mixture of conc HNO3 (100 mL) and conc H2SO4 (120 mL) at 50-55 °C over 1 h. The resulting suspension is stirred at 50 °C for 3 h, left at rt for 90 h and poured onto ice. The precipitate is washed with iced water and dried in vacuo over P2O5. This affords bis(2,4-dinitrophenyl) carbonate (31.2 g, 85%) which recrystallizes from hexane/benzene giving crystals, mp 144-146 °C.

Precautions

Store in a cool dry place to preclude contact with moisture; the hazardous and toxicological properties have not been investigated; may explode if heated rapidly

BIS(2,4-DINITROPHENYL) CARBONATE Preparation Products And Raw materials

Raw materials

Preparation Products

BIS(2,4-DINITROPHENYL) CARBONATE Suppliers

Global( 9)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Meryer (Shanghai) Chemical Technology Co., Ltd.	4006356688 18621169109	market03@meryer.com	China	40202	62
TargetMol Chemicals Inc.	15002134094	marketing@targetmol.cn	China	29874	58
TargetMol Chemicals Inc.	+1-781-999-5354;	support@targetmol.com	United States	38999	58

Supplier	Advantage
Meryer (Shanghai) Chemical Technology Co., Ltd.	62
TargetMol Chemicals Inc.	58
TargetMol Chemicals Inc.	58

7497-12-3(BIS(2,4-DINITROPHENYL) CARBONATE)Related Search:

Bis(2,4-dinitrophenyl) carbonate Diphenoxymethane Diphenyl carbonate BIS(4-NITROPHENYL) CARBONATE 4-METHOXY-3-NITROANILINE

1-Methoxy-2,4-dinitrobenzene

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BIS(2,4-DINITROPHENYL) CARBONATE Phenol, 2,4-dinitro-, 1,1'-carbonate AI3-14991 7497-12-3 C13H6N4O11 pharmacetical