3-Bromopropylacetate
- CAS No.
- 592-33-6
- Chemical Name:
- 3-Bromopropylacetate
- Synonyms
- 1-Propanol, 3-bromo-, 1-acetate
- CBNumber:
- CB9971628
- Molecular Formula:
- C5H9BrO2
- Molecular Weight:
- 181.03
- MDL Number:
- MFCD02258489
- MOL File:
- 592-33-6.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H315-H319-H335 | |||||||||
| Precautionary statements | P261-P305+P351+P338 | |||||||||
| HS Code | 2915.39.9000 | |||||||||
| NFPA 704 |
|
3-Bromopropylacetate price More Price(16)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemical | B5650 | 3-Bromopropyl Acetate >98.0%(GC) | 592-33-6 | 1g | $59 | 2026-04-30 | Buy |
| TCI Chemical | B5650 | 3-Bromopropyl Acetate >98.0%(GC) | 592-33-6 | 5g | $204 | 2026-04-30 | Buy |
| Synthonix | B41266 | 3-Bromopropyl acetate 95% | 592-33-6 | 100mg | $15 | 2026-05-06 | Buy |
| Synthonix | B41266 | 3-Bromopropyl acetate 95% | 592-33-6 | 250mg | $56.96 | 2026-05-06 | Buy |
| Synthonix | B41266 | 3-Bromopropyl acetate 95% | 592-33-6 | 1g | $60 | 2026-05-06 | Buy |
3-Bromopropylacetate Chemical Properties, Uses, Production
Synthesis
108-24-7
627-18-9
592-33-6
General procedure for the synthesis of propyl 3-bromoacetate from ethanoic anhydride and 3-bromo-1-propanol: To a stirred solution of 3-bromo-1-propanol (8.0 g, 57.55 mmol) in anhydrous dichloromethane (40 mL) was added triethylamine (12 mL, 86.32 mmol) and stirred for 1 h at room temperature. Ethanoic anhydride (6.5 mL, 69.06 mmol) dissolved in dichloromethane (5 mL) was added dropwise at 0 °C, followed by stirring for 16 h at room temperature. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was quenched with 1N hydrochloric acid solution and extracted with dichloromethane. The combined organic layers were washed with brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by column chromatography with 10% ethyl acetate/hexane as eluent to give the target product propyl 3-bromoacetate. Yield: 10.0 g, 96% yield; 1H NMR (400 MHz, CDCl3) δ 4.19-4.17 (m, 2H), 3.47 (t, J=6.5 Hz, 2H), 2.21-2.18 (m, 2H), 2.06 (s, 3H).
References
[1] Patent: WO2017/6283, 2017, A1. Location in patent: Paragraph 0474; 0475
[2] Patent: WO2018/98206, 2018, A1. Location in patent: Paragraph 0940
[3] Patent: WO2008/39999, 2008, A1. Location in patent: Page/Page column 49
[4] Patent: TW2017/8220, 2017, A. Location in patent: Page/Page column 73; 74
[5] Chemistry - A European Journal, 2003, vol. 9, # 14, p. 3353 - 3366
3-Bromopropylacetate Preparation Products And Raw materials
3-Bromopropylacetate Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Nanjing Chemlin Chemical Co., Ltd | 025-83697070 13770331960 | info@chemlin.com.cn | China | 16305 | 64 |
| TOKYO CHEMICAL INDUSTRY CO., LTD. | 03-36680489 | Sales-JP@TCIchemicals.com | Japan | 28364 | 80 |
| TCI Europe | 320-37350700 | sales@tcieurope.eu | Europe | 23654 | 75 |
| TCI AMERICA | 800-4238616 | sales@tciamerica.com | Americas | 23636 | 75 |
| Mashilabs (Shanghai) Co.,Ltd. | 19916721580 | mafarm@126.com | China | 4534 | 58 |
| Taizhou GreenChem Pharmaceutical Co., Ltd. | 0514-86654616 15366892466; | greenchem@tzglmk.com | China | 498 | 56 |
| BTC Pharmaceutical CO. Ltd | +86-15716293042 15716293042 | info@btcpharm.com | China | 822 | 55 |
| Shanghai YuanYe Biotechnology Co., Ltd. | 15026964105 | 2881489226@qq.com | China | 89667 | 60 |
| Zhengzhou Huiju Chemical Co., Ltd. | 0371-55900031 18137872243 | 3927209986@qq.com | China | 9999 | 55 |
| Aikon International Limited | 025-58859352 15955137747 | sales01@aikonchem.com | China | 16021 | 58 |
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