| Company Name: |
DebyeTec.com Inc.
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| Tel: |
18086626237 18086626237 |
| Email: |
2693528373@qq.com |
| Products Intro: |
CAS:326-67-0
Purity:95+% Package:1g;25g;100g;1kg;
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| Company Name: |
SuZhou ShiYa Biopharmaceuticals, Inc.
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| Tel: |
0512-0512-52358471 17715136450 |
| Email: |
sales@shiyabiopharm.com |
| Products Intro: |
Product Name:N-(2-Fluoro-4-methyl-phenyl)-acetamide
CAS:326-67-0
Purity:>97% Package:1g;5g Remarks:B1-1249
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| | Acetamide, N-(2-fluoro-4-methylphenyl)- Basic information |
| | Acetamide, N-(2-fluoro-4-methylphenyl)- Chemical Properties |
| storage temp. | Sealed in dry,Room Temperature | | Appearance | White to off-white Solid |
| | Acetamide, N-(2-fluoro-4-methylphenyl)- Usage And Synthesis |
| Synthesis | To a solution of 2-fluoro-4-methylaniline (250 g, 2 mol) and triethylamine (202 g, 2 mol) dissolved in 2 L of dichloromethane, acetyl chloride (156 g, 2 mol) was added slowly and dropwise. The reaction mixture was stirred at 0 °C for 2 h and subsequently washed with dilute hydrochloric acid. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude intermediate N-(2-fluoro-4-methylphenyl)acetamide (334 g, 87% yield). | | References | [1] Patent: WO2010/100189, 2010, A1. Location in patent: Page/Page column 70
[2] Patent: WO2013/30262, 2013, A1. Location in patent: Page/Page column 51
[3] Patent: WO2013/30319, 2013, A2. Location in patent: Page/Page column 45
[4] Patent: WO2013/30338, 2013, A2. Location in patent: Page/Page column 60 |
| | Acetamide, N-(2-fluoro-4-methylphenyl)- Preparation Products And Raw materials |
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