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1-ACETYLPIPERIDIN-4-OL

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1-ACETYLPIPERIDIN-4-OL Basic information
Uses
Product Name:1-ACETYLPIPERIDIN-4-OL
Synonyms:1-ACETYLPIPERIDIN-4-OL;ETHANONE, 1-(4-HYDROXY-1-PIPERIDINYL)-;OTAVA-BB 1272196;4-piperidinol, 1-acetyl-;Ethanone, 1-(4-hydroxy-1-...;1-acetyl-4-hydroxypiperidine;N-Acetyl-4-hydroxypiperidine;1-(4-hydroxy-1-piperidinyl)ethanone
CAS:4045-22-1
MF:C7H13NO2
MW:143.18
EINECS:
Product Categories:
Mol File:4045-22-1.mol
1-ACETYLPIPERIDIN-4-OL Structure
1-ACETYLPIPERIDIN-4-OL Chemical Properties
Melting point 70-73℃
Boiling point 143-145 °C
density 1.138±0.06 g/cm3(Predicted)
storage temp. 2-8°C
pka14.47±0.20(Predicted)
AppearanceWhite to off-white Solid
CAS DataBase Reference4045-22-1
Safety Information
HazardClass IRRITANT
HS Code 2933399990
MSDS Information
1-ACETYLPIPERIDIN-4-OL Usage And Synthesis
Uses1-Acetyl-4-piperidine can be used as a pharmaceutical synthesis intermediate, mainly in laboratory research and development processes and chemical and pharmaceutical synthesis processes.
SynthesisTriethylamine (6.41 mL) and acetic anhydride (3.49 mL) were added to a commercially available chloroform (50 mL) solution of 4-piperidinemethanol (3.98 g) and stirred at room temperature for 2 hours. Saturated aqueous sodium bicarbonate solution was added to the reaction mixture and the solvent was evaporated under reduced pressure. The resulting residue was purified by silica gel column chromatography (chloroform: methanol = 99:1 to 4:1) and then purified again by NH silica gel column chromatography (ethyl acetate: methanol = 99:1 to 4:1). Purification gave the title compound 1-acetyl-4-piperidine (4.87 g) as a colorless oil.
Tag:1-ACETYLPIPERIDIN-4-OL(4045-22-1) Related Product Information
Pazinaclone lamifiban 1-Benzyl-4-hydroxypiperidine KIFUNENSINE 2-CHLORO-2,2-DIFLUORO-1-(4-HYDROXYPIPERIDINO)-1-ETHANONE L371,257 (4-([(4-BROMOPHENYL)SULFANYL]METHYL)-4-HYDROXYPIPERIDINO)(4-CHLOROPHENYL)METHANONE (4-CHLOROPHENYL)(4-HYDROXY-4-([(4-METHYLPHENYL)SULFANYL]METHYL)PIPERIDINO)METHANONE (3,4-DICHLOROPHENYL)[4-HYDROXY-4-(MORPHOLINOMETHYL)PIPERIDINO]METHANONE 1-(Oxo(2-phenyl-1H-indol-3-yl)acetyl)-4-phenyl-4-piperidinol HPR 611 1-((6-Chloro-2,3-dihydro-2-(4-methoxyphenyl)-3-oxo-1H-isoindol-1-yl)ac etyl)-4-piperidinol 1,4-DIOXA-8-AZASPIRO[4.5]DEC-8-YL[1-(PHENYLSULFONYL)-4-PIPERIDINYL]METHANONE (4-CHLOROPHENYL)(4-HYDROXY-4-[(4-METHYLPHENOXY)METHYL]PIPERIDINO)METHANONE CBI-BB ZERO/005006 (4-CHLOROPHENYL)(4-([(4-CHLOROPHENYL)SULFANYL]METHYL)-4-HYDROXYPIPERIDINO)METHANONE (4-CHLOROPHENYL)(4-HYDROXY-4-[(PHENYLSULFANYL)METHYL]PIPERIDINO)METHANONE 1-(3-(4-Methoxyphenyl)-2-methyl-1-oxo-2-propenyl)-4-phenyl-4-piperidin ol