2-Methoxybenzylhydrazine dihydrochloride manufacturers
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| | 2-Methoxybenzylhydrazine dihydrochloride Basic information | | Synthesis |
| Product Name: | 2-Methoxybenzylhydrazine dihydrochloride | | Synonyms: | Methyl 4-trifluoromethylbenzoylacetate,95%;Methyl 3-oxo-3-[4-(trifluoromethyl)phenyl]propanoate;Methyl 4-trifluoroMethylbenzoylacetate, 95% 2.5GR;METHYL 4-TRIFLUOROMETHYLBENZOYLACETATE 95%;Methyl [4-(trifluoromethyl)benzoyl]acetate, 4-(3-Methoxy-3-oxopropanoyl)benzotrifluoride;JR-13912, Methyl 3-(4-(trifluoromethyl)phenyl)-3-oxopropanoate, 95%;2-methyl-3-oxo-3-[3-(trifluoromethyl)phenyl]propanoate;Methyl 3-(4-(trifluoromethyl)phenyl)-3-oxopropanoate | | CAS: | 212755-76-5 | | MF: | C11H9F3O3 | | MW: | 246.18 | | EINECS: | | | Product Categories: | Benzoic acid | | Mol File: | 212755-76-5.mol |  |
| | 2-Methoxybenzylhydrazine dihydrochloride Chemical Properties |
| Melting point | 58-61 | | Boiling point | 277.4±40.0 °C(Predicted) | | density | 1.3318 (estimate) | | storage temp. | Sealed in dry,Room Temperature | | solubility | soluble in Methanol | | pka | 9.06±0.25(Predicted) | | form | Crystalline Powder | | color | Yellow |
| Hazard Codes | Xi | | Safety Statements | 24/25 | | HazardClass | IRRITANT | | HS Code | 29183000 |
| | 2-Methoxybenzylhydrazine dihydrochloride Usage And Synthesis |
| Synthesis | 
1-(4-(trifluoromethyl)phenyl)ethyl ketone (15.27 g, 81.22 mmol, 1.00 equivalent), dimethyl carbonate (50 mL), and sodium hydride (5.53 g, 138.25 mmol, 1.70 equivalent, 60%) were placed in a 500 mL three-necked round-bottom flask. The resulting solution was stirred at 25 °C for 5 minutes. The mixture was concentrated by evaporation, the solid was collected by filtration, and washed with 3×50 mL H2O to give Methyl 4-(trifluoromethyl)benzoylacetate, a yellow solid, yield 19.28 g, 96%. | | Chemical Properties | yellow crystalline powder | | Uses | Methyl 4-trifluoromethylbenzoylacetate |
| | 2-Methoxybenzylhydrazine dihydrochloride Preparation Products And Raw materials |
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