N-BENZOYLIMIDAZOLE manufacturers
- N-BENZOYLIMIDAZOLE
-
- $1.00 / 1KG
-
2020-01-03
- CAS:10364-94-0
- Min. Order: 1KG
- Purity: 99%
- Supply Ability: 10000kgs
|
| | N-BENZOYLIMIDAZOLE Basic information |
| | N-BENZOYLIMIDAZOLE Chemical Properties |
| Melting point | 19-20 °C(Solv: ligroine (8032-32-4)) | | Boiling point | 120 °C | | density | 1.15±0.1 g/cm3(Predicted) | | Fp | 120-121°C/0.8mm | | storage temp. | Inert atmosphere,2-8°C | | solubility | Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly) | | pka | 3.65±0.10(Predicted) | | form | Oil | | color | Pale Yellow to Yellow | | Sensitive | Moisture Sensitive | | BRN | 125881 | | CAS DataBase Reference | 10364-94-0(CAS DataBase Reference) |
| Hazard Codes | Xi | | Risk Statements | 36/38 | | Safety Statements | 26-36/37/39 | | HazardClass | IRRITANT, MOISTURE SENSITIVE, KEEP COLD |
| Provider | Language |
|
ALFA
| English |
| | N-BENZOYLIMIDAZOLE Usage And Synthesis |
| Chemical Properties | Slightly Coloured Oil | | Synthesis Reference(s) | The Journal of Organic Chemistry, 54, p. 5620, 1989 DOI: 10.1021/jo00284a043
Tetrahedron, 36, p. 2409, 1980 DOI: 10.1016/0040-4020(80)80219-5 | | Synthesis | A suspension of imidazole (4.54 g, 0.0668 mol) in anhydrous benzene (200 mL) in a flask fitted with a drying apparatus was treated at 8C with a solution of benzoyl chloride (4.69 ) in benzene (20 mL).
g, 0.0333 mol) in benzene (20 mL). The mixture was allowed to warm to room temperature and stirred for 16 hours.
The precipitated imidazole hydrochloride was removed by filtration through a funnel and the clarified filtrate was concentrated under reduced pressure to give N-benzoyl imidazolylide as a viscous, hygroscopic oil in a yield of 5.78 g. It was stored at 0C in a tightly closed container. |
| | N-BENZOYLIMIDAZOLE Preparation Products And Raw materials |
|