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J & K SCIENTIFIC LTD.
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18210857532; 18210857532 |
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jkinfo@jkchemical.com |
| Products Intro: |
Product Name:4-bromo-2-thiophenecarboxamide(SALTDATA: FREE)
CAS:83933-17-9
Purity:95% Package:1G, 5G, 10G, 25G
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| | 4-BROMO-2-THIOPHENECARBOXAMIDE Basic information |
| Product Name: | 4-BROMO-2-THIOPHENECARBOXAMIDE | | Synonyms: | 4-BROMO-2-THIOPHENECARBOXAMIDE;4-bromothiophene-2-carboxamide;2-thiophenecarboxamide, 4-bromo-;4-bromo-2-thiophenecarboxamide(SALTDATA: FREE) | | CAS: | 83933-17-9 | | MF: | C5H4BrNOS | | MW: | 206.06 | | EINECS: | | | Product Categories: | | | Mol File: | 83933-17-9.mol |  |
| | 4-BROMO-2-THIOPHENECARBOXAMIDE Chemical Properties |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature | | Appearance | White to off-white Solid |
| Risk Statements | 43 | | Safety Statements | 36/37 | | HazardClass | IRRITANT |
| | 4-BROMO-2-THIOPHENECARBOXAMIDE Usage And Synthesis |
| Synthesis | The general procedure for the synthesis of 4-bromothiophene-2-carboxamide from the compound (CAS: 31767-01-8) is as follows: in a 25 mL round-bottomed flask equipped with a magnetic stirrer, aldoxime (5 mmol), copper(II) acetate (45 mg, 0.25 mmol), acetonitrile (10 mg, 0.25 mmol), and ethanol (15 mL) were added in sequence. The reaction mixture was stirred for 4-8 hours at 78 °C or 12 hours at room temperature. After completion of the reaction, the solvent was removed by rotary evaporator. The crude product was purified by column chromatography to afford the target compound 4-bromothiophene-2-carboxamide. | | References | [1] RSC Advances, 2016, vol. 6, # 43, p. 37093 - 37098
[2] Journal of Chemical Research, 2016, vol. 40, # 10, p. 594 - 596
[3] Bulletin de la Societe Chimique de France, 1967, p. 4115 - 4120 |
| | 4-BROMO-2-THIOPHENECARBOXAMIDE Preparation Products And Raw materials |
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