2-Bromoindene

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2-Bromoindene manufacturers

  • 2-Bromoindene
  • 2-Bromoindene pictures
  • 2026-09-11
  • CAS:10485-09-3
  • Min. Order: 1KG
  • Purity: 98%min
  • Supply Ability: 30tons/month
  • 2-Bromoindene
  • 2-Bromoindene pictures
  • $1.10
  • 2026-08-20
  • CAS:10485-09-3
  • Min. Order: 1g
  • Purity: 99.00%
  • Supply Ability: 100 Tons
  • 2-Bromoindene
  • 2-Bromoindene pictures
  • $15.00
  • 2021-07-02
  • CAS:10485-09-3
  • Min. Order: 1KG
  • Purity: 99%+ HPLC
2-Bromoindene Basic information
Product Name:2-Bromoindene
Synonyms:2-BROMOINDENE;1H-INDENE, 2-BROMO-;2-BroMoindene, 95+%;2-Bromoindene,99%;2-Bromoindene >;2-Bromoindene ISO 9001：2015 REACH;ETTD;2- indene bromide
CAS:10485-09-3
MF:C9H7Br
MW:195.06
EINECS:678-249-5
Product Categories:Indoles and derivatives
Mol File:10485-09-3.mol
2-Bromoindene Structure
2-Bromoindene Chemical Properties
Melting point 35-37°C
Boiling point 127 °C / 23mmHg
density 1.570±0.06 g/cm3(Predicted)
storage temp. Inert atmosphere,2-8°C
form powder to crystal
color White to Light yellow to Light orange
Water Solubility Insoluble in water.
InChIInChI=1S/C9H7Br/c10-9-5-7-3-1-2-4-8(7)6-9/h1-5H,6H2
InChIKeyCCUYEVNCRQDQRF-UHFFFAOYSA-N
SMILESC1C2=C(C=CC=C2)C=C1Br
CAS DataBase Reference10485-09-3(CAS DataBase Reference)
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 37/39-26
Hazard Note Irritant
HS Code 29036990
MSDS Information
ProviderLanguage
ACROS English
2-Bromoindene Usage And Synthesis
Chemical PropertiesYellow to pale brown low melting solid
Uses2-Bromoindene is used as pharmaceutical intermediate.
Synthesis
2-Bromo-1-indanol

5400-80-6

2-Bromoindene

10485-09-3

General procedure for the synthesis of 2-bromoindene from 2-bromo-1-indanol: In a 25 mL round-bottomed flask, 250 mg (1.2 mmol) of 2-bromo-1-phenylethanol (1a), 50 mg (20 wt%) of H-β zeolite and 1.0 mL of chlorobenzene were added. The reaction flask was heated in an oil bath at 120 °C for 6 h. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the flask was cooled to room temperature and the reaction mixture was filtered through Wattman filter paper and the filter cake was washed with 10 mL of diethyl ether. The filtrate was concentrated under reduced pressure to remove the solvent. The resulting crude product was purified by column chromatography on silica gel (200-400 mesh) to afford 2-bromoindene (2a, 0.16 g) in 72% yield using hexane as eluent.

References[1] Tetrahedron Letters, 2014, vol. 55, # 10, p. 1793 - 1795
[2] Patent: US2016/194422, 2016, A1. Location in patent: Paragraph 0129; 0138
[3] Journal of Organic Chemistry, 1982, vol. 47, # 4, p. 705 - 709
[4] Patent: EP2390249, 2011, A2. Location in patent: Page/Page column 20-21
[5] Journal of Medicinal Chemistry, 2006, vol. 49, # 7, p. 2222 - 2231
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