| Company Name: |
Energy Chemical |
| Tel: |
400-0056266 |
| Email: |
sales8178@energy-chemical.com |
- ETHYL-O-TOLYL KETONE
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- $1.00
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2020-01-09
- CAS:2040-14-4
- Min. Order: 1KG
- Purity: 98% HPLC
- Supply Ability: 10 tons/month
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| | ETHYL-O-TOLYL KETONE Basic information |
| Product Name: | ETHYL-O-TOLYL KETONE | | Synonyms: | 2'-Methylpropiophenone 98%;1-(2-Methylphenyl)propan-1-one, 2-(Ethylcarbonyl)toluene;2'-Methylpropiophenone98%;O-METHYL-PROPIOPHENONE;ETHYL-O-TOLYL KETONE;o-Methyl-propiophenone, 97 % min.;1-(2-methylphenyl)propan-1-one;Tolperisone Impurity D | | CAS: | 2040-14-4 | | MF: | C10H12O | | MW: | 148.2 | | EINECS: | | | Product Categories: | | | Mol File: | 2040-14-4.mol |  |
| | ETHYL-O-TOLYL KETONE Chemical Properties |
| Melting point | -27.6°C | | Boiling point | 219.5°C (estimate) | | density | 1.0119 | | refractive index | 1.5413 (estimate) | | storage temp. | Sealed in dry,Room Temperature | | solubility | Chloroform (Sparingly), Methanol (Slightly) | | form | liquid | | color | Light Yellow | | InChI | InChI=1S/C10H12O/c1-3-10(11)9-7-5-4-6-8(9)2/h4-7H,3H2,1-2H3 | | InChIKey | VQHKICGSBBPFFJ-UHFFFAOYSA-N | | SMILES | C(C1=CC=CC=C1C)(=O)CC |
| | ETHYL-O-TOLYL KETONE Usage And Synthesis |
| Uses | 2'-Methylpropiophenone can be used for volatile component analysis in infant formula using SPME coupled with GCxGC-TOFMS. | | Synthesis | 1-(p-formyl)ethanol (1 mmol) was used as starting material with chloramine-T (1 mmol) and In(OTf)3 (0.3 mmol) in a 100 mL round-bottomed flask fitted with a magnetic stirrer and dissolved in acetonitrile (10 mL). The reaction mixture was heated and refluxed under argon protection for 3 h. The reaction progress was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the mixture was cooled to room temperature and the solvent was removed by rotary evaporator. The residue was purified by fast column chromatography on silica gel. The final product was analyzed by spectroscopy for structural confirmation. | | References | [1] Journal of Organic Chemistry, 1986, vol. 51, # 9, p. 1402 - 1406
[2] Phytochemistry, 2013, vol. 96, p. 223 - 234
[3] European Journal of Medicinal Chemistry, 1995, vol. 30, # 1, p. 85 - 94
[4] Journal of Organic Chemistry, 2003, vol. 68, # 4, p. 1594 - 1596
[5] Chemical and Pharmaceutical Bulletin, 2017, vol. 65, # 8, p. 801 - 804 |
| | ETHYL-O-TOLYL KETONE Preparation Products And Raw materials |
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