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| | 2-ethoxy-5-methylaniline Basic information |
| Product Name: | 2-ethoxy-5-methylaniline | | Synonyms: | 2-ethoxy-5-methylbenzenamine;Benzenamine,2-ethoxy-5-methyl-;o-Amino-p-toluene ethyl ether;2-Ethoxy-5-methyl-anilin;5-Methyl-o-phenetidine;6-Ethoxy-3-methylaniline;6-Ethoxy-m-toluidine;(2-ethoxy-5-methyl-phenyl)amine | | CAS: | 6331-70-0 | | MF: | C9H13NO | | MW: | 151.21 | | EINECS: | 228-708-7 | | Product Categories: | | | Mol File: | 6331-70-0.mol |  |
| | 2-ethoxy-5-methylaniline Chemical Properties |
| storage temp. | Keep in dark place,Inert atmosphere,Room temperature | | Appearance | Yellow to brown Solid |
| | 2-ethoxy-5-methylaniline Usage And Synthesis |
| Synthesis | General procedure for the synthesis of 2-amino-4-methylphenylethyl ether from 4-ethoxy-3-nitrotoluene: A suspension formed by 1-ethoxy-4-methyl-2-nitrobenzene (2.71 g) with 10% palladium-carbon catalyst (0.27 g) in anhydrous tetrahydrofuran (40 mL) was stirred at room temperature. After 25.5 hours of reaction in a hydrogen atmosphere, the reaction mixture was filtered through cellulose powder. The filtrate was concentrated under reduced pressure and dried to give 2.26 g of 2-amino-4-methylphenylethyl ether as a dark brown solid in 100% yield. | | References | [1] Patent: EP1764360, 2007, A1. Location in patent: Page/Page column 106
[2] Justus Liebigs Annalen der Chemie, 1883, vol. 217, p. 172
[3] Gazzetta Chimica Italiana, 1969, vol. 99, p. 397 - 410 |
| | 2-ethoxy-5-methylaniline Preparation Products And Raw materials |
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